CN106520324A - Lubricant composition for nickel-based anti-wear alloy grinding machining process - Google Patents
Lubricant composition for nickel-based anti-wear alloy grinding machining process Download PDFInfo
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- CN106520324A CN106520324A CN201610963572.9A CN201610963572A CN106520324A CN 106520324 A CN106520324 A CN 106520324A CN 201610963572 A CN201610963572 A CN 201610963572A CN 106520324 A CN106520324 A CN 106520324A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/16—Naphthenic acids
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/086—Imides
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/041—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds involving a condensation reaction
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/022—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of hydrocarbons, e.g. olefines
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
- C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
- C10M2219/087—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Derivatives thereof, e.g. sulfurised phenols
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- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/045—Metal containing thio derivatives
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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- C10M2290/00—Mixtures of base materials or thickeners or additives
- C10M2290/04—Synthetic base oils
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
Abstract
The invention discloses a lubricant composition for a nickel-based anti-wear alloy grinding machining process. No. 7 industrial white oil is used as base oil and matched with a plurality of composite additives. The lubricant composition comprises an antioxidant, a metal deactivator, an oiliness agent, a friction modifier, an extreme-pressure agent, an anti-wear agent, an anti-rust agent, an anti-foaming agent, an anti-emulsifying agent, an anti-oxidant and anti-corrosive agent, a dispersant, a cooling accelerant and the like. The composition disclosed by the invention is high in cooling property, lubricating property, extreme-pressure anti-wear bearing property, diffusibility, cleaning property, anti-rust property and anti-oxidant and anti-corrosive property, low in volatility and smoke, capable of reducing surface scratches and abrasion of a workpiece, high in thermal capacity, high in surface smoothness, and long in anti-corrosive period.
Description
Technical field
A kind of nickel-base antiwear alloy grinding technique lubricant compositions of the present invention belong to metal working lubricant field.
Background technology
Nickel-base antiwear alloy main alloy element is chromium, molybdenum, tungsten, also containing a small amount of niobium, tantalum and indium.Except with wearability
Can be outer, its anti-oxidant, corrosion-resistant, welding performance might as well.Wear-resisting spare part can be manufactured, also can be as covering material, by built-up welding
Other substrate material surfaces are coated on spraying coating process.
Grinding fluid is that one kind is used in metal removal process, industrial with workpiece for cooling down and lubricating cutter
Liquid.Metal cutting is important mechanical processing toolses, and as used by which, cutting element type can be divided into two big class.One class is to use knife
Tool carries out machining, and such as turning, drilling, boring, milling, wound is cut and broached;Another kind of is that the grinding carried out with abrasive material adds
Work, such as grinding, the top gem of a girdle-pendant are cut, grinding and superfinishing etc..By processing severe arrangement, machining can be divided into 16 kinds, wherein
Grinding ranks the first.Cutting lubricant is divided into two big class so as to use, that is, cut lubricant and grinding lubricant, be required for good
Good cooling and lubricant effect, but two kinds of processing modes have basic difference.In grinding, grinding speed is up to
More than 1000r/min, temperature is more than 1100 DEG C, therefore it is required that there is higher cooling performance;In addition, grinding tool (such as emery wheel) hole holds
Easily block, also therefore need higher detergency.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of with good cooling, lubricity, extreme-pressure anti-wear carrying
Property, diffusivity, cleaning, rust-preventing characteristic, antioxygen anti-corrosive properties, low volatility, low smog reduce work piece surface cut and scratch,
Thermal capacity is big, and surface smoothness is high, the nickel alloy grinding technique lubricant compositions of anticorrosive cycle length.
The present invention solves above-mentioned technical problem by following technical solution:
A kind of nickel-base antiwear alloy grinding technique lubricant compositions, using oil based on No. 7 technical white oils, coordinate
Various compound additives, its each mass percent into being grouped into:
The mass percent summation of above each component is 100%.
Antioxidant is that dialkyl diphenylamine T534 of the sulfenyl phenolate T504 and 50% of mass ratio 50% is combined.
Metal deactivator is benzotriazole derivative T551.Oiliness improver is sulfurized lard.Friction improver is phosphate T451.
Extreme pressure agent is chlorinated paraffin T301.Antiwear additive is sulfide isobutene T321.
Antirust agent is that the zinc naphthenate T704 of the alkenyl succinic acid half ester T747 and 50% of mass ratio 50% is combined.
Anti-foaming agent is methyl-silicone oil T901.Anti emulsifier is amine and epoxide condensation product T1001.
Oxidation and corrosion inhibitor is molybdenum dithiophosphate MoPTC.Dispersant is polyisobutylene succinamide T154B.
Cryogen is urged to be petroleum sodium sulfonate.
The remarkable advantage of the present invention:There is the composition of the present invention good cooling, lubricity, extreme-pressure anti-wear to carry
Property, diffusivity, cleaning, rust-preventing characteristic, antioxygen anti-corrosive properties, low volatility, low smog reduces work piece surface cut and scratch,
Thermal capacity is big, and surface smoothness is high, and the anticorrosive cycle is long.
Specific embodiment
Embodiment 1:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
No. 7 technical white oils | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% is combined with 50% dialkyl diphenylamine (T534) | 0.04% |
Benzotriazole derivative (T551) | 0.03% |
Sulfurized lard | 4% |
Phosphate (T451) | 1% |
Chlorinated paraffin (T301) | 4% |
Sulfide isobutene (T321) | 3% |
The alkenyl succinic acid half ester (T747) of mass ratio 50% is combined with 50% zinc naphthenate (T704) | 0.05% |
Methyl-silicone oil (T901) | 10ppm |
Amine and epoxide condensation product (T1001) | 0.05% |
Molybdenum dithiophosphate (MoPTC) | 0.8% |
Polyisobutylene succinamide (T154B) | 1% |
Petroleum sodium sulfonate (T702) | 1% |
Above each component mass percentage content summation is 100%.
Embodiment 2:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
No. 7 technical white oils | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% is combined with 50% dialkyl diphenylamine (T534) | 0.1% |
Benzotriazole derivative (T551) | 0.06% |
Sulfurized lard | 6% |
Phosphate (T451) | 2% |
Chlorinated paraffin (T301) | 5% |
Sulfide isobutene (T321) | 5% |
The alkenyl succinic acid half ester (T747) of mass ratio 50% is combined with 50% zinc naphthenate (T704) | 0.1% |
Methyl-silicone oil (T901) | 20ppm |
Amine and epoxide condensation product (T1001) | 0.1% |
Molybdenum dithiophosphate (MoPTC) | 1.2% |
Polyisobutylene succinamide (T154B) | 2% |
Petroleum sodium sulfonate (T702) | 1.5% |
Above each component mass percentage content summation is 100%.
Embodiment 3:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
No. 7 technical white oils | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% is combined with 50% dialkyl diphenylamine (T534) | 0.2% |
Benzotriazole derivative (T551) | 0.1% |
Sulfurized lard | 8% |
Phosphate (T451) | 3% |
Chlorinated paraffin (T301) | 6% |
Sulfide isobutene (T321) | 6% |
The alkenyl succinic acid half ester (T747) of mass ratio 50% is combined with 50% zinc naphthenate (T704) | 0.2% |
Methyl-silicone oil (T901) | 30ppm |
Amine and epoxide condensation product (T1001) | 0.2% |
Molybdenum dithiophosphate (MoPTC) | 1.5% |
Polyisobutylene succinamide (T154B) | 4% |
Petroleum sodium sulfonate (T702) | 2% |
Above each component mass percentage content summation is 100%.
The typical physiochemical techniques index of 3 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 8.3 |
Flash-point (opening)/DEG C | 184 |
Condensation point/DEG C | -15 |
Viscosity index (VI) | 131 |
Coefficient of friction | 0.082 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 293 |
Shear stability (40 DEG C of kinematic viscosity rates of descent)/% | 3.5 |
Tetra-ball machine test/Pb/N | 888 |
Sintering load/PD/N | 6799 |
Terraced nurse agrees/N | 287 |
FZG/ levels | 14 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Demulsification number, 54 DEG C of (40-37-3)/min | 11 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
The typical physiochemical techniques index of 2 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 7.9 |
Flash-point (opening)/DEG C | 181 |
Condensation point/DEG C | -11 |
Viscosity index (VI) | 123 |
Coefficient of friction | 0.083 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 307 |
Shear stability (40 DEG C of kinematic viscosity rates of descent)/% | 3.8 |
Tetra-ball machine test/Pb/N | 895 |
Sintering load/PD/N | 6990 |
Terraced nurse agrees/N | 314 |
FZG/ levels | 14 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Demulsification number, 54 DEG C of (40-37-3)/min | 12 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
The typical physiochemical techniques index of 1 product of embodiment:
Project | Quality index |
Kinematic viscosity (40 DEG C)/mm2/s-1 | 8.4 |
Flash-point (opening)/DEG C | 179 |
Condensation point/DEG C | -13 |
Viscosity index (VI) | 112 |
Coefficient of friction | 0.081 |
Oxidation stability (rotary oxygen bomb, 150 DEG C)/min | 387 |
Shear stability (40 DEG C of kinematic viscosity rates of descent)/% | 3.2 |
Tetra-ball machine test/Pb/N | 886 |
Sintering load/PD/N | 6850 |
Terraced nurse agrees/N | 304 |
FZG/ levels | 14 |
Corrosivity (copper sheet, 100 DEG C, 3h)/level | 1 |
Demulsification number, 54 DEG C of (40-37-3)/min | 9 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
Claims (9)
1. a kind of nickel-base antiwear alloy grinding technique lubricant compositions, it is characterised in that:No. 7 technical white oils are adopted for base
Plinth oil, coordinates various compound additives, its each mass percent into being grouped into:
The mass percent summation of above each component is 100%.
2. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that anti-
Oxygen agent is that dialkyl diphenylamine T534 of the sulfenyl phenolate T504 and 50% of mass ratio 50% is combined.
3. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that gold
Category passivator is benzotriazole derivative T551.
4. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that oil
Property agent is sulfurized lard;Friction improver is phosphate T451.
5. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that pole
Pressure agent is chlorinated paraffin T301;Antiwear additive is sulfide isobutene T321.
6. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that anti-
Rust agent is that the zinc naphthenate T704 of the alkenyl succinic acid half ester T747 and 50% of mass ratio 50% is combined.
7. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that anti-
Infusion is methyl-silicone oil T901;Anti emulsifier is amine and epoxide condensation product T1001.
8. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that anti-
Oxygen anti-corrosion additive is molybdenum dithiophosphate MoPTC;Dispersant is polyisobutylene succinamide T154B.
9. a kind of nickel-base antiwear alloy grinding technique lubricant compositions as claimed in claim 1, it is characterised in that urge
Cryogen is petroleum sodium sulfonate.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104450087A (en) * | 2014-11-27 | 2015-03-25 | 昆山瑞昱化工有限公司 | Environmentally-friendly antirust cutting agent |
CN105062630A (en) * | 2015-07-20 | 2015-11-18 | 广西大学 | Lubricant for drawn austenitic stainless steel wire material |
CN105838487A (en) * | 2016-05-10 | 2016-08-10 | 浙江师范大学 | Low-oil-mist grinding oil and preparation method thereof |
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2016
- 2016-11-04 CN CN201610963572.9A patent/CN106520324A/en not_active Withdrawn
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CN105062630A (en) * | 2015-07-20 | 2015-11-18 | 广西大学 | Lubricant for drawn austenitic stainless steel wire material |
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