CN106565348A - Pest-resistant organic mineral element foliar fertilizer and preparation method thereof - Google Patents
Pest-resistant organic mineral element foliar fertilizer and preparation method thereof Download PDFInfo
- Publication number
- CN106565348A CN106565348A CN201610987532.8A CN201610987532A CN106565348A CN 106565348 A CN106565348 A CN 106565348A CN 201610987532 A CN201610987532 A CN 201610987532A CN 106565348 A CN106565348 A CN 106565348A
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- pest
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a pest-resistant organic mineral element foliar fertilizer and a preparation method thereof. The pest-resistant organic mineral element foliar fertilizer is prepared by the following raw materials in parts by weight: plant-source fresh material, ethyl acetate, ethanol, fish bone meal, chitosan, salicylic acid, medical stone, iron ore powder, agricultural rare earth, soybean meal, potato skins, EM bacterium agent, sheep manure ball, zinc powder, plant ash and a proper amount of water. According to the technical scheme of the invention, a pest-resistant foliar fertilizer containing various organic mineral elements is finally prepared. Mineral type rocks are subjected to pyrolysis treatment, and then are mixed with organic matters to be subjected to fermentation together with the organic matters. The fermentation process is also a slowly chelating process, so that organic matters are corrupted in the forward direction. Organic acid complex mineral elements are generated through the corruption of organic matters, and the elements are prepared and absorbed more easily. Therefore, the pest-resistant organic mineral element foliar fertilizer, which is momentarily retained, is remarkable in fertilizer effect.
Description
Technical field
The invention belongs to the Technology field of fertilizer, and in particular to a kind of insect pest organic mineral element foliage fertilizer and
Its preparation method.
Background technology
Plant waxiness is having for element of the first species's complexity that plant is formed to adapt to external environment in growth and development process
The general name of machine mixture, is covered in exposed aerial plant tissue, including the bolt matter substrate of underground, calluss and flower
Powder etc., plays a part of to protect plant.Its main component has aliphatic compound, cyclic compound, phytosterin compound etc.,
With aliphatic compound, including long-chain fatty acid, aldehyde, primary and secondary alcohol etc. are modal components.The thing of plant surface waxiness
Physical chemistry characteristic can resist various biological with abiotic infringement, and these infringements include fungal disease, plant-feed insect, too
Positive ray, solidification point etc..
The arena that plant surface waxiness or plant, plant-feed insect and its Predator and host marking interact, its
It is plant and phytophagous elder brother that distinctive chemical composition and morphological feature give one of its distinctive ecological function, these functions
The medium of the interphase interaction of worm.The physical arrangement and quantity of plant surface waxiness can affect the attachment and shifting of plant-feed insect
It is dynamic.Surface waxiness can pass through the predation for affecting the hostile phytophagous insect in day, so as to the behavior of remote-effects phytophagous insect.Surface
Waxiness extract and single wax component can stimulate or suppress plant-feed insect spawning, activity and take food.Alkane, wax
The aliphatic compounds such as ester, free alkyl alcohol and acid are the main components of surface waxiness, select host plant in plant-feed insect
In, aliphatic compound plays particularly important effect；Aromatic compound also affects selection of the insecticide to host plant.
Plant-feed insect is less to be taken food on the few phenotypic crop of smooth waxiness, on the few phenotypic crop of smooth waxiness, surface
The quantity of waxiness is few, and chemical constituent and morphological feature are also different.Surface waxiness can pass through to affect the hostile phytophagous insect in day
Predation, so as to the behavior of remote-effects phytophagous insect.The adhesive ability of the multipair natural enemy of surface waxiness has detrimental effect, such as may be used
Reduce the predations of the natural enemy insect to plant-feed insect such as Chrysopa, the considerable ladybug of anchor speckle, minute pirate bugs.
The wax coat on blade top layer is into these waxinesss are protecting blade by high light spoke by hydrophobic compound group
Penetrate, the infringement of insect and microorganism serves very crucial effect, but the using effect which results in foliage fertilizer is not good, one
The characteristics of aspect foliage fertilizer will overcome surface hydrophobicity, stops in the effective time of blade face in foliage fertilizer, is extremely difficult to good effect
Really, and foliage fertilizer is substantially into blade, have experiment to prove that the thin blade of waxiness absorbs by way of free diffusing
Nutrient is more preferable.
The content of the invention
The present invention seeks to improve adhesive force of the foliage fertilizer on crop leaf surface, absorbability and the life of foliage fertilizer are improved
Thing insect resistance capacity, invention develop a kind of foliage fertilizer that with the addition of plant leaf blade top layer waxiness, realize particular by following methods
's：
A kind of insect pest organic mineral element foliage fertilizer, it is characterised in that be made up of the raw material of following weight portion：The fresh material of plant source
20 ~ 30, ethyl acetate 15 ~ 20, ethanol 6 ~ 12, fishbone powder 20 ~ 30, shitosan 4 ~ 8, salicylic acid 2 ~ 5, Maifanitum 70 ~ 120, ferrum
Breeze 20 ~ 35, agricultural rare-earth 40 ~ 55, soybean meal 30 ~ 45, potato peel 15 ~ 25, EM bacteria agent 2 ~ 3, sheep stool ball 10 ~ 18, zinc powder 1 ~
3rd, plant ash 5 ~ 10 and appropriate water；
The fresh material of described plant source is with weight（Part）Following raw material for unit is mixed：Eucalyptus leaveses 10 ~ 15, Fructus Rubi 7 ~
10th, lucerne place 15 ~ 20, Folium Populi Davidianae 4 ~ 8, cercis leaf 1 ~ 4, wheat leaf 6 ~ 10, Folium Crataegi 2 ~ 5, leaf of Semen Maydis 3 ~ 7.
A kind of preparation method of insect pest organic mineral element foliage fertilizer, it is characterised in that including following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Medical stone powder is broken into into powder, mixing agricultural rare-earth, Iron Ore Powder are put into pyrolysis oven, 800 ~ 1000 DEG C under airtight condition
60 ~ 100min of heat treatment, natural cooling are standby；
（3）The mixing soya beans dregs of rice, potato peel and other following residual componentss being not directed to, add to（2）In described mixed dust formulation,
Moisturizing 50 ~ 60%, is inoculated with EM bacteria agent heap fermentation 20 ~ 30 days after high-temp steam sterilizing, after the completion of press solid-liquid ratio 1:100 ~ 150 points
Fermentation material is cleaned multiple times, it is standby after filtrate clarification；
（4）Will（1）Add after gained lixiviating solution mixing shitosan, salicylic acid（3）Clear liquor in, mix.
Compositing characteristic and its pest-resistant principle of the invention according to waxiness in background technology, the basic point of departure of preparation are to utilize
Plant waxiness extract is raw material, prepares the additive of foliage fertilizer, crop is protected using natural insect resistace active component,
This measure can reduce the pesticide residues of crop, improve crop quality, can improve substantially extraction step through years of researches
Suddenly：（1）It is to choose containing abundant waxiness and the plant leaf blade with insect pest characteristic, eucalyptus leaveses have to diamond-back moth significantly walks quickly and keeps away
Effect, the surface waxiness of Herba Medicaginiss then has good protective effect to variegation aphid, in the surface waxiness of Fructus Rubi containing Squalene,
The good insect repelling components such as plant sterol, tocopherol and vanillin, the also Cortex Populi dividianae with the effect of above effect same
Leaf, cercis, Folium Crataegi, wheat leaf, leaf of Semen Maydis etc.；（2）Using certain density ethyl acetate aqueous solution as extractant, then
Defibrination is carried out to the blade rich in waxiness, is mixed after ethyl acetate extractant is added, 60 DEG C of extractions of water-bath, this process is not only
Blade face top layer wax component can be extracted, while the volatility lipid in blade can be extracted, is equally had and is walked quickly and kept away evil well
The effect of worm, after the completion of high speed centrifugation remove blade residue, by gained filtrate by Rotary Evaporators heating concentration.
By in the plant leaf blade lixiviating solution that above method is obtained containing the volatile aromatic fat and surface lipophilic in blade
Property compound wax component, and all there are obvious boiling characteristics, after being sprayed to blade, insect had and walks quickly and keeps away work well
With, by the use of being slightly soluble in the ethyl acetate of water as extractant, can with the problem of the neutralizing plant extract poorly water-soluble of a part,
Remaining ethyl acetate after the completion of extraction, its characteristic for being slightly soluble in water serve the work of bridge well as a kind of intermediate
With, add to the water miscible foliage fertilizer of water-wet side connection after foliage fertilizer, and the wax component that the connection of lipophilic end is extracted, and according to
Similar compatibility principle, waxiness and the waxiness perfect adaptation of blade surface, promote foliage fertilizer to adsorb in blade surface, improve foliage fertilizer
Utilization rate.
Beneficial effects of the present invention：Invention is finally a kind of pest-resistant type foliage fertilizer containing various organic mineral elements, right
Mineral nitrogen rocks carry out pyrolysis processing, and then mixed organic matter together ferments, and the process of fermentation is also the process of slow chelating, is made
Organic matter corruption is presented forward direction all the time and carries out, and degenerates the mineral element of the organic acid complexation for producing, is more prone to be produced absorption,
It is notable for the effect of fertilizer of this short stay of foliage fertilizer.
Specific embodiment
Embodiment 1：
A kind of insect pest organic mineral element foliage fertilizer, it is characterised in that by following weight portion（Kg）Raw material make：Plant source
Fresh material 26, ethyl acetate 18, ethanol 9, fishbone powder 25, shitosan 5, salicylic acid 3, Maifanitum 100, Iron Ore Powder 30, agricultural rare-earth
50th, soybean meal 40, potato peel 20, EM bacteria agent 2, sheep stool ball 15, zinc powder 1, plant ash 8 and appropriate water；
The fresh material of described plant source is with weight（Kg）Following raw material for unit is mixed：Eucalyptus leaveses 12, Fructus Rubi 8, lucerne
Place 18, Folium Populi Davidianae 6, cercis leaf 3, wheat leaf 7, Folium Crataegi 3, leaf of Semen Maydis 5.
A kind of preparation method of insect pest organic mineral element foliage fertilizer, it is characterised in that including following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Medical stone powder is broken into into powder, mixing agricultural rare-earth, Iron Ore Powder are put into pyrolysis oven, 800 ~ 1000 DEG C under airtight condition
60 ~ 100min of heat treatment, natural cooling are standby；
（3）The mixing soya beans dregs of rice, potato peel and other following residual componentss being not directed to, add to（2）In described mixed dust formulation,
Moisturizing 50 ~ 60%, is inoculated with EM bacteria agent heap fermentation 20 ~ 30 days after high-temp steam sterilizing, after the completion of press solid-liquid ratio 1:100 ~ 150 points
Fermentation material is cleaned multiple times, it is standby after filtrate clarification；
（4）Will（1）Add after gained lixiviating solution mixing shitosan, salicylic acid（3）Clear liquor in, mix.
By the present invention foliage fertilizer be used for Fructus Lycopersici esculenti planting experiment, by invention foliage fertilizer by per mu of 150 ~ 200Kg amount
Uniformly it is sprayed on the blade of Fructus Lycopersici esculenti, as a result relative to conventional common foliage fertilizer, the assimilation effect of foliage fertilizer of the present invention is more preferable,
More preferably, the incidence rate of pest and disease damage is low the resistance of Fructus Lycopersici esculenti, and few pesticide is sprayed, and the several aspect features of quality of fruit are
Lifted.
Claims (2)
1. a kind of insect pest organic mineral element foliage fertilizer, it is characterised in that be made up of the raw material of following weight portion：Plant source is fresh
Material 20 ~ 30, ethyl acetate 15 ~ 20, ethanol 6 ~ 12, fishbone powder 20 ~ 30, shitosan 4 ~ 8, salicylic acid 2 ~ 5, Maifanitum 70 ~ 120,
Iron Ore Powder 20 ~ 35, agricultural rare-earth 40 ~ 55, soybean meal 30 ~ 45, potato peel 15 ~ 25, EM bacteria agent 2 ~ 3, sheep stool ball 10 ~ 18, zinc powder 1
~ 3, plant ash 5 ~ 10 and appropriate water；
The fresh material of described plant source is with weight（Part）Following raw material for unit is mixed：Eucalyptus leaveses 10 ~ 15, Fructus Rubi 7 ~
10th, lucerne place 15 ~ 20, Folium Populi Davidianae 4 ~ 8, cercis leaf 1 ~ 4, wheat leaf 6 ~ 10, Folium Crataegi 2 ~ 5, leaf of Semen Maydis 3 ~ 7.
2. a kind of preparation method of insect pest organic mineral element foliage fertilizer according to claim 1, it is characterised in that include
Following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Medical stone powder is broken into into powder, mixing agricultural rare-earth, Iron Ore Powder are put into pyrolysis oven, 800 ~ 1000 DEG C under airtight condition
60 ~ 100min of heat treatment, natural cooling are standby；
（3）The mixing soya beans dregs of rice, potato peel and other following residual componentss being not directed to, add to（2）In described mixed dust formulation,
Moisturizing 50 ~ 60%, is inoculated with EM bacteria agent heap fermentation 20 ~ 30 days after high-temp steam sterilizing, after the completion of press solid-liquid ratio 1:100 ~ 150 points
Fermentation material is cleaned multiple times, it is standby after filtrate clarification；
（4）Will（1）Add after gained lixiviating solution mixing shitosan, salicylic acid（3）Clear liquor in, mix.
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| CN201610987532.8A CN106565348A (en) | 2016-11-10 | 2016-11-10 | Pest-resistant organic mineral element foliar fertilizer and preparation method thereof |
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| CN201610987532.8A CN106565348A (en) | 2016-11-10 | 2016-11-10 | Pest-resistant organic mineral element foliar fertilizer and preparation method thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107162810A (en) * | 2017-07-18 | 2017-09-15 | 合肥百绿盛农业科技有限公司 | A kind of pakchoi plantation foliar fertilizer and preparation method |
| CN107188746A (en) * | 2017-07-31 | 2017-09-22 | 合肥信文农业科技有限公司 | A kind of blade face persistence high efficiency liquid fertilizer and preparation method thereof |
| CN107188747A (en) * | 2017-07-31 | 2017-09-22 | 合肥信文农业科技有限公司 | A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof |
| CN107226755A (en) * | 2017-07-31 | 2017-10-03 | 合肥信文农业科技有限公司 | A kind of long-acting foliar fertilizer of organic complex microelement type and preparation method thereof |
| CN107244983A (en) * | 2017-07-31 | 2017-10-13 | 合肥信文农业科技有限公司 | A kind of long-acting foliar fertilizer of soil retting extract solution and preparation method thereof |
| CN107266208A (en) * | 2017-07-31 | 2017-10-20 | 合肥信文农业科技有限公司 | A kind of continuation yeast fermentation extract solution foliar fertilizer and preparation method thereof |
| CN107337530A (en) * | 2017-07-31 | 2017-11-10 | 合肥信文农业科技有限公司 | A kind of long-term effect foliar fertilizer of chelant inorganic mineral element and preparation method thereof |
| CN107382478A (en) * | 2017-07-31 | 2017-11-24 | 合肥信文农业科技有限公司 | A kind of extract solution foliar fertilizer of liquid state fermentation chelant and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105967897A (en) * | 2016-06-22 | 2016-09-28 | 望江乐和生态农业有限公司 | Effect promoting agent for improving foliar fertilizer effect and preparation method of effect promoting agent |
| CN105985194A (en) * | 2016-07-01 | 2016-10-05 | 安徽万利生态园林景观有限公司 | Ginkgo foliage spray fertilizer additive and preparation method thereof |
-
2016
- 2016-11-10 CN CN201610987532.8A patent/CN106565348A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105967897A (en) * | 2016-06-22 | 2016-09-28 | 望江乐和生态农业有限公司 | Effect promoting agent for improving foliar fertilizer effect and preparation method of effect promoting agent |
| CN105985194A (en) * | 2016-07-01 | 2016-10-05 | 安徽万利生态园林景观有限公司 | Ginkgo foliage spray fertilizer additive and preparation method thereof |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107162810A (en) * | 2017-07-18 | 2017-09-15 | 合肥百绿盛农业科技有限公司 | A kind of pakchoi plantation foliar fertilizer and preparation method |
| CN107188746A (en) * | 2017-07-31 | 2017-09-22 | 合肥信文农业科技有限公司 | A kind of blade face persistence high efficiency liquid fertilizer and preparation method thereof |
| CN107188747A (en) * | 2017-07-31 | 2017-09-22 | 合肥信文农业科技有限公司 | A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof |
| CN107226755A (en) * | 2017-07-31 | 2017-10-03 | 合肥信文农业科技有限公司 | A kind of long-acting foliar fertilizer of organic complex microelement type and preparation method thereof |
| CN107244983A (en) * | 2017-07-31 | 2017-10-13 | 合肥信文农业科技有限公司 | A kind of long-acting foliar fertilizer of soil retting extract solution and preparation method thereof |
| CN107266208A (en) * | 2017-07-31 | 2017-10-20 | 合肥信文农业科技有限公司 | A kind of continuation yeast fermentation extract solution foliar fertilizer and preparation method thereof |
| CN107337530A (en) * | 2017-07-31 | 2017-11-10 | 合肥信文农业科技有限公司 | A kind of long-term effect foliar fertilizer of chelant inorganic mineral element and preparation method thereof |
| CN107382478A (en) * | 2017-07-31 | 2017-11-24 | 合肥信文农业科技有限公司 | A kind of extract solution foliar fertilizer of liquid state fermentation chelant and preparation method thereof |
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Application publication date: 20170419 |