CN106538626A - A kind of composite pesticide for peanut cultivation and preparation method thereof - Google Patents
A kind of composite pesticide for peanut cultivation and preparation method thereof Download PDFInfo
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- CN106538626A CN106538626A CN201610926418.4A CN201610926418A CN106538626A CN 106538626 A CN106538626 A CN 106538626A CN 201610926418 A CN201610926418 A CN 201610926418A CN 106538626 A CN106538626 A CN 106538626A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/36—Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F3/00—Fertilisers from human or animal excrements, e.g. manure
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
The invention provides a kind of composite pesticide for peanut cultivation, belongs to technical field of pesticide.A kind of composite pesticide for peanut cultivation, is prepared from by fowl and animal excrement, peanut residue, Pepper stalk, pine needle powder, lignocellulose, nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition, and the Chinese medicine composition is prepared from by the raw material of following weight portion：10 ~ 30 parts of Fructus Zanthoxyli Plansipini, 10 ~ 30 parts of wild spinach, 10 ~ 30 parts of Folium seu Semen Daphniphylli macropodi, 10 ~ 30 parts of horse knotweed, 5 ~ 20 parts of Pericarpium Zanthoxyli, 5 ~ 20 parts of Herba euphorbiae lunulatae, 5 ~ 20 parts of Folium catalpae ovatae, 5 ~ 15 parts of Radix Et Rhizoma Nardostachyos, 3 ~ 12 parts of Folium Viticis Negundo, 3 ~ 12 parts of the Radix Euphorbiae Pekinensis.The present invention is compounded through science, serves the effect of Synergistic, and gained composite pesticide fertility is strong, improves crop yield, and antibacterial insecticidal effect is notable.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of composite pesticide and its preparation side for peanut cultivation
Method.
Background technology
In recent years, Semen arachidis hypogaeae pest and disease damage presents early, multiple and repeating transmission trend, from seedling to ripe aphid, tetranychid, Radix Betae
Noctuid and the harm of the high instar larvae of bollworm low instar larvae, beet armyworm and bollworm, subterranean pest-insect and leaf diseases are gone up year by year
Rise, serious threat is caused to peanut production.Therefore, preventing and treating in time is the key that Semen arachidis hypogaeae obtains high yield.In traditional Semen arachidis hypogaeae pest and disease damage
In preventing and treating, get used to controlling again light anti-, see that worm controls worm, control worm not diseases prevention, Pesticide use amount is big, and effect is poor, to sprout term disease and in
The anopia such as later stage southern blight, often result in be short of seedling disconnected ridge and plumpness reduction etc., and this prophylactico-therapeutic measuress often lead to Semen arachidis hypogaeae
Pesticide residues severe overweight, content of beary metal is exceeded to wait food-safety problem.The defect of Prevention Technique cannot be kept pace with the times
Green health food paces.Accordingly, it would be desirable to be optimized to Semen arachidis hypogaeae pest control techniques.
Existing prophylactico-therapeutic measuress, the drawbacks of avoiding traditional heavy dressing pesticide, often for multi-pronged, to adhere to " put prevention first, it is comprehensive
The plant protection policy of preventing and treating ", mainly including physics, medicine and Biological control.Biological control mainly uses Peanut Pest and equally deposits
In the food chain characteristic of natural enemy, corresponding insect pest natural enemy is found, while focusing on the protection to Semen arachidis hypogaeae, but there is the new insect pest of introduction
Potential feasibility.For physical control, mostly optimize the scheme of lamp light trapping, set lamp source more, height adjustment to optimal, and in lamp
Sex attractant is positioned over lamp source nearby to strengthen the captivation to worm by lower setting water source or colloid net etc. in addition；Coordinate medicine again
Thing parasite killing, effect meeting vertical rod are shown in shadow, and preventing and treating of this kind of measure mainly for Peanut Pest is stronger using restricted gender.For Semen arachidis hypogaeae
Disease, mainly still based on medical treatment, while strictly forbid the medicine containing illegal drug or heavy metal to be sprayed, even if such as
This, the use of violated pesticide still remains existing despite repeated prohibition.For really generally realize Semen arachidis hypogaeae greenization, No-harmful apple orchard, plant source agriculture
The large-scale development of medicine is very urgent.
Botanical pesticide product is directed to vegetable material mostly, is generally rich in N, P, K etc. in a large number and trace element, because
And after applying on crop, show to promote " fertilizer efficiency " such as growth, improvement qualities.If in addition, carry out soil treatment, plant source agriculture
Medicine can also adjust soil microbial community composition, further show " fertilizer efficiency " function.Azadirachta Indica A. slag after extracting such as nimbin can
As a kind of excellent organic fertilizer, not only can improved soil, adjust soil beneficial microbe colony, while Azadirachta Indica A. slag degraded
Product also has toxic action to nematicide；The medicine fertilizer of Herba Sophorae alopecuroidiss and Cynanchum Komarovii residue mixture also has identity function.
The patent of Application No. 201510023269 discloses a kind of environment friendly agricultural of prevention Semen arachidis hypogaeae underground pests, by as follows
The raw material of weight portion is mixed：Biological potentiating agent 1-3 parts, Chinese medicine composition 2-5 parts, the biological potentiating agent by sesame seed meal with
Soybean meal compound through biofermentation be obtained, the Chinese medicine composition by Chinese medicine Herba Polygoni Avicularis, Semen Arecae, change perfume, Caulis seu folium premnae microphyllae (Herba Premnae Microphyllae), Herba Artemisiae annuae,
After Rhizoma Coptidis, Fructus Zanthoxyli, Rhizoma Atractylodis, Herba Cayatiae Japonicae, cat's eye are mixed in proportion, fine powder are processed into, then are mixed to prepare with sawdust.Try in Jing fields
Test, prevent and treat subterranean pest-insect effect is significant, medicine fertilizer dual-purpose, environmental protection.The patent of Application No. 201510305423 discloses one
Organic biological medical fertilizer is planted, the medicine fertilizer is mixed with biological pesticide slurry by organic fertilizer, adjustment biological pesticide slurry quality 5-7%, moisture
Content is 28-32%, then pelletize, packaging after obtain；After the medicine fertilizer is applied, providing directly to plant outside growth desired nutritional
Nutrient substance conversion can be promoted, improves soil aggregate, strengthen soil fertilizer water conservation with the potential nutrients in activating soil
Ability, strengthens soil nutrient and fertility, has to insect pests such as Pieris rapae and by diseases such as fungus-caused downy mildew higher
Preventive and therapeutic effect, while increasing both production and income, the effect of parasite killing may be up to 90 ~ 95%, can be effectively protected crops and not invaded by insect
Evil.In above-mentioned technology botanical pesticide have medicine, it is fertile dual-purpose the characteristics of or botanical pesticide and organic fertilizer are implemented in combination with into medicine
Fertilizer is dual-purpose, and let us sees that botanical pesticide has potential application advantage in medicine fertilizer is prepared.But botanical pesticide is opened
Send out using still slowly, limiting factor is a lot, not high including the activity of Activities of Some Plants source pesticide, dosage is big, knocks down power
Not strong, drug effect plays relatively slow, is unfavorable for the prevention and control of the epizootic disease insect pest of burst；The species of its active component, content receive itself
Genetic factor, external environmental condition such as soil, temperature, illumination, the impact of soil value, have the change such as region and seasonality；
And active component is also different in plant different piece content, is particularly some active component unstable etc. to light and heat.
The content of the invention
In view of this, the technical problem to be solved is to provide a kind of pesticide, by organic fertilizer and plant source agriculture
Medicine is combined, and both provides nutritional need for peanut growth, can efficiently prevent and treat Semen arachidis hypogaeae common disease and pest, environmental protection, effect again
Fruit is significantly.
To solve above-mentioned technical problem, the technical solution adopted in the present invention is：
A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：20 ~ 40 parts of fowl and animal excrement, flower
Raw 10 ~ 20 parts of bran, 10 ~ 20 parts of Pepper stalk, 5 ~ 15 parts of pine needle powder, 3 ~ 12 parts of lignocellulose, 1 ~ 10 part of nitrogen-phosphorus-potassium compound fertilizer,
1 ~ 10 part of Chinese medicine composition, the Chinese medicine composition is prepared from by the raw material of following weight portion：10 ~ 30 parts of Fructus Zanthoxyli Plansipini, wild spinach
10 ~ 30 parts of dish, 10 ~ 30 parts of Folium seu Semen Daphniphylli macropodi, 10 ~ 30 parts of horse knotweed, 5 ~ 20 parts of Pericarpium Zanthoxyli, 5 ~ 20 parts of Herba euphorbiae lunulatae, 5 ~ 20 parts of Folium catalpae ovatae, Radix Et Rhizoma Nardostachyos 5 ~
15 parts, 3 ~ 12 parts of Folium Viticis Negundo, 3 ~ 12 parts of the Radix Euphorbiae Pekinensis.
Preferably, the Chinese medicine composition is prepared from by the raw material of following weight portion：15 ~ 25 parts of Fructus Zanthoxyli Plansipini, wild spinach
15 ~ 25 parts, 15 ~ 25 parts of Folium seu Semen Daphniphylli macropodi, 15 ~ 25 parts of horse knotweed, 10 ~ 15 parts of Pericarpium Zanthoxyli, 10 ~ 15 parts of Herba euphorbiae lunulatae, 10 ~ 15 parts of Folium catalpae ovatae, Radix Et Rhizoma Nardostachyos 8
~ 12 parts, 6 ~ 8 parts of Folium Viticis Negundo, 6 ~ 8 parts of the Radix Euphorbiae Pekinensis.
Preferably, the Chinese medicine composition is prepared from by the raw material of following weight portion：20 parts of Fructus Zanthoxyli Plansipini, wild spinach 20
Part, 20 parts of Folium seu Semen Daphniphylli macropodi, 20 parts of horse knotweed, 12 parts of Pericarpium Zanthoxyli, 12 parts of Herba euphorbiae lunulatae, 12 parts of Folium catalpae ovatae, 10 parts of Radix Et Rhizoma Nardostachyos, 7 parts of Folium Viticis Negundo, the Radix Euphorbiae Pekinensis 7
Part.
Preferably, the composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Fowl and animal excrement
30 ~ 35 parts, 12 ~ 18 parts of peanut residue, 12 ~ 18 parts of Pepper stalk, 8 ~ 12 parts of pine needle powder, 6 ~ 8 parts of lignocellulose, N P and K be combined
Fertile 5 ~ 7 parts, 6 ~ 8 parts of Chinese medicine composition.
Preferably, the Chinese medicine composition is prepared by method acquisition, specifically includes following steps：
1）5 ~ 20 parts of 10 ~ 30 parts of Fructus Zanthoxyli Plansipini, 10 ~ 30 parts of wild spinach, 5 ~ 20 parts of Pericarpium Zanthoxyli and the Herba euphorbiae lunulatae of weight portion are weighed respectively, are mixed
Close, crush, obtain comminuting matter I；10 ~ 30 parts of the Folium seu Semen Daphniphylli macropodi of weight portion, 10 ~ 30 parts of horse knotweed, 5 ~ 20 parts of Folium catalpae ovatae, sweet is weighed respectively
3 ~ 12 parts of 5 ~ 15 parts of pine, 3 ~ 12 parts of Folium Viticis Negundo and the Radix Euphorbiae Pekinensis, mixing are crushed, and obtain comminuting matter II；
2）The comminuting matter I is added to into supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row frozen centrifugation, removes impurity, obtains extract I；
3）The water of 4 ~ 6 times of its weight is added in the comminuting matter II, is soaked 15 ~ 20 minutes, start supersonic generator, plus
Heat is kept for 45 ~ 60 minutes to 60 ~ 70 DEG C, and filtered while hot obtains filtrate I and medicinal residues；After I natural cooling of filtrate, by the filter
When liquid I is concentrated into 75 ~ 80 DEG C, relative density is 1.20 ~ 1.25 extractum；
4）The extract I and extractum are mixed, is dried, fully crushed, obtain final product.
Preferably, step 2）Described in the pressure that extracts be 30 ~ 40MPa, extraction temperature is 30 ~ 45 DEG C, CO2Fluid flow
For 40 ~ 55L/h, extraction time is 2 ~ 4h.
Preferably, step 2）Described in ethanol volume fraction be 90 ~ 95%, addition be 200 ~ 400ml.
Preferably, step 3）Described in extractum and the ethanol solution w/v 1g：10~20ml.
A kind of preparation method of the composite pesticide for peanut cultivation, comprises the following steps：
1）30 ~ 35 parts of the fowl and animal excrement of dry weight portion, 12 ~ 18 parts of peanut residue, 12 ~ 18 parts of Pepper stalk, pine are weighed respectively
6 ~ 8 parts of 8 ~ 12 parts of pin powder and lignocellulose, mixing add organic matter decomposing inoculant, and mix is uniform, is covered using plastic foil,
It is 20 ~ 30% to control humidity, and temperature is 40 ~ 50 DEG C, banks up 7 ~ 10 days, obtains the material that becomes thoroughly decomposed；
2）1 ~ 10 part of 1 ~ 10 part of the nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition of weight portion are weighed respectively, are mixed with the material that becomes thoroughly decomposed
Even, control humidity is less than 10%, obtains final product composite pesticide.
Compared with prior art, its advantage is as follows for the present invention：
1）Present invention applicant has deeply research to peanut cultivation, and is based on peanut growth environment and rule, there is provided one kind is used for
The composite pesticide of peanut cultivation, organic fertilizer and botanical pesticide are assembled and making carry out furtheing investigate, mixture and institute
The achievement for obtaining.Composite pesticide of the present invention can promote nutrient substance to convert as base manure, improve soil aggregate, as base
Fertilizer, it is possible to increase Semen arachidis hypogaeae emergence rate, and had good sustained release effect, activating soil, meets the nutritional need of the whole growth cycle of Semen arachidis hypogaeae；Carry
High Quality of Peanuts, increases peanut yield；The disease resistance ability of Semen arachidis hypogaeae is simultaneously improved, Semen arachidis hypogaeae common disease and pest is had good anti-
Effect is controlled, it is especially more excellent to the prevention effect of subterranean pest-insect.
2）The raw materials used environmental protection of Chinese medicine composition of the present invention, wide material sources.Wherein, Fructus Zanthoxyli Plansipini, is Rutaceae Pericarpium Zanthoxyli
The fruit of platymiscium Fructus Zanthoxyli Plansipini.Pungent, slight bitter, temperature.It is slightly poisonous.Warming middle-JIAO qi-regulating, expelling wind and removing dampness, promoting blood circulation and stopping pain.Wild spinach, is Polygonaceae
The herb of plant golden dock.Acid；It is bitter；It is cold in nature, removing heat from blood；Removing toxic substances；Parasite killing.Herb ethanol extraction have suppress Trichophyton mentagrophytes and
The effect of Microspore and megaspore bacteria growing.The antifungic action of its hexane and butanol dissolving part is higher.Folium seu Semen Daphniphylli macropodi, another name mountain Huang Shu,
Bean curd head, Chinese holly city, thrush pearl, Folium seu Semen Daphniphylli oldhami, are the leaf of Daphniphyllaceae plant Folium seu Semen Daphniphylli macropodi.It is bitter；It is cool, enter Liver Channel, heat-clearing and toxic substances removing.Horse
Knotweed, is called big knotweed, Mo Jicao, lady's thumb, is the herb of polygonaceae plant red shank, is used as medicine with leaf.It is pungent；It is bitter；It is warm in nature, enter lung, spleen, big
Intestinal Jing, diaphoresis dehumidifying；Help digestion；Parasite killing.Pericarpium Zanthoxyli, the fragrant green pepper of another name, big Pericarpium Zanthoxyli, Semen zanthoxyli, are the drying and ripening of rutaceae Pericarpium Zanthoxyli
Peel.It is pungent, temperature.Returns spleen, stomach, kidney channel.Warming middle-JIAO to relieve pain, killing parasites for relieving itching.Herba euphorbiae lunulatae, Euphorbiaceae euphorbia Herba euphorbiae lunulatae it is complete
Grass.Hardship, it is cool.It is poisonous.Inducing diuresis to remove edema, draws out pus by applying a plaster to the affected part antipruritic.Folium catalpae ovatae, is the leaf of Bignoniaceae plant Chinese catalpa.Bitter in the mouth；It is cold in nature.Enter the heart, lung meridian.
Heat-clearing and toxic substances removing；Killing parasites for relieving itching.Radix Et Rhizoma Nardostachyos, are the rhizome and root of Valerianaceae plant Nardostachys chinensis Batal..It is sweet, temperature.Enter spleen, stomach.Folium Viticis Negundo, be
The leaf of Verbenaceae Herba Viticis Cannabifoliae.Acrid in the mouth, it is bitter, it is mild-natured.Induce sweat removing dampness, eliminating phlegm and relieving asthma, removing toxic substances.The Radix Euphorbiae Pekinensis, is that euphorbia plant is big
The root of halberd.Toil, trembles with fear, poisonous.Enter lung, spleen, kidney channel.Removing fluid-retention by purgation；Dispersing swelling and dissipating binds.Used by of the invention, organic fertilizer source is wide
It is general, the pollution problem of fowl and animal excrement, agricultural wastes etc. is can solve the problem that, and makes simple, it is easy to accomplish.Peanut residue, is Semen arachidis hypogaeae
Accessory substance after core oil expression, uses after dry, crushing.Fowl and animal excrement refers to that chicken manure and pig manure compare 1 with weight：The mixing of 2 ~ 3 collocation
Thing.Pepper stalk, is the residue after pepper picking, uses after drying, crushing.Pine needle powder, is that pinaster children is tender or withered
Branch and needle, resulting mixture after drying, crushing.Lignocellulose is natural reproducible timber at chemistry
The organic wadding fibrous material that reason, Mechanical Method processing are obtained.Above-mentioned each raw material is compounded by science, and mutual tonification meets Semen arachidis hypogaeae
There is obvious prevention effect to the pest and disease damage that the whole growth cycle of Semen arachidis hypogaeae occurs while nutritional need, good absorbing effect is right
Non- target object does not have any harm.
Specific embodiment
For a better understanding of the present invention, present disclosure, but this are further fairly set out with reference to embodiment
Bright protection content is not limited solely to the following examples.In the following description, a large amount of concrete details are given so as to
More thorough understanding of the invention is provided.It will be apparent, however, to one skilled in the art that the present invention can be with
It is carried out without the need for one or more of these details.
Embodiment 1：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 35 parts, 15 parts of peanut residue, 15 parts of Pepper stalk, 10 parts of pine needle powder, 7 parts of lignocellulose, 6 parts of nitrogen-phosphorus-potassium compound fertilizer, Chinese medicine
7 parts of compositionss, the Chinese medicine composition is prepared from by the raw material of following weight portion：20 parts of Fructus Zanthoxyli Plansipini, 20 parts of wild spinach, friendship allow
20 parts of wood, 20 parts of horse knotweed, 12 parts of Pericarpium Zanthoxyli, 12 parts of Herba euphorbiae lunulatae, 12 parts of Folium catalpae ovatae, 10 parts of Radix Et Rhizoma Nardostachyos, 7 parts of Folium Viticis Negundo, 7 parts of the Radix Euphorbiae Pekinensis.
In the present invention, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 1 ~ 3：0.5~1.2：0.3~1.
In the present embodiment, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 2：0.8：0.5.
Chinese medicine composition described in the present embodiment is prepared by method acquisition, specifically includes following steps：
1）Fructus Zanthoxyli Plansipini, wild spinach, Pericarpium Zanthoxyli and the Herba euphorbiae lunulatae of above-mentioned weight portion are weighed respectively, is mixed, crushed, obtain comminuting matter I；
Folium seu Semen Daphniphylli macropodi, horse knotweed, Folium catalpae ovatae, Radix Et Rhizoma Nardostachyos, Folium Viticis Negundo and the Radix Euphorbiae Pekinensis of above-mentioned weight portion are weighed respectively, is mixed, crushed, obtain comminuting matter
Ⅱ；
2）The comminuting matter I is added to into supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row frozen centrifugation, removes impurity, obtains extract I；
3）The water of 5 times of its weight is added in the comminuting matter II, is soaked 18 minutes, started supersonic generator, be heated to
65 DEG C, kept for 55 minutes, filtered while hot obtains filtrate I and medicinal residues；After I natural cooling of filtrate, the filtrate I is concentrated into
When 75 DEG C, relative density is 1.23 extractum；
4）The extract I and extractum are mixed, is dried, fully crushed, obtain final product.
In the present embodiment, step 2）Described in the pressure that extracts be 35MPa, extraction temperature is 35 DEG C, CO2Fluid flow is
45L/h, extraction time are 3h.
In the present embodiment, step 2）Described in ethanol volume fraction be 95%, addition is 300ml.
In the present embodiment, step 3）Described in extractum and the ethanol solution w/v 1g：15ml.
In the present invention, step 4）The organic solvent can be selected using dichloromethane or chloroform, similarly hereinafter.
A kind of preparation method of the composite pesticide for peanut cultivation, comprises the following steps：
1）Weigh respectively 35 parts of the fowl and animal excrement of dry weight portion, 15 parts of peanut residue, 15 parts of Pepper stalk, 10 parts of pine needle powder and
7 parts of lignocellulose, mixing add organic matter decomposing inoculant, and mix is uniform, is covered using plastic foil, and it is 25% to control humidity,
Temperature is 45 DEG C, banks up 8 days, obtains the material that becomes thoroughly decomposed；
2）7 parts of 6 parts of the nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition of weight portion are weighed respectively, are mixed homogeneously with the material that becomes thoroughly decomposed, are controlled
Humidity processed is less than 10%, obtains final product composite pesticide.
The use of organic matter decomposing inoculant meets the requirement of industry standard NY609-00.
The present invention is used for the using method of the composite pesticide of peanut cultivation：The planting soil of Semen arachidis hypogaeae is directly applied to, can
As base manure, also may be selected to use in arbitrary periods such as the initial bloom stage of peanut growth phase, lower pin phase, fruiting periods.
Embodiment 2：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 30 parts, 12 parts of peanut residue, 12 parts of Pepper stalk, 8 parts of pine needle powder, 6 parts of lignocellulose, 5 parts of nitrogen-phosphorus-potassium compound fertilizer, Chinese medicine group
6 parts of compound, the Chinese medicine composition is prepared from by the raw material of following weight portion：15 parts of Fructus Zanthoxyli Plansipini, 15 parts of wild spinach, Folium seu Semen Daphniphylli macropodi
15 parts, 15 parts of horse knotweed, 10 parts of Pericarpium Zanthoxyli, 10 parts of Herba euphorbiae lunulatae, 10 parts of Folium catalpae ovatae, 8 parts of Radix Et Rhizoma Nardostachyos, 6 parts of Folium Viticis Negundo, 6 parts of the Radix Euphorbiae Pekinensis.The present embodiment
In, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 1：0.5：0.3.
Chinese medicine composition described in the present embodiment is prepared by method acquisition, specifically includes following steps：
1）Fructus Zanthoxyli Plansipini, wild spinach, Pericarpium Zanthoxyli and the Herba euphorbiae lunulatae of above-mentioned weight portion are weighed respectively, is mixed, crushed, obtain comminuting matter I；
Folium seu Semen Daphniphylli macropodi, horse knotweed, Folium catalpae ovatae, Radix Et Rhizoma Nardostachyos, Folium Viticis Negundo and the Radix Euphorbiae Pekinensis of above-mentioned weight portion are weighed respectively, is mixed, crushed, obtain comminuting matter
Ⅱ；
2）The comminuting matter I is added to into supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row frozen centrifugation, removes impurity, obtains extract I；
3）The water of 4 times of its weight is added in the comminuting matter II, is soaked 15 minutes, started supersonic generator, be heated to
60 DEG C, kept for 45 minutes, filtered while hot obtains filtrate I and medicinal residues；After I natural cooling of filtrate, the filtrate I is concentrated into
When 75 DEG C, relative density is 1.20 extractum；
4）The extract I and extractum are mixed, is dried, fully crushed, obtain final product.
In the present embodiment, step 2）Described in the pressure that extracts be 30MPa, extraction temperature is 45 DEG C, CO2Fluid flow is
40L/h, extraction time are 4h.
In the present embodiment, step 2）Described in ethanol volume fraction be 90%, addition is 400ml.
In the present embodiment, step 3）Described in extractum and the ethanol solution w/v 1g：10ml.
A kind of preparation method of the composite pesticide for peanut cultivation, comprises the following steps：
1）Weigh respectively 30 parts of the fowl and animal excrement of dry weight portion, 12 parts of peanut residue, 12 parts of Pepper stalk, 8 parts of pine needle powder and
6 parts of lignocellulose, mixing add organic matter decomposing inoculant, and mix is uniform, is covered using plastic foil, and it is 20% to control humidity,
Temperature is 40 DEG C, banks up 7 days, obtains the material that becomes thoroughly decomposed；
2）6 parts of 5 parts of the nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition of weight portion are weighed respectively, are mixed homogeneously with the material that becomes thoroughly decomposed, are controlled
Humidity processed is less than 10%, obtains final product composite pesticide.
The use of organic matter decomposing inoculant meets the requirement of industry standard NY609-00.
The using method of the composite pesticide for peanut cultivation is repeated no more with embodiment 1.
Embodiment 3：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 32 parts, 18 parts of peanut residue, 18 parts of Pepper stalk, 12 parts of pine needle powder, 8 parts of lignocellulose, 7 parts of nitrogen-phosphorus-potassium compound fertilizer, Chinese medicine
8 parts of compositionss, the Chinese medicine composition is prepared from by the raw material of following weight portion：25 parts of Fructus Zanthoxyli Plansipini, 25 parts of wild spinach, friendship allow
25 parts of wood, 25 parts of horse knotweed, 15 parts of Pericarpium Zanthoxyli, 15 parts of Herba euphorbiae lunulatae, 15 parts of Folium catalpae ovatae, 12 parts of Radix Et Rhizoma Nardostachyos, 8 parts of Folium Viticis Negundo, 8 parts of the Radix Euphorbiae Pekinensis.This reality
Apply in example, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 3：1.2：1.
Chinese medicine composition described in the present embodiment is prepared by method acquisition, specifically includes following steps：
1）Fructus Zanthoxyli Plansipini, the wild spinach of above-mentioned weight portion are weighed respectively, is mixed, crushed, obtain comminuting matter I；Weigh respectively above-mentioned
The Folium seu Semen Daphniphylli macropodi of weight portion, horse knotweed, Herba euphorbiae lunulatae, Folium catalpae ovatae, the Radix Euphorbiae Pekinensis, fresh Herba Ranunculi Japonici and Gypsum Fibrosum, mixing are crushed, and obtain comminuting matter II；
2）The comminuting matter I is added to into supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is entered
Row frozen centrifugation, removes impurity, obtains extract I；
3）The water of 6 times of its weight is added in the comminuting matter II, is soaked 20 minutes, started supersonic generator, be heated to
70 DEG C, kept for 60 minutes, filtered while hot obtains filtrate I and medicinal residues；After I natural cooling of filtrate, the filtrate I is concentrated into
When 80 DEG C, relative density is 1.25 extractum；
4）The extract I and extractum are mixed, is dried, fully crushed, obtain final product.
In the present embodiment, step 2）Described in the pressure that extracts be 40MPa, extraction temperature is 30 DEG C, CO2Fluid flow is
55L/h, extraction time are 2h.
In the present embodiment, step 2）Described in ethanol volume fraction be 95%, addition is 200ml.
In the present embodiment, step 3）Described in extractum and the ethanol solution w/v 1g：20ml.
A kind of preparation method of the composite pesticide for peanut cultivation, comprises the following steps：
1）Weigh respectively 32 parts of the fowl and animal excrement of dry weight portion, 18 parts of peanut residue, 18 parts of Pepper stalk, 12 parts of pine needle powder and
8 parts of lignocellulose, mixing add organic matter decomposing inoculant, and mix is uniform, is covered using plastic foil, and it is 30% to control humidity,
Temperature is 50 DEG C, banks up 10 days, obtains the material that becomes thoroughly decomposed；
2）8 parts of 7 parts of the nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition of weight portion are weighed respectively, are mixed homogeneously with the material that becomes thoroughly decomposed, are controlled
Humidity processed is less than 10%, obtains final product composite pesticide.
The use of organic matter decomposing inoculant meets the requirement of industry standard NY609-00.
The using method of the composite pesticide for peanut cultivation is repeated no more with embodiment 1.
Embodiment 4：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 20 parts, 10 parts of peanut residue, 10 parts of Pepper stalk, 5 parts of pine needle powder, 3 parts of lignocellulose, 1 part of nitrogen-phosphorus-potassium compound fertilizer, Chinese medicine group
1 part of compound, the Chinese medicine composition is prepared from by the raw material of following weight portion：10 parts of Fructus Zanthoxyli Plansipini, 10 parts of wild spinach, Folium seu Semen Daphniphylli macropodi
10 parts, 10 parts of horse knotweed, 5 parts of Pericarpium Zanthoxyli, 5 parts of Herba euphorbiae lunulatae, 5 parts of Folium catalpae ovatae, 5 parts of Radix Et Rhizoma Nardostachyos, 3 parts of Folium Viticis Negundo, 3 parts of the Radix Euphorbiae Pekinensis.In the present embodiment,
In nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 1.5：0.6：0.4.
Embodiment 5：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 40 parts, 20 parts of peanut residue, 20 parts of Pepper stalk, 15 parts of pine needle powder, 12 parts of lignocellulose, 10 parts of nitrogen-phosphorus-potassium compound fertilizer, in
10 parts of drug composition, the Chinese medicine composition is prepared from by the raw material of following weight portion：30 parts of Fructus Zanthoxyli Plansipini, 30 parts of wild spinach,
30 parts of Folium seu Semen Daphniphylli macropodi, 30 parts of horse knotweed, 20 parts of Pericarpium Zanthoxyli, 20 parts of Herba euphorbiae lunulatae, 20 parts of Folium catalpae ovatae, 15 parts of Radix Et Rhizoma Nardostachyos, 12 parts of Folium Viticis Negundo, the Radix Euphorbiae Pekinensis 12
Part.In the present embodiment, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 2.5：1：0.8.
Embodiment 6：A kind of composite pesticide for peanut cultivation, is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 25 parts, 16 parts of peanut residue, 15 parts of Pepper stalk, 6 parts of pine needle powder, 10 parts of lignocellulose, 5 parts of nitrogen-phosphorus-potassium compound fertilizer, Chinese medicine
4 parts of compositionss, the Chinese medicine composition is prepared from by the raw material of following weight portion：12 parts of Fructus Zanthoxyli Plansipini, 15 parts of wild spinach, friendship allow
15 parts of wood, 18 parts of horse knotweed, 12 parts of Pericarpium Zanthoxyli, 10 parts of Herba euphorbiae lunulatae, 15 parts of Folium catalpae ovatae, 12 parts of Radix Et Rhizoma Nardostachyos, 8 parts of Folium Viticis Negundo, 7 parts of the Radix Euphorbiae Pekinensis.This reality
Apply in example, in nitrogen-phosphorus-potassium compound fertilizer, nitrogen, phosphorus, the weight ratio of potassium are 2.2：0.9：0.6.
Embodiment 7：The composite pesticide for peanut cultivation described by the present embodiment, as different from Example 1：Also wrap
Include：5 weight portion of microbial bacterial agent, the microbial bacterial agent by mass percent 50% bacillus thuringiensiss and 50% ball spore it is white
Stiff bacterium composition.
Bacillus thuringiensiss, Bacillus thuringiensis, active compound, effective bacterium number >=20,000,000,000/g；Ball spore is white
Stiff bacterium, Streptomyces microflavus, powder, effective bacterium number >=20,000,000,000 cfu/g.Above-mentioned microbial inoculum can be purchased by market
Buy acquisition or buy strain and voluntarily cultivate acquisition.
Embodiment 8：The composite pesticide for peanut cultivation described by the present embodiment, with embodiment 1 except that：Also
Including：4 weight portion of microbial bacterial agent, the microbial bacterial agent are white by 60% bacillus thuringiensiss of mass percent and 40% ball spore
Stiff bacterium composition.
Comparative example 1：For the composite pesticide of peanut cultivation, it is prepared from by the raw material of following weight portion：Fowl and animal excrement 35
Part, 15 parts of peanut residue, 15 parts of Pepper stalk, 10 parts of pine needle powder, 7 parts of lignocellulose, 6 parts of nitrogen-phosphorus-potassium compound fertilizer.Preparation method
Refering to embodiment 1.
Comparative example 2：For the composite pesticide of peanut cultivation, it is prepared from by the raw material of following weight portion：20 parts of Fructus Zanthoxyli Plansipini,
20 parts of wild spinach, 20 parts of Folium seu Semen Daphniphylli macropodi, 20 parts of horse knotweed, 12 parts of Pericarpium Zanthoxyli, 12 parts of Herba euphorbiae lunulatae, 12 parts of Folium catalpae ovatae, 10 parts of Radix Et Rhizoma Nardostachyos, Folium Viticis Negundo 7
Part, 7 parts of the Radix Euphorbiae Pekinensis.Preparation method refers to embodiment 1.
Comparative example 3：For the composite pesticide of peanut cultivation, formula refers to embodiment 1, Chinese medicine with embodiment 1, preparation method
Compositionss using the extracting method same with Folium seu Semen Daphniphylli macropodi, specifically with step 3）.
Effect assessment
Reagent agent：
Experimental group：A1~A8：It is followed successively by the pesticide of the preparation of embodiment 1 ~ 8；Matched group：B1~B3：It is followed successively by the preparation of comparative example 1 ~ 3
Pesticide；B0：Non- dispenser.
1.1 EXPERIMENTAL DESIGN
12 chemicals treatment of field design, are specifically shown in Table 1, and each reagent agent is done 3 groups and repeats to test.Experimental plot is divided into into 36
Part, per part be 50 ㎡, random alignment.
Before peanut seeding, reagent agent 100kg is uniformly spread fertilizer over the fields in every piece of experimental plot, harrows even rear bedder- planter.
Select to apply foliage top dressing in the initial bloom stage of peanut growth phase, lower pin phase, 3 critical periods of fruiting period.
1 chemicals treatment of table is designed
Note：☆ represents the period corresponding to chemicals treatment.
1.2 survey content and method
1.2.1 emergence rate investigation.After planting 15 days（May 15）Emergence rate investigation is carried out, and 100 plants is investigated per cell, is calculated
Seedling rate.
Death rate is investigated.When observe field have seedling death phenomenon to occur, that is, proceed by each cell main plot investigation, note
Record dead seedling situation, calculates death rate and relative death rate.
Death rate（%）=（Process dead seedling strain number/investigation total strain number）× 100,
With respect to death rate（%）=（Process the average death rate of death rate/control）×100.
1.2.2 diseases control investigation.Peanut sclerotium rolfsii is before dispenser, each investigation 1 in 5,10,15 days after last time dispenser
It is secondary, 5 points of samplings, per is fixed 5 piers, records morbidity strain number, the diseased plant order of severity.Using 0 ~ 4 grade of Pyatyi grade scale：0 grade,
Plant is asymptomatic；1 grade, only scab is produced in basal part of stem；2 grades, basal part of stem produces contracting symptom of hanging, less than 1/3 performance system of whole strain
System symptom (withered, dead, wilting etc.)；3 grades, less than the 2/3 of whole strain shows systemic symptom；4 grades, more than 2/3 performance of whole strain
Systemic symptom.Disease index and prevention effect are calculated, computing formula is as follows：
Disease index=［ ∑ (sick series × this grade of diseased plant number)/(highest disease series × investigation total strain number) ］ × 100；
Prevention effect (%)=［ (control disease index-process disease index)/control disease index ］ × 100.
1.2.3 subterranean pest-insect preventive effect is investigated.5 point are processed during September harvesting peanut on the 15th often, per takes 1 ㎡, investigation underground evil
Worm investigation, fruit number of causing harm, insect pest fruit number, calculate Revision insect recluced rate.Computing formula is as follows：
Revision insect recluced rate (%)=[(population number after the process of before processing insect population one)/before processing insect population] × 100.
1.2.4 effect of increasing production investigation.Observation impact of the reagent agent to peanut growth.Investigate each reagent agent to produce Semen arachidis hypogaeae
The impact of amount, often processes 5 points of investigation, per 5 piers of investigation, and carries out indoor species test, calculate effect of increasing production.
1.3 result
Impact of 2 dressing seed of table to Semen arachidis hypogaeae emergence rate and death rate
Note：Number of emerging survey scope is 100 plants of peanut plants selected in cell, and dead seedling number is then investigated all Semen arachidis hypogaeaes in cell and planted
Strain.
Table 2 shows that reagent agent of the present invention can promote to emerge, harmless to seed.
3 chemicals treatment of table prevents and treats the result of the test of peanut sclerotium rolfsii
Table 3 shows, applies chemicals treatment in the different stages, have different effects to preventing and treating peanut sclerotium rolfsii.A8 preventive effects are most
Good, A6 takes second place, compared with other treatment groups, it is sufficient to illustrate crucial in the initial bloom stage of peanut growth phase, lower pin phase, fruiting period 3
Period applies respectively and topdresses, and is more beneficial for the preventing and treating of southern blight.Contrast A2 ~ A4 can be seen that selection in the above three critical period
In arbitrary period apply, effect also has difference.Compared with A6, preventive effect significant difference shows that experimental group medicament is obtained to B1 ~ B3
More excellent prevention effect, material combination are more excellent, and potentiation is notable；And medicament preparation method affects the performance of drug effect.
4 chemicals treatment of table prevents and treats the result of the test of peanut soil pest
Table 4 shows, applies different chemicals treatment in different phase, have visibly different effect to preventing and treating peanut soil pest
Really.The best results of experimental group A8, A6 are taken second place.Experimental group general effect is superior to matched group.
5 chemicals treatment of table prevents and treats the yield survey result of Semen arachidis hypogaeae
Table 5 shows, can significantly improve the yield of Semen arachidis hypogaeae using medicament of the present invention, and whole using effect is more preferably.Change this
Invention formula and preparation method, have to yield and significantly affect, and this may have certain relation with the prevention effect of pest and disease damage.
Specifically, experimental group A8 and A6 has the rate of growth of use, experimental group A8 to be in initial bloom stage, lower pin phase, fruiting period
The rate of growth of 96.93%, A6 is 89.04%, illustrates that use of the microbial bacterial agent to medicament of the present invention has facilitation.Experimental group
A1 ~ A4 is only used in a certain period of sowing time, initial bloom stage, lower pin phase, fruiting period, and effect of increasing production is significantly lower than experimental group A6
And A8, and only for effect of increasing production, trophophase using effect be better than sowing time.The rate of growth of matched group B1 is
The rate of growth of 12.72%, B2 is 46.35% for the rate of growth of 29.48%, B3, than A6 and A8 for, equal significant difference illustrate
The combination collocation for inventing each raw material is suitable, and synergy is obvious.
The result of the test of 2 ~ table of table 5 shows that pesticide combination of the present invention can prevent and treat peanut sclerotium rolfsii, and effective control is entirely given birth to
Educate phase peanut soil pest（Mainly Holotrichia diomphalia Batess）Cause harm, significantly improve peanut yield, be suitable as Semen arachidis hypogaeae medicine fertilizer use.
Although the foregoing describing the specific embodiment of the present invention, those familiar with the art should manage
Solution, the specific embodiment described by us are merely exemplary, rather than for the restriction to the scope of the present invention, are familiar with this
The technical staff in field should be covered the present invention's in the equivalent modification and change made according to the spirit of the present invention
In scope of the claimed protection.
Claims (9)
1. a kind of composite pesticide for peanut cultivation, it is characterised in that：It is prepared from by the raw material of following weight portion：Manure of livestock and poultry
Just 20 ~ 40 parts, 10 ~ 20 parts of peanut residue, 10 ~ 20 parts of Pepper stalk, 5 ~ 15 parts of pine needle powder, 3 ~ 12 parts of lignocellulose, N P and K
1 ~ 10 part of compound fertilizer, 1 ~ 10 part of Chinese medicine composition, the Chinese medicine composition is prepared from by the raw material of following weight portion：Fructus Zanthoxyli Plansipini
10 ~ 30 parts, 10 ~ 30 parts of wild spinach, 10 ~ 30 parts of Folium seu Semen Daphniphylli macropodi, 10 ~ 30 parts of horse knotweed, 5 ~ 20 parts of Pericarpium Zanthoxyli, 5 ~ 20 parts of Herba euphorbiae lunulatae, Folium catalpae ovatae 5
~ 20 parts, 5 ~ 15 parts of Radix Et Rhizoma Nardostachyos, 3 ~ 12 parts of Folium Viticis Negundo, 3 ~ 12 parts of the Radix Euphorbiae Pekinensis.
2. the composite pesticide of peanut cultivation is used for as claimed in claim 1, it is characterised in that：The Chinese medicine composition is by as follows
The raw material of weight portion is prepared from：15 ~ 25 parts of Fructus Zanthoxyli Plansipini, 15 ~ 25 parts of wild spinach, 15 ~ 25 parts of Folium seu Semen Daphniphylli macropodi, 15 ~ 25 parts of horse knotweed, flower
10 ~ 15 parts of green pepper, 10 ~ 15 parts of Herba euphorbiae lunulatae, 10 ~ 15 parts of Folium catalpae ovatae, 8 ~ 12 parts of Radix Et Rhizoma Nardostachyos, 6 ~ 8 parts of Folium Viticis Negundo, 6 ~ 8 parts of the Radix Euphorbiae Pekinensis.
3. the composite pesticide of peanut cultivation is used for as claimed in claim 2, it is characterised in that：The Chinese medicine composition is by as follows
The raw material of weight portion is prepared from：20 parts of Fructus Zanthoxyli Plansipini, 20 parts of wild spinach, 20 parts of Folium seu Semen Daphniphylli macropodi, 20 parts of horse knotweed, 12 parts of Pericarpium Zanthoxyli, opal
12 parts of grass, 12 parts of Folium catalpae ovatae, 10 parts of Radix Et Rhizoma Nardostachyos, 7 parts of Folium Viticis Negundo, 7 parts of the Radix Euphorbiae Pekinensis.
4. the composite pesticide of peanut cultivation is used for as claimed in claim 3, it is characterised in that：By the raw material system of following weight portion
It is standby to form：30 ~ 35 parts of fowl and animal excrement, 12 ~ 18 parts of peanut residue, 12 ~ 18 parts of Pepper stalk, 8 ~ 12 parts of pine needle powder, lignocellulose 6
~ 8 parts, 5 ~ 7 parts of nitrogen-phosphorus-potassium compound fertilizer, 6 ~ 8 parts of Chinese medicine composition.
5. the composite pesticide of peanut cultivation is used for as claimed in claim 4, it is characterised in that：The Chinese medicine composition is by such as
Lower preparation method is obtained, and specifically includes following steps：
1）5 ~ 20 parts of 10 ~ 30 parts of Fructus Zanthoxyli Plansipini, 10 ~ 30 parts of wild spinach, 5 ~ 20 parts of Pericarpium Zanthoxyli and the Herba euphorbiae lunulatae of weight portion are weighed respectively, are mixed
Close, crush, obtain comminuting matter I；10 ~ 30 parts of the Folium seu Semen Daphniphylli macropodi of weight portion, 10 ~ 30 parts of horse knotweed, 5 ~ 20 parts of Folium catalpae ovatae, sweet is weighed respectively
3 ~ 12 parts of 5 ~ 15 parts of pine, 3 ~ 12 parts of Folium Viticis Negundo and the Radix Euphorbiae Pekinensis, mixing are crushed, and obtain comminuting matter II；
2）The comminuting matter I is added to into supercritical CO2In extraction kettle, ethanol is extracted for entrainer, and extract is carried out
Frozen centrifugation, removes impurity, obtains extract I；
3）The water of 4 ~ 6 times of its weight is added in the comminuting matter II, is soaked 15 ~ 20 minutes, start supersonic generator, plus
Heat is kept for 45 ~ 60 minutes to 60 ~ 70 DEG C, and filtered while hot obtains filtrate I and medicinal residues；After I natural cooling of filtrate, by the filter
When liquid I is concentrated into 75 ~ 80 DEG C, relative density is 1.20 ~ 1.25 extractum；
4）The extract I and extractum are mixed, is dried, fully crushed, obtain final product.
6. the composite pesticide of peanut cultivation is used for as claimed in claim 5, it is characterised in that：Step 2）Described in the pressure that extracts
Power is 30 ~ 40MPa, and extraction temperature is 30 ~ 45 DEG C, CO2Fluid flow is 40 ~ 55L/h, and extraction time is 2 ~ 4h.
7. the composite pesticide of peanut cultivation is used for as claimed in claim 6, it is characterised in that：Step 2）Described in ethanol body
Fraction is 90 ~ 95%, and addition is 200 ~ 400ml.
8. the composite pesticide of peanut cultivation is used for as claimed in claim 5, it is characterised in that：Step 3）Described in extractum and institute
State the w/v 1g of ethanol solution：10~20ml.
9. a kind of preparation method of the composite pesticide for peanut cultivation, it is characterised in that：Comprise the following steps：
1）30 ~ 35 parts of the fowl and animal excrement of dry weight portion, 12 ~ 18 parts of peanut residue, 12 ~ 18 parts of Pepper stalk, pine are weighed respectively
6 ~ 8 parts of 8 ~ 12 parts of pin powder and lignocellulose, mixing add organic matter decomposing inoculant, and mix is uniform, is covered using plastic foil,
It is 20 ~ 30% to control humidity, and temperature is 40 ~ 50 DEG C, banks up 7 ~ 10 days, obtains the material that becomes thoroughly decomposed；
2）1 ~ 10 part of 1 ~ 10 part of the nitrogen-phosphorus-potassium compound fertilizer and Chinese medicine composition of weight portion are weighed respectively, are mixed with the material that becomes thoroughly decomposed
Even, control humidity is less than 10%, obtains final product composite pesticide.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106946619A (en) * | 2017-05-02 | 2017-07-14 | 王丽雯 | A kind of composite fertilizer and preparation method thereof |
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Application publication date: 20170329 |