CN107188747A - A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof - Google Patents

A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof Download PDF

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Publication number
CN107188747A
CN107188747A CN201710636636.9A CN201710636636A CN107188747A CN 107188747 A CN107188747 A CN 107188747A CN 201710636636 A CN201710636636 A CN 201710636636A CN 107188747 A CN107188747 A CN 107188747A
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China
Prior art keywords
plant
foliar fertilizer
raw material
rice husk
life
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CN201710636636.9A
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Chinese (zh)
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不公告发明人
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Hefei Xinwen Agricultural Technology Co Ltd
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Hefei Xinwen Agricultural Technology Co Ltd
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Priority to CN201710636636.9A priority Critical patent/CN107188747A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers
    • C05G5/23Solutions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Organic Chemistry (AREA)
  • Plant Pathology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof, it is made up of the raw material of following parts by weight:The fresh raw material of plant, NaCl, ether, chitosan, brassin lactones, ascorbic acid, 2,4 D sodium salts, bamboo vinegar, vitamin powder, paclobutrazol medicament, the dry slag of Chinese medicine, sodium tetraborate, rice husk, vermiculite power and appropriate water.By the irritating hormone of plant and similar component come rapid stimulation plant, dying crop is quickly brought back to life on maximum possibility, the major ingredient of foliar fertilizer is used as using the water extract of unburnt rice husk and the dry slag of Chinese medicine, it wherein with the addition of various auxin, growth-stimulating factor and plant similar effects parahormone, in the way of foliage dressing, it is quick to improve effect, wherein the essential oil chitosan film added can improve the efficiency of foliar fertilizer.

Description

A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof
Technical field
The invention belongs to the technology field of foliar fertilizer, and in particular to a kind of foliar fertilizer for quickly bringing back to life dying plant And preparation method thereof.
Background technology
Chitosan is the product of chitin deacetylase, is a kind of Biodegradable material.Its molecular structure is by dividing at random The linear polysaccharide that the D- Glucosamines and 2-acetylamino-2-deoxy-D-glucose of cloth are connected into by β-(Isosorbide-5-Nitrae) glycosidic bond. Chitosan is water insoluble, most organic acid formation thick liquids can be dissolved in, with good film forming.
Lemon grass (Cymbopogon citratus) is grass family Cymbopogon, and herbaceos perennial, lemon grass (Cymbopogon citratus) has large area in Yunnan Province Dehong prefecture area Plantation, it has strong citrus scented, and cauline leaf can be used directly as flavoring, can also extract plants essential oil.Lemon Careless essential oil is rich in a variety of special compositions such as citral, limonenes, to staphylococcus aureus, bacillus subtilis and Escherichia coli Deng with good bacteriostatic activity.Essential oil is usually the armaticity oily from acquisitions such as the bud of plant, seed, fruit or rhizomes Material, recent studies suggest that, most plants essential oil all has certain antibacterial activity.
Foliar fertilizer belongs to a kind of liquid fertilizer, by the elements such as N, P, K, iron, calcium, magnesium, zinc, iron, copper are circulated from Sub- form, first adheres on the surface of leaf, then passes through Premeabilisation of cells, the active absorption either mode such as respiration of blade Into in blade, its action character is:Rapid-action, utilization rate of fertilizer is high, effect is obvious etc.;But, with respect to solid fertilizer root The mode applied, the very big weak point of foliage dressing is exactly that fertilizer is extremely difficult to one on the plant crop blade face for being covered with wax Individual prolonged stop, it is meant that foliar fertilizer can not be fully absorbed, although modern science and technology is by adding the modes such as surfactant Repulsion hydrophobic effect of the blade face wax for foliar fertilizer is reduced, but under hot weather state, even if foliar fertilizer is longer Between be attached on blade, evaporation can also be quickly make liquid fertilizer desiccation, foliar fertilizer is lost the meaning of foliage dressing, this The characteristics of invention with chitosan by plants essential oil by combining film forming, is applied to the surface of foliar fertilizer, slows down evaporation, The attachment of longer time is reached, is conducive to the progress absorbed.
The content of the invention
Foliar fertilizer is longer in blade face residence time in order to improve by the present invention, and preventing the effect of rapid evaporation, there is provided blade face Action effect of the fertilizer under liquid condition is there is provided a kind of foliar fertilizer of surface fertilizer surface overlay film and preparation method thereof, specifically Realized by following technological means:
A kind of foliar fertilizer for quickly bringing back to life dying plant, is made up of the raw material of following parts by weight:The fresh raw material 50 ~ 80 of plant, NaCl 2 ~ 6, ether 10 ~ 25, chitosan 2 ~ 8, brassin lactones 0.5 ~ 1.0, ascorbic acid, 2,4 D sodium salt 0.01 ~ 0.02, bamboo vinegar 0.2 ~ 0.6, the dry slag 30 ~ 45 of vitamin powder 1 ~ 4, paclobutrazol medicament 2 ~ 5, Chinese medicine, sodium tetraborate 1 ~ 3, rice husk 40 ~ 60, vermiculite power 5 ~ 10 and appropriate water;
The fresh raw material of plant is made up of the raw material of following parts by weight:Wormwood 10 ~ 15, lemon grass (Cymbopogon citratus) 10 ~ 18, pomelo peel 25 ~ 45, kind Eggplant leaf 2 ~ 8, chinaberry leaf 7 ~ 15, garlic stem 5 ~ 10, santal leaf 2 ~ 6.
A kind of preparation method for the foliar fertilizer for quickly bringing back to life dying plant, including following steps,
(1)60 ~ 80 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, the micro mist of ground 80 ~ 120 mesh sieve is molten by NaCl The aqueous solution of 1 ~ 2wt% of configuration concentration concentration in enough water, by solid-liquid ratio 3:10 ~ 15 ratios by the micro mist add to In the NaCl aqueous solution, 6 ~ 10h of immersion carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 30 ~ 50%, after stirring stand 10 ~ 20min, then carries out extraction process by 60 ~ 90min of vacuum distillation, is reused while flowing back and reclaiming ether, molten to residue Liquid carries out suction filtration and obtains the extract solution containing extraction of essential oil thing;
(3)Vermiculite power was screened into 60 ~ 100 mesh sieves, it is underproof to repeat to grind, then mixed with rice husk and the dry slag of Chinese medicine, so After be packed together, after lighting control closed environment under oxygen supply, rice husk is slowly simmered burnings, finally by not exclusively then Rice husk mixed with 20 ~ 30 times of water immersion 50 ~ 80min, after the completion of centrifuging and taking supernatant.
(4)Will(2)The extract solution mixing bamboo vinegar, vitamin powder, paclobutrazol and it is other it is following be not directed to it is remaining into Point, add extremely(3)Supernatant in, stir and evenly mix, be then diluted with water 5 ~ 10 times, finally using preceding making according to foliar fertilizer Consumption is sprayed to plant leaf surface after adding the chitosan of its total amount 1.5 ~ 4.5%, dissolving.
Invention adds chitosan solution, is prepared for the crosslinking antiseepage of chitosan/essential oil using the essential oil in plant as extract Film layer, in foliar fertilizer, effect can be crosslinked on the surface of foliar fertilizer, forms very thin vaporization prevention layer, effectively improves leaf The time that leaven is rested on blade, while extraction of essential oil is from all parts of a plant, have plants essential oil extract also has The effect of antibacterial, worm-expelling, for foliar fertilizer can be to pest and disease damage preventing and treating and blade morbidity have which preventive effect.
Several fresh raw materials of plant for possessing and necessarily walking quickly and keeping away that insect and essential oil content enrich have been selected in invention:Wormwood, lemon grass (Cymbopogon citratus), Pomelo peel, tomato leaf, chinaberry leaf, garlic stem, santal leaf.
60 ~ 80 DEG C of low temperature was carried out to fresh plant raw material before this and dries to obtain siccative, then the micro mist of ground 80 ~ 120 mesh sieve, For the extraction of essential oil, the smaller progress for being more conducive to extracting of the particle degree of plant cell, this is can not by fresh material defibrination Reach, then configure the NaCl aqueous solution of 1 ~ 2wt% concentration, the fresh raw material of plant of milling was soaked before this, this process The osmotic pressure that can be destroyed inside and outside plant cell, causes cell to be swelled rupture, is easy to the extraction process of follow-up essential oil, soaks here Time is 6 ~ 10h, and solid-liquid ratio is 3:10 ~ 15, after the completion of toward addition 30 ~ 50% in solution ether solvent, ether can be very good Derived essential oil is dissolved, essential oil in cell with combining the fine of absorption, and simple water extraction is inefficient, a certain amount of by adding Ether can improve extraction efficiency, while shorten distillation used in time, then carried by 60 ~ 90min of vacuum distillation Process is taken, is reused while flowing back and reclaiming ether, what the solution after the completion of distillation also can be relative is concentrated, extract solution is mixed Thing carries out suction filtration, has obtained the required extraction of essential oil aqueous solution.
The essential oil content 1.5 ~ 3.0% that the method is obtained, but the goal of the invention of the present invention is sufficient for, reason is that shell gathers The film forming requirement of sugar and essential oil and need not too high essential oil concentration and chitosan concentration, essential oil swims in leaf due to hydrophobic effect The surface of leaven, so such concentration meets the requirements, and chitosan foliar fertilizer concentration requirement 1.5 ~ 4.5%, it is high The chitosan of concentration makes the air-tightness after film forming and vaporization prevention performance more preferably, it is contemplated that blade is also required to be breathed in itself Effect, so chitosan concentration is not that the higher the better.
Beneficial effects of the present invention:By the irritating hormone of plant and similar component come rapid stimulation plant, in maximum Dying crop is quickly brought back to life above the possibility of degree, using the water extract of unburnt rice husk and the dry slag of Chinese medicine as The major ingredient of foliar fertilizer, wherein various auxin, growth-stimulating factor and plant similar effects parahormone are with the addition of, with foliage dressing Mode, effect is quickly improved, wherein the essential oil-chitosan film added can improve the efficiency of foliar fertilizer.
Embodiment
Embodiment 1:
A kind of foliar fertilizer for quickly bringing back to life dying plant, by following weight(Kg)Raw material be made:The fresh raw material 65 of plant, NaCl 4th, ether 20, chitosan 5, brassin lactones 0.7, ascorbic acid, 2,4 D sodium salt 0.01, bamboo vinegar 0.2, vitamin powder 4, many Imitate azoles medicament 3, the dry slag 40 of Chinese medicine, sodium tetraborate 2, rice husk 55, vermiculite power 6 and appropriate water;
The fresh raw material of plant is by following weight(Kg)Raw material be made:Wormwood 14, lemon grass (Cymbopogon citratus) 15, pomelo peel 35, tomato leaf 7, Chinaberry leaf 12, garlic stem 8, santal leaf 5.
A kind of preparation method for the foliar fertilizer for quickly bringing back to life dying plant, including following steps,
(1)75 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, NaCl is dissolved in enough by the micro mist of ground 90 mesh sieve The aqueous solution of configuration concentration 1.5wt% concentration in water, by solid-liquid ratio 3:12 ratios add the micro mist into the NaCl aqueous solution, Immersion 8h carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 35%, 15min is stood after stirring, so Extraction process is carried out by vacuum distillation 75min afterwards, reused while flowing back and reclaiming ether, carrying out suction filtration to surplus solution obtains Extract solution containing extraction of essential oil thing;
(3)Vermiculite power was screened into 80 mesh sieves, it is underproof to repeat to grind, then mixed with rice husk and the dry slag of Chinese medicine, Ran Houdui Product controls the oxygen supply under closed environment together, after lighting, and rice husk is slowly simmered burning, finally by rice husk not exclusively then Mixed with 25 times of water immersion 65min, after the completion of centrifuging and taking supernatant.
(4)Will(2)The extract solution mixing bamboo vinegar, vitamin powder, paclobutrazol and it is other it is following be not directed to it is remaining into Point, add extremely(3)Supernatant in, stir and evenly mix, be then diluted with water 8 times, finally using the preceding use according to foliar fertilizer Amount adds the chitosan of its total amount 2.5%, and plant leaf surface is sprayed to after dissolving.
Practical application effect is studied, and the foliar fertilizer of the present invention is applied to the plantation foliar fertilizer of tomato, as experimental group, Set control group as reference simultaneously, the foliar fertilizer of control group is not added with plant extract essential oil and chitosan, other formulas and system Preparation Method is identical with experimental group, the management method all same in later stage.Specific effect such as following table:(Indices are full marks)
The fresh and tender degree plant growing way prevention and control of plant diseases, pest control situation dry-matter accumulation of the detailed blade of packet
Experimental group 9879
Control group 776 7.5

Claims (2)

1. a kind of foliar fertilizer for quickly bringing back to life dying plant, it is characterised in that:It is made up of the raw material of following parts by weight:The fresh original of plant Material 50 ~ 80, NaCl 2 ~ 6, ether 10 ~ 25, chitosan 2 ~ 8, brassin lactones 0.5 ~ 1.0, ascorbic acid, 2,4 D sodium salt 0.01 ~ 0.02, the dry slag 30 ~ 45 of bamboo vinegar 0.2 ~ 0.6, vitamin powder 1 ~ 4, paclobutrazol medicament 2 ~ 5, Chinese medicine, sodium tetraborate 1 ~ 3, rice husk 40 ~ 60, vermiculite power 5 ~ 10 and appropriate water;
The fresh raw material of plant is made up of the raw material of following parts by weight:Wormwood 10 ~ 15, lemon grass (Cymbopogon citratus) 10 ~ 18, pomelo peel 25 ~ 45, kind Eggplant leaf 2 ~ 8, chinaberry leaf 7 ~ 15, garlic stem 5 ~ 10, santal leaf 2 ~ 6.
2. a kind of preparation method for the foliar fertilizer for quickly bringing back to life dying plant according to claim 1, it is characterised in that:Including Following steps,
(1)60 ~ 80 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, the micro mist of ground 80 ~ 120 mesh sieve is molten by NaCl The aqueous solution of 1 ~ 2wt% of configuration concentration concentration in enough water, by solid-liquid ratio 3:10 ~ 15 ratios by the micro mist add to In the NaCl aqueous solution, 6 ~ 10h of immersion carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 30 ~ 50%, after stirring stand 10 ~ 20min, then carries out extraction process by 60 ~ 90min of vacuum distillation, is reused while flowing back and reclaiming ether, molten to residue Liquid carries out suction filtration and obtains the extract solution containing extraction of essential oil thing;
(3)Vermiculite power was screened into 60 ~ 100 mesh sieves, it is underproof to repeat to grind, then mixed with rice husk and the dry slag of Chinese medicine, so After be packed together, after lighting control closed environment under oxygen supply, rice husk is slowly simmered burnings, finally by not exclusively then Rice husk mixed with 20 ~ 30 times of water immersion 50 ~ 80min, after the completion of centrifuging and taking supernatant;
(4)Will(2)The extract solution mixing bamboo vinegar, vitamin powder, paclobutrazol and other following residual components being not directed to, plus Enter to(3)Supernatant in, stir and evenly mix, be then diluted with water 5 ~ 10 times, finally using the preceding usage amount according to foliar fertilizer Plant leaf surface is sprayed to after adding the chitosan of its total amount 1.5 ~ 4.5%, dissolving.
CN201710636636.9A 2017-07-31 2017-07-31 A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof Withdrawn CN107188747A (en)

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Application Number Priority Date Filing Date Title
CN201710636636.9A CN107188747A (en) 2017-07-31 2017-07-31 A kind of foliar fertilizer for quickly bringing back to life dying plant and preparation method thereof

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102040408A (en) * 2010-06-25 2011-05-04 厦门三和利生物技术有限公司 Foliar fertilizer
CN106565348A (en) * 2016-11-10 2017-04-19 凤台县牧碧农业发展有限公司 Pest-resistant organic mineral element foliar fertilizer and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102040408A (en) * 2010-06-25 2011-05-04 厦门三和利生物技术有限公司 Foliar fertilizer
CN106565348A (en) * 2016-11-10 2017-04-19 凤台县牧碧农业发展有限公司 Pest-resistant organic mineral element foliar fertilizer and preparation method thereof

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Application publication date: 20170922