CN107244983A - A kind of long-acting foliar fertilizer of soil retting extract solution and preparation method thereof - Google Patents
A kind of long-acting foliar fertilizer of soil retting extract solution and preparation method thereof Download PDFInfo
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- CN107244983A CN107244983A CN201710636625.0A CN201710636625A CN107244983A CN 107244983 A CN107244983 A CN 107244983A CN 201710636625 A CN201710636625 A CN 201710636625A CN 107244983 A CN107244983 A CN 107244983A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Plant Pathology (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a kind of long-acting foliar fertilizer of soil retting extract solution and preparation method thereof, it is made up of the raw material of following parts by weight:The fresh raw material of plant, NaCl, ether, chitosan, leaf mould, cellulase, trichoderma, diethyl aminoethyl hexanoate, ammonium dihydrogen phosphate, zinc sulfate, powder of straw, cinnamomum camphora wood chip, lotus pool mud, selenium powder, frerrous chloride, rabbit excrement and appropriate water.In order to prevent the more difficult decomposition of cellulose, invention with the addition of cellulase, the raw material enriched with cellulose, which is directly contacted, also contains the more undecomposed cellulose utilized in mixing, rabbit excrement, the mode that mud is wrapped up then is applied into outer layer, the ambient influnence that so enzyme is subject to will be substantially reduced, the material that becomes thoroughly decomposed after becoming thoroughly decomposed, for spraying for blade face, reduces the use of inorganic fertilizer by extracting to obtain extract solution, and absorption efficiency is high, the material that becomes thoroughly decomposed of one time fermentation can carry out extracted many times.
Description
Technical field
The invention belongs to the technology field of foliar fertilizer, and in particular to a kind of long-acting foliar fertilizer of soil retting extract solution
And preparation method thereof.
Background technology
Chitosan is the product of chitin deacetylase, is a kind of Biodegradable material.Its molecular structure is by dividing at random
The linear polysaccharide that the D- Glucosamines and 2-acetylamino-2-deoxy-D-glucose of cloth are connected into by β-(Isosorbide-5-Nitrae) glycosidic bond.
Chitosan is water insoluble, most organic acid formation thick liquids can be dissolved in, with good film forming.
Lemon grass (Cymbopogon citratus) is grass family Cymbopogon, and herbaceos perennial, lemon grass (Cymbopogon citratus) has large area in Yunnan Province Dehong prefecture area
Plantation, it has strong citrus scented, and cauline leaf can be used directly as flavoring, can also extract plants essential oil.Lemon
Careless essential oil is rich in a variety of special compositions such as citral, limonenes, to staphylococcus aureus, bacillus subtilis and Escherichia coli
Deng with good bacteriostatic activity.Essential oil is usually the armaticity oily from acquisitions such as the bud of plant, seed, fruit or rhizomes
Material, recent studies suggest that, most plants essential oil all has certain antibacterial activity.
Foliar fertilizer belongs to a kind of liquid fertilizer, by the elements such as N, P, K, iron, calcium, magnesium, zinc, iron, copper are circulated from
Sub- form, first adheres on the surface of leaf, then passes through Premeabilisation of cells, the active absorption either mode such as respiration of blade
Into in blade, its action character is:Rapid-action, utilization rate of fertilizer is high, effect is obvious etc.;But, with respect to solid fertilizer root
The mode applied, the very big weak point of foliage dressing is exactly that fertilizer is extremely difficult to one on the plant crop blade face for being covered with wax
Individual prolonged stop, it is meant that foliar fertilizer can not be fully absorbed, although modern science and technology is by adding the modes such as surfactant
Repulsion hydrophobic effect of the blade face wax for foliar fertilizer is reduced, but under hot weather state, even if foliar fertilizer is longer
Between be attached on blade, evaporation can also be quickly make liquid fertilizer desiccation, foliar fertilizer is lost the meaning of foliage dressing, this
The characteristics of invention with chitosan by plants essential oil by combining film forming, is applied to the surface of foliar fertilizer, slows down evaporation,
The attachment of longer time is reached, is conducive to the progress absorbed.
The content of the invention
Foliar fertilizer is longer in blade face residence time in order to improve by the present invention, and preventing the effect of rapid evaporation, there is provided blade face
Action effect of the fertilizer under liquid condition is there is provided a kind of foliar fertilizer of surface fertilizer surface overlay film and preparation method thereof, specifically
Realized by following technological means:
A kind of long-acting foliar fertilizer of soil retting extract solution, is made up of the raw material of following parts by weight:The fresh raw material 50 ~ 80 of plant, NaCl
2 ~ 6, ether 10 ~ 25, chitosan 2 ~ 8, leaf mould 10 ~ 20, cellulase 1 ~ 3, trichoderma 0.5 ~ 1.0, diethyl aminoethyl hexanoate 0.05 ~
0.10th, ammonium dihydrogen phosphate 4 ~ 8, zinc sulfate 1 ~ 4, powder of straw 20 ~ 35, cinnamomum camphora wood chip 25 ~ 40, lotus pool mud 8 ~ 15, selenium powder 0.5 ~
1.5th, frerrous chloride 3 ~ 7, rabbit excrement 5 ~ 10 and appropriate water;
The fresh raw material of plant is made up of the raw material of following parts by weight:Wormwood 10 ~ 15, lemon grass (Cymbopogon citratus) 10 ~ 18, pomelo peel 25 ~ 45, kind
Eggplant leaf 2 ~ 8, chinaberry leaf 7 ~ 15, garlic stem 5 ~ 10, santal leaf 2 ~ 6.
A kind of preparation method of the long-acting foliar fertilizer of soil retting extract solution, including following steps,
(1)60 ~ 80 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, the micro mist of ground 80 ~ 120 mesh sieve is molten by NaCl
The aqueous solution of 1 ~ 2wt% of configuration concentration concentration in enough water, by solid-liquid ratio 3:10 ~ 15 ratios by the micro mist add to
In the NaCl aqueous solution, 6 ~ 10h of immersion carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 30 ~ 50%, after stirring stand 10 ~
20min, then carries out extraction process by 60 ~ 90min of vacuum distillation, is reused while flowing back and reclaiming ether, molten to residue
Liquid carries out suction filtration and obtains the extract solution containing extraction of essential oil thing;
(3)Mixed straw powder, cinnamomum camphora wood chip and rabbit excrement, pulverize after crushing, spray the cellulase and trichoderma of dilution,
Appropriate water is kept to turn into scoriform, mixed leaf soil, lotus pool mud, zinc sulfate and other following residual components being not directed to are fitted
Amount turns into lotion after adding water, and is wrapped on foregoing slag charge, landfill of then digging pit, retting 30 ~ 50 days, digs out material drying of becoming thoroughly decomposed and dissipates
Taste.
(4)Will(3)Gained, which becomes thoroughly decomposed, expects to mix with 10 ~ 20 times of water, and standing sedimentation after stirring takes supernatant to add diethyl aminoethyl hexanoate
And(2)The extract solution of gained, is stirred and evenly mixed, and is finally adding its total amount 1.5 ~ 4.5% using the preceding usage amount according to foliar fertilizer
Plant leaf surface is sprayed to after chitosan, dissolving.
Invention adds chitosan solution, is prepared for the crosslinking antiseepage of chitosan/essential oil using the essential oil in plant as extract
Film layer, in foliar fertilizer, effect can be crosslinked on the surface of foliar fertilizer, forms very thin vaporization prevention layer, effectively improves leaf
The time that leaven is rested on blade, while extraction of essential oil is from all parts of a plant, have plants essential oil extract also has
The effect of antibacterial, worm-expelling, for foliar fertilizer can be to pest and disease damage preventing and treating and blade morbidity have which preventive effect.
Several fresh raw materials of plant for possessing and necessarily walking quickly and keeping away that insect and essential oil content enrich have been selected in invention:Wormwood, lemon grass (Cymbopogon citratus),
Pomelo peel, tomato leaf, chinaberry leaf, garlic stem, santal leaf.
60 ~ 80 DEG C of low temperature was carried out to fresh plant raw material before this and dries to obtain siccative, then the micro mist of ground 80 ~ 120 mesh sieve,
For the extraction of essential oil, the smaller progress for being more conducive to extracting of the particle degree of plant cell, this is can not by fresh material defibrination
Reach, then configure the NaCl aqueous solution of 1 ~ 2wt% concentration, the fresh raw material of plant of milling was soaked before this, this process
The osmotic pressure that can be destroyed inside and outside plant cell, causes cell to be swelled rupture, is easy to the extraction process of follow-up essential oil, soaks here
Time is 6 ~ 10h, and solid-liquid ratio is 3:10 ~ 15, after the completion of toward addition 30 ~ 50% in solution ether solvent, ether can be very good
Derived essential oil is dissolved, essential oil in cell with combining the fine of absorption, and simple water extraction is inefficient, a certain amount of by adding
Ether can improve extraction efficiency, while shorten distillation used in time, then carried by 60 ~ 90min of vacuum distillation
Process is taken, is reused while flowing back and reclaiming ether, what the solution after the completion of distillation also can be relative is concentrated, extract solution is mixed
Thing carries out suction filtration, has obtained the required extraction of essential oil aqueous solution.
The essential oil content 1.5 ~ 3.0% that the method is obtained, but the goal of the invention of the present invention is sufficient for, reason is that shell gathers
The film forming requirement of sugar and essential oil and need not too high essential oil concentration and chitosan concentration, essential oil swims in leaf due to hydrophobic effect
The surface of leaven, so such concentration meets the requirements, and chitosan foliar fertilizer concentration requirement 1.5 ~ 4.5%, it is high
The chitosan of concentration makes the air-tightness after film forming and vaporization prevention performance more preferably, it is contemplated that blade is also required to be breathed in itself
Effect, so chitosan concentration is not that the higher the better.
Beneficial effects of the present invention:In order to prevent the more difficult decomposition of cellulose, invention with the addition of cellulase, rich with cellulose
Rich raw material, which is directly contacted, also contains the more undecomposed cellulose utilized, the mode for then wrapping up mud in mixing, rabbit excrement
Outer layer is applied to, the ambient influnence that such enzyme is subject to will be substantially reduced, the material that becomes thoroughly decomposed after becoming thoroughly decomposed is used for by extracting to obtain extract solution
Spraying for blade face, reduces the use of inorganic fertilizer, and absorption efficiency is high, and the material that becomes thoroughly decomposed of one time fermentation can repeatedly be soaked
Carry.
Embodiment
Embodiment 1:
A kind of long-acting foliar fertilizer of soil retting extract solution, by following weight(Kg)Raw material be made:The fresh raw material 60 of plant, NaCl
3rd, ether 18, chitosan 6, leaf mould 14, cellulase 1, trichoderma 0.6, diethyl aminoethyl hexanoate 0.06, ammonium dihydrogen phosphate 6, zinc sulfate
2nd, powder of straw 30, cinnamomum camphora wood chip 30, lotus pool mud 12, selenium powder 0.8, frerrous chloride 3, rabbit excrement 9 and appropriate water;
The fresh raw material of plant is by following weight(Kg)Raw material be made:Wormwood 14, lemon grass (Cymbopogon citratus) 16, pomelo peel 30, tomato leaf 7,
Chinaberry leaf 12, garlic stem 6, santal leaf 3.
A kind of preparation method of the long-acting foliar fertilizer of soil retting extract solution, including following steps,
(1)70 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, NaCl is dissolved in enough by the micro mist of ground 120 mesh sieve
Water in configuration concentration 2wt% concentration the aqueous solution, by solid-liquid ratio 3:14 ratios add the micro mist into the NaCl aqueous solution,
Immersion 7h carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 45%, 12min is stood after stirring, so
Extraction process is carried out by vacuum distillation 75min afterwards, reused while flowing back and reclaiming ether, carrying out suction filtration to surplus solution obtains
Extract solution containing extraction of essential oil thing;
(3)Mixed straw powder, cinnamomum camphora wood chip and rabbit excrement, pulverize after crushing, spray the cellulase and trichoderma of dilution,
Appropriate water is kept to turn into scoriform, mixed leaf soil, lotus pool mud, zinc sulfate and other following residual components being not directed to are fitted
Amount turns into lotion after adding water, and is wrapped on foregoing slag charge, landfill of then digging pit, retting 45 days, digs out the material that becomes thoroughly decomposed and dries scattered taste.
(4)Will(3)Gained become thoroughly decomposed material mixed with 14 times of water, standing sedimentation after stirring, take supernatant addition diethyl aminoethyl hexanoate and
(2)The extract solution of gained, is stirred and evenly mixed, and is finally gathered in the shell that its total amount 2.5% is added using the preceding usage amount according to foliar fertilizer
Plant leaf surface is sprayed to after sugar, dissolving.
Practical application effect is studied, and the foliar fertilizer of the present invention is applied to the plantation foliar fertilizer of apple tree, experiment is used as
Group, at the same set control group as reference, the foliar fertilizer of control group is not added with plant extract essential oil and chitosan, other formula and
Preparation method is identical with experimental group, the management method all same in later stage.Specific effect such as following table:(Indices are full marks)
The fresh and tender degree plant growing way prevention and control of plant diseases, pest control situation dry-matter accumulation of the detailed blade of packet
Experimental group 9879
Control group 776 7.5
Claims (2)
1. a kind of long-acting foliar fertilizer of soil retting extract solution, it is characterised in that:It is made up of the raw material of following parts by weight:The fresh original of plant
Material 50 ~ 80, NaCl 2 ~ 6, ether 10 ~ 25, chitosan 2 ~ 8, leaf mould 10 ~ 20, cellulase 1 ~ 3, trichoderma 0.5 ~ 1.0,
Diethyl aminoethyl hexanoate 0.05 ~ 0.10, ammonium dihydrogen phosphate 4 ~ 8, zinc sulfate 1 ~ 4, powder of straw 20 ~ 35, cinnamomum camphora wood chip 25 ~ 40, lotus pool mud 8 ~
15th, selenium powder 0.5 ~ 1.5, frerrous chloride 3 ~ 7, rabbit excrement 5 ~ 10 and appropriate water;
The fresh raw material of plant is made up of the raw material of following parts by weight:Wormwood 10 ~ 15, lemon grass (Cymbopogon citratus) 10 ~ 18, pomelo peel 25 ~ 45, kind
Eggplant leaf 2 ~ 8, chinaberry leaf 7 ~ 15, garlic stem 5 ~ 10, santal leaf 2 ~ 6.
2. a kind of preparation method of the long-acting foliar fertilizer of soil retting extract solution according to claim 1, it is characterised in that:Including
Following steps,
(1)60 ~ 80 DEG C of low temperature is carried out to fresh plant raw material and dries to obtain siccative, the micro mist of ground 80 ~ 120 mesh sieve is molten by NaCl
The aqueous solution of 1 ~ 2wt% of configuration concentration concentration in enough water, by solid-liquid ratio 3:10 ~ 15 ratios by the micro mist add to
In the NaCl aqueous solution, 6 ~ 10h of immersion carries out being swelled for cell;
(2)According to(1)The amount of described solution, adds the ether solvent of its parts by weight 30 ~ 50%, after stirring stand 10 ~
20min, then carries out extraction process by 60 ~ 90min of vacuum distillation, is reused while flowing back and reclaiming ether, molten to residue
Liquid carries out suction filtration and obtains the extract solution containing extraction of essential oil thing;
(3)Mixed straw powder, cinnamomum camphora wood chip and rabbit excrement, pulverize after crushing, spray the cellulase and trichoderma of dilution,
Appropriate water is kept to turn into scoriform, mixed leaf soil, lotus pool mud, zinc sulfate and other following residual components being not directed to are fitted
Amount turns into lotion after adding water, and is wrapped on foregoing slag charge, landfill of then digging pit, retting 30 ~ 50 days, digs out material drying of becoming thoroughly decomposed and dissipates
Taste;
(4)Will(3)Gained become thoroughly decomposed material mixed with 10 ~ 20 times of water, standing sedimentation after stirring, take supernatant addition diethyl aminoethyl hexanoate and
(2)The extract solution of gained, is stirred and evenly mixed, and the shell of its total amount 1.5 ~ 4.5% is finally being added using the preceding usage amount according to foliar fertilizer
Plant leaf surface is sprayed to after glycan, dissolving.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111406462A (en) * | 2020-04-26 | 2020-07-14 | 广州隆盛景观建设有限公司 | Method for improving soil by garden organic mulch |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106565348A (en) * | 2016-11-10 | 2017-04-19 | 凤台县牧碧农业发展有限公司 | Pest-resistant organic mineral element foliar fertilizer and preparation method thereof |
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2017
- 2017-07-31 CN CN201710636625.0A patent/CN107244983A/en not_active Withdrawn
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Publication number | Priority date | Publication date | Assignee | Title |
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CN106565348A (en) * | 2016-11-10 | 2017-04-19 | 凤台县牧碧农业发展有限公司 | Pest-resistant organic mineral element foliar fertilizer and preparation method thereof |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111406462A (en) * | 2020-04-26 | 2020-07-14 | 广州隆盛景观建设有限公司 | Method for improving soil by garden organic mulch |
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Application publication date: 20171013 |