CN106699302A - Special fertilizer for flowering and fruit bearing stage of Shatian pomelos - Google Patents
Special fertilizer for flowering and fruit bearing stage of Shatian pomelos Download PDFInfo
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- CN106699302A CN106699302A CN201611266650.6A CN201611266650A CN106699302A CN 106699302 A CN106699302 A CN 106699302A CN 201611266650 A CN201611266650 A CN 201611266650A CN 106699302 A CN106699302 A CN 106699302A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/50—Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- General Chemical & Material Sciences (AREA)
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- Fertilizers (AREA)
Abstract
The invention relates to the field of Shatian pomelo planting and discloses a special fertilizer for the flowering and fruit bearing stage of Shatian pomelos. The special fertilizer consists of the following components: artificial water-logged compost, monopotassium phosphate, calcium superphosphate, ammonium hydrogen phosphate, potassium nitrate, calcium hydrogen phosphate, magnesium nitrate, sulfur and micro-element fertilizer. Fertilization management in the flowering and fruit bearing stage of Shatian pomelos plays a crucial role in yield and quality; however, the existing fertilization method unavoidably adopts urea to supplement nitrogen fertilizer, and the urea takes effect very slowly at the temperature of the flowering and fruit bearing stage of Shatian pomelos, so that the nutrition supply for the flowering and fruit bearing stage is easily missed, and more importantly, biuret in the urea seriously hinders the increase of the fruit setting rate. In the invention, the problem is solved by use of the artificial water-logged compost, the yield is increased by over 40%, and the sugar content of pomelos is increased by 15-20%.
Description
Technical field
The present invention relates to shatian pomelo field of planting, and in particular to a kind of shatian pomelo flowering fruit bearing stage special fertilizer.
Background technology
Shatian pomelo original name poplar nucleon, according to legend old times Rong County Shatian village there is the summer law being an official in other places to take back two plants of poplar cores
Sub- seed is planted on the fertile soil of the side of a pond and household's intensive care is advised, and poplar nucleon is original not only sour but also puckery in order to change fruit quality
The tender and crisp fragrant and sweet, fruit that sweet taste is good to eat is cultivated into finally by pains cultivation.The ground that summer law is an official is come in later emperor's tour of inspection
Square summer law just dedicates this fruit to can't help rainning praise on " nice " and calling in the inquiry of summer law after emperor emperor eats
He Jiaguo.Summer law is replied and " is poplar nucleon." " this fruit name is not good should separately to take fruit name in emperor road." minister say the summer on side
Government authorities Shatian mail from afar good fruit dedicate to the emperor according to the postal of minister my humble opinion by unisonance again therefore fruit for arbor is given birth to wooden side
It is suitable that " shaddock " is referred to as " shatian pomelo ".Emperor listens to stop imperial countenance exultation and blurt out and praises " shatian pomelo is carefully " shatian pomelo one and obtain praising for emperor
Reward just quickly procreation get up the soil for planting more and more there near the village of Shatian be particularly suitable for its growth produce shaddock really truly have it is " sweet
The characteristics of crisp slag only authentic brand that disappears ", Shatian was also referred to as in " township of shaddock ".County other than where one lives other provinces come to introduce a fine variety one after another after reputation spreads
Although product quality can not catch up with completely tunnel shatian pomelo be just also fruit in top grade because introduces a collection from Shatian again and hold its reputation
It is reluctant that setting up another alias still continues to use the name of shatian pomelo until today.
Shatian pomelo is loved by people with its abundant nutrition and sour-sweet mouthfeel, and annual listing season turns into the head of people
Fruit is selected, nowadays the planting range of shatian pomelo is also not limited to Guangxi province, middle part can also plant out good sand
Field shaddock, but because fertilizing management is referring also to the pattern of other fruit trees, cause the yield of shatian pomelo not high, and quality is also unstable
It is fixed.
The content of the invention
In order to solve the problems, such as current shatian pomelo yield poorly, quality it is unstable, the invention provides a kind of shatian pomelo flowers and fruits
Phase special fertilizer, more than 40% by output increased, and the sugar content of shaddock improves 15-20%.
The present invention is achieved by the following technical solutions:
A kind of shatian pomelo flowering fruit bearing stage special fertilizer, consists of the following composition in parts by weight:Manually make compost 120-150 parts, phosphoric acid
Potassium dihydrogen 10-14 parts, calcium superphosphate 11-13 parts, ammonium hydrogen phosphate 8.8-9.2 parts, potassium nitrate 7.7-7.9 parts, calcium monohydrogen phosphate 5.6-
5.8 parts, magnesium nitrate 3.2-3.6 parts, sulphur 0.4-0.6 parts, it is micro- fertile 0.05-0.06 parts.
Further described as to such scheme, it is described artificial to make compost preparation method and be:
(1)Prepare following raw material in parts by weight:Humus 100-110 parts, chicken manure 60-70 parts, vinasse 50-60 parts, biogas
Liquid 40-50 parts, discarded 35-38 parts of mushroom matrix, 30-35 parts of fish pond mud, powder of straw 20-30 parts, corn stalk powder 15-20 parts,
Chinese medicine slag 10-15 parts, water 150-200 parts, using humus as soil nutrient main source, grapefruit not only absorbs to it
Saturation is higher, and physics to shatian pomelo, chemistry, biological property all have a major impact, and can effectively facilitate photosynthesis
And improve percentage of fertile fruit;
(2)The raw material of above-mentioned weight portion is well mixed, ventilation fermentation is placed in, temperature survey dress is installed in the middle of fermentation heap
Put, the center fermentation temperature for the treatment of reaches 55-60 DEG C, fermentation heap and overlay film are stirred again, carried out after discharging substantial amounts of carbon dioxide
Fermentation can reduce acidity, continue to ferment 30-35 days;
(3)After fermentation ends, overlay film is opened, fermentation heap is divided, dried at 25-35 DEG C to water content in 65-75% scopes,
Can build up fertility, you can use.
Further described as to such scheme, each element fertilizer mass content is in micro- fertilizer:Boron fertilizer account for 15-20%,
Zinc fertilizer account for 17-20%, molydbenum fertilizer account for 10-15%, manganese fertilizer account for 8-12%, copper fertilizer account for 5-7%, remaining as iron fertilizer content, promote plant hormone
Synthesis, with reach volume increase stable yields effect.
Further described as to such scheme, the fertile application method is:Depth is dug out around Shatian Pomelo root
It is 15-20 centimetres, radius is 40-50 centimetres of hole, the earthing landfill after uniformly apply fertilizer of the invention in hole the dusk, and
Watered, this is done so that shatian pomelo is high to the absorption rate of fertilizer.
Further described as to such scheme, the fertile usage amount is:Average every plant of shatian pomelo applies fertilizer consumption every time
It it is 2-3 kilograms, the flowers are in blossom, the initial stage uses once, is used once when young fruit is formed, the nutrient needed for supplementing shatian pomelo enough.
Beneficial effects of the present invention:It is because shatian pomelo is in flowers and fruits that existing shatian pomelo yield and quality cannot be improved
The fertilizing management of phase plays vital effect for yield and quality, and existing fertilizing method will unavoidably use urea
Supplement nitrogenous fertilizer, the temperature that shatian pomelo was yielded positive results under period, urea action effect is extremely slow, it is easy to miss the nutrition of florescence fruiting period
Supply, the biuret in what is more important urea seriously hinders the raising of percentage of fertile fruit, present invention utilizes artificial preparation
Make compost and solve this problem, more than 40% by output increased, and the sugar content of shaddock improves 15-20%, the sand for obtaining
Field shaddock pulp is sharp and clear, and grain grain is full, and taste giving off a strong fragrance is sweet.
Specific embodiment
With reference to specific embodiment, the present invention will be further described.
Embodiment 1
A kind of shatian pomelo flowering fruit bearing stage special fertilizer, consists of the following composition in parts by weight:Manually make compost 120 parts, biphosphate
10 parts of potassium, 11 parts of calcium superphosphate, 8.8 parts of ammonium hydrogen phosphate, 7.7 parts of potassium nitrate, 5.6 parts of calcium monohydrogen phosphate, 3.2 parts of magnesium nitrate, sulphur
0.4 part, micro- fertile 0.05 part.
Further described as to such scheme, it is described artificial to make compost preparation method and be:
(1)Prepare following raw material in parts by weight:It is 100 parts of humus, 60 parts of chicken manure, 50 parts of vinasse, 40 parts of methane liquid, discarded
35 parts of mushroom matrix, 30 parts of fish pond mud, 20 parts of powder of straw, 15 parts of corn stalk powder, 10 parts of Chinese medicine slag, 150 parts of water, use humic
Matter as soil nutrient main source, grapefruit not only absorbs that saturation is higher to it, and physics to shatian pomelo, changes
Learn, biological property all has a major impact, photosynthesis can be effectively facilitated and percentage of fertile fruit is improved;
(2)The raw material of above-mentioned weight portion is well mixed, ventilation fermentation is placed in, temperature survey dress is installed in the middle of fermentation heap
Put, the center fermentation temperature for the treatment of reaches 55 DEG C, fermentation heap and overlay film are stirred again, fermented after discharging substantial amounts of carbon dioxide
Acidity can be reduced, continues to ferment 30 days;
(3)After fermentation ends, overlay film is opened, fermentation heap is divided, dried at 25 DEG C to water content in 65-75% scopes, can be with
Build up fertility, you can use.
Further described as to such scheme, each element fertilizer mass content is in micro- fertilizer:Boron fertilizer accounts for 15%, zinc
Fertilizer account for 17%, molydbenum fertilizer account for 10%, manganese fertilizer account for 8%, copper fertilizer account for 5%, remaining as iron fertilizer content, promote the synthesis of plant hormone, to reach
Increase production the effect of stable yields.
Further described as to such scheme, the fertile application method is:Depth is dug out around Shatian Pomelo root
It is 15 centimetres, radius is 40 centimetres of hole, the earthing landfill after uniformly apply fertilizer of the invention in hole the dusk, and poured
Water, this is done so that shatian pomelo is high to the absorption rate of fertilizer.
Further described as to such scheme, the fertile usage amount is:Average every plant of shatian pomelo applies fertilizer consumption every time
It it is 2 kilograms, the flowers are in blossom, the initial stage uses once, is used once when young fruit is formed, the nutrient needed for supplementing shatian pomelo enough.
Embodiment 2
A kind of shatian pomelo flowering fruit bearing stage special fertilizer, consists of the following composition in parts by weight:Manually make compost 135 parts, biphosphate
12 parts of potassium, 12 parts of calcium superphosphate, 9.0 parts of ammonium hydrogen phosphate, 7.8 parts of potassium nitrate, 5.7 parts of calcium monohydrogen phosphate, 3.4 parts of magnesium nitrate, sulphur
0.5 part, micro- fertile 0.055 part.
Further described as to such scheme, it is described artificial to make compost preparation method and be:
(1)Prepare following raw material in parts by weight:It is 105 parts of humus, 65 parts of chicken manure, 55 parts of vinasse, 45 parts of methane liquid, discarded
36 parts of mushroom matrix, 33 parts of fish pond mud, 25 parts of powder of straw, 17 parts of corn stalk powder, 12 parts of Chinese medicine slag, 180 parts of water, use humic
Matter as soil nutrient main source, grapefruit not only absorbs that saturation is higher to it, and physics to shatian pomelo, changes
Learn, biological property all has a major impact, photosynthesis can be effectively facilitated and percentage of fertile fruit is improved;
(2)The raw material of above-mentioned weight portion is well mixed, ventilation fermentation is placed in, temperature survey dress is installed in the middle of fermentation heap
Put, the center fermentation temperature for the treatment of reaches 57 DEG C, fermentation heap and overlay film are stirred again, fermented after discharging substantial amounts of carbon dioxide
Acidity can be reduced, continues to ferment 33 days;
(3)After fermentation ends, overlay film is opened, fermentation heap is divided, dried at 30 DEG C to water content in 65-75% scopes, can be with
Build up fertility, you can use.
Further described as to such scheme, each element fertilizer mass content is in micro- fertilizer:Boron fertilizer accounts for 17%, zinc
Fertilizer account for 18%, molydbenum fertilizer account for 12%, manganese fertilizer account for 10%, copper fertilizer account for 6%, remaining as iron fertilizer content, promote the synthesis of plant hormone, to reach
Increase production the effect of stable yields.
Further described as to such scheme, the fertile application method is:Depth is dug out around Shatian Pomelo root
It is 17 centimetres, radius is 45 centimetres of hole, the earthing landfill after uniformly apply fertilizer of the invention in hole the dusk, and poured
Water, this is done so that shatian pomelo is high to the absorption rate of fertilizer.
Further described as to such scheme, the fertile usage amount is:Average every plant of shatian pomelo applies fertilizer consumption every time
It it is 2.5 kilograms, the flowers are in blossom, the initial stage uses once, is used once when young fruit is formed, the nutrient needed for supplementing shatian pomelo enough.
Embodiment 3
A kind of shatian pomelo flowering fruit bearing stage special fertilizer, consists of the following composition in parts by weight:Manually make compost 150 parts, biphosphate
14 parts of potassium, 13 parts of calcium superphosphate, 9.2 parts of ammonium hydrogen phosphate, 7.9 parts of potassium nitrate, 5.8 parts of calcium monohydrogen phosphate, 3.6 parts of magnesium nitrate, sulphur
0.6 part, micro- fertile 0.06 part.
Further described as to such scheme, it is described artificial to make compost preparation method and be:
(1)Prepare following raw material in parts by weight:It is 110 parts of humus, 70 parts of chicken manure, 60 parts of vinasse, 50 parts of methane liquid, discarded
38 parts of mushroom matrix, 35 parts of fish pond mud, 30 parts of powder of straw, 20 parts of corn stalk powder, 15 parts of Chinese medicine slag, 200 parts of water, use humic
Matter as soil nutrient main source, grapefruit not only absorbs that saturation is higher to it, and physics to shatian pomelo, changes
Learn, biological property all has a major impact, photosynthesis can be effectively facilitated and percentage of fertile fruit is improved;
(2)The raw material of above-mentioned weight portion is well mixed, ventilation fermentation is placed in, temperature survey dress is installed in the middle of fermentation heap
Put, the center fermentation temperature for the treatment of reaches 60 DEG C, fermentation heap and overlay film are stirred again, fermented after discharging substantial amounts of carbon dioxide
Acidity can be reduced, continues to ferment 35 days;
(3)After fermentation ends, overlay film is opened, fermentation heap is divided, dried at 35 DEG C to water content in 65-75% scopes, can be with
Build up fertility, you can use.
Further described as to such scheme, each element fertilizer mass content is in micro- fertilizer:Boron fertilizer accounts for 20%, zinc
Fertilizer account for 20%, molydbenum fertilizer account for 15%, manganese fertilizer account for 12%, copper fertilizer account for 7%, remaining as iron fertilizer content, promote the synthesis of plant hormone, to reach
Increase production the effect of stable yields.
Further described as to such scheme, the fertile application method is:Depth is dug out around Shatian Pomelo root
It is 20 centimetres, radius is 50 centimetres of hole, the earthing landfill after uniformly apply fertilizer of the invention in hole the dusk, and poured
Water, this is done so that shatian pomelo is high to the absorption rate of fertilizer.
Further described as to such scheme, the fertile usage amount is:Average every plant of shatian pomelo applies fertilizer consumption every time
It it is 3 kilograms, the flowers are in blossom, the initial stage uses once, is used once when young fruit is formed, the nutrient needed for supplementing shatian pomelo enough.
Comparative example 1
With the urea that making compost artificial in embodiment 1 and changing isodose into of differing only in of embodiment 1, other contents are constant.
Comparative example 2
With the urea that making compost artificial in embodiment 2 and changing isodose into of differing only in of embodiment 2, other contents are constant.
Comparative example 3
With the urea that making compost artificial in embodiment 3 and changing isodose into of differing only in of embodiment 3, other contents are constant.
Contrast test
Fertilizing management, every group of random division are carried out to the shatian pomelo of same planting site using the fertilizer of embodiment and comparative example respectively
Test tree, is respectively 50, and shatian pomelo yield and quality results statistics is as shown in the table:
Be can be seen that by comparing:The present invention is solved existing for the effect of being significantly improved of the yield and quality of shatian pomelo
There is the yield of shatian pomelo not high, and the also unstable problem of quality.
Claims (5)
1. a kind of shatian pomelo flowering fruit bearing stage special fertilizer, it is characterised in that consist of the following composition in parts by weight:Manually make compost
120-150 parts, potassium dihydrogen phosphate 10-14 parts, calcium superphosphate 11-13 parts, ammonium hydrogen phosphate 8.8-9.2 parts, potassium nitrate 7.7-7.9
Part, calcium monohydrogen phosphate 5.6-5.8 parts, magnesium nitrate 3.2-3.6 parts, sulphur 0.4-0.6 parts, it is micro- fertile 0.05-0.06 parts.
2. a kind of shatian pomelo flowering fruit bearing stage special fertilizer according to claim 1, it is characterised in that described manually to make compost preparation side
Method is:
(1)Prepare following raw material in parts by weight:Humus 100-110 parts, chicken manure 60-70 parts, vinasse 50-60 parts, biogas
Liquid 40-50 parts, discarded 35-38 parts of mushroom matrix, 30-35 parts of fish pond mud, powder of straw 20-30 parts, corn stalk powder 15-20 parts,
Chinese medicine slag 10-15 parts, water 150-200 parts;
(2)The raw material of above-mentioned weight portion is well mixed, ventilation fermentation is placed in, temperature survey dress is installed in the middle of fermentation heap
Put, the center fermentation temperature for the treatment of reaches 55-60 DEG C, fermentation heap and overlay film are stirred again, continue to ferment 30-35 days;
(3)After fermentation ends, overlay film is opened, fermentation heap is divided, dried at 25-35 DEG C to water content in 65-75% scopes,
Can be used.
3. a kind of shatian pomelo flowering fruit bearing stage special fertilizer according to claim 1, it is characterised in that each element fertilizer in micro- fertilizer
Mass content is:Boron fertilizer accounts for 15-20%, zinc fertilizer and accounts for 17-20%, molydbenum fertilizer and account for 10-15%, manganese fertilizer and account for 8-12%, copper fertilizer and accounts for 5-7%, residue
It is iron fertilizer content.
4. a kind of shatian pomelo flowering fruit bearing stage special fertilizer according to claim 1, it is characterised in that the fertile application method is:
Depth is dug out around Shatian Pomelo root for 15-20 centimetres, radius is 40-50 centimetres of hole, in the dusk by fertilizer of the invention
It is uniform to apply rear earthing landfill in hole, and watered.
5. a kind of shatian pomelo flowering fruit bearing stage special fertilizer according to claim 1, it is characterised in that the fertile usage amount is:It is flat
Every plant shatian pomelo applies fertilizer consumption for 2-3 kilograms every time, and the flowers are in blossom, the initial stage uses once, when young fruit is formed using once.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107556096A (en) * | 2017-08-22 | 2018-01-09 | 广西容县兴邦有机肥有限公司 | A kind of shatian pomelo fertilizer special for organic |
CN107624480A (en) * | 2017-09-30 | 2018-01-26 | 广西吉朋投资有限公司 | A kind of grapefruit high-yield cultivating method |
CN107739231A (en) * | 2017-12-16 | 2018-02-27 | 柳州市合联农业有限公司 | A kind of tulip nutrition composite fertilizer and preparation method thereof |
CN108059494A (en) * | 2018-02-01 | 2018-05-22 | 云南省农业科学院热带亚热带经济作物研究所 | A kind of crystal shaddock fruit retention fertilizer and preparation method and application |
CN108191571A (en) * | 2018-01-29 | 2018-06-22 | 广西驰胜农业科技有限公司 | A kind of shatian pomelo rush spends strong fruit organic fertilizer and preparation method thereof |
CN109463192A (en) * | 2018-11-20 | 2019-03-15 | 界首市百果园农业科技有限公司 | A method of extending the mulberry tree result time limit |
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CN105237298A (en) * | 2015-09-28 | 2016-01-13 | 广西洪喜肥业有限公司 | Citrus reticulata blanco compound fertilizer and production method thereof |
CN105254452A (en) * | 2015-11-02 | 2016-01-20 | 大新县生产力促进中心 | Fertilizer for fruit trees and production method of fertilizer |
CN105732236A (en) * | 2016-05-05 | 2016-07-06 | 云南省农业科学院热带亚热带经济作物研究所 | Biological organic fertilizer and preparation method thereof |
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CN105237298A (en) * | 2015-09-28 | 2016-01-13 | 广西洪喜肥业有限公司 | Citrus reticulata blanco compound fertilizer and production method thereof |
CN105254452A (en) * | 2015-11-02 | 2016-01-20 | 大新县生产力促进中心 | Fertilizer for fruit trees and production method of fertilizer |
CN105732236A (en) * | 2016-05-05 | 2016-07-06 | 云南省农业科学院热带亚热带经济作物研究所 | Biological organic fertilizer and preparation method thereof |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107556096A (en) * | 2017-08-22 | 2018-01-09 | 广西容县兴邦有机肥有限公司 | A kind of shatian pomelo fertilizer special for organic |
CN107624480A (en) * | 2017-09-30 | 2018-01-26 | 广西吉朋投资有限公司 | A kind of grapefruit high-yield cultivating method |
CN107739231A (en) * | 2017-12-16 | 2018-02-27 | 柳州市合联农业有限公司 | A kind of tulip nutrition composite fertilizer and preparation method thereof |
CN108191571A (en) * | 2018-01-29 | 2018-06-22 | 广西驰胜农业科技有限公司 | A kind of shatian pomelo rush spends strong fruit organic fertilizer and preparation method thereof |
CN108059494A (en) * | 2018-02-01 | 2018-05-22 | 云南省农业科学院热带亚热带经济作物研究所 | A kind of crystal shaddock fruit retention fertilizer and preparation method and application |
CN109463192A (en) * | 2018-11-20 | 2019-03-15 | 界首市百果园农业科技有限公司 | A method of extending the mulberry tree result time limit |
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Application publication date: 20170524 |
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RJ01 | Rejection of invention patent application after publication |