CN106520323A - 一种钴合金强力温旋压加工工艺润滑剂组合物 - Google Patents

一种钴合金强力温旋压加工工艺润滑剂组合物 Download PDF

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CN106520323A
CN106520323A CN201610963571.4A CN201610963571A CN106520323A CN 106520323 A CN106520323 A CN 106520323A CN 201610963571 A CN201610963571 A CN 201610963571A CN 106520323 A CN106520323 A CN 106520323A
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lubricant composition
cobalt alloy
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pressing processing
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黄福川
唐弓斌
肖锋
张姗姗
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Guangxi University
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Abstract

本发明公开了一种钴合金强力温旋压加工工艺润滑剂组合物，采用50％的MIV90BS基础油和50％的酯类油(Radialube7251)复合作为复合基础油，配合多种复合添加剂。包括：抗氧剂、金属减活剂、油性剂、摩擦改进剂、极压剂、抗磨剂、防锈剂、抗泡剂、抗氧抗腐剂、增粘剂等。本发明的组合物具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性以及粘附性，减少表面擦伤和划痕。

Description

一种钴合金强力温旋压加工工艺润滑剂组合物
技术领域
本发明一种钴合金强力温旋压加工工艺润滑剂组合物属于金属加工工艺润滑剂领域。
背景技术
钴基高温合金是高温合金中的一种，它是以钴作为主要成分，含有相当数量的镍、铬、钨和少量的钼、铌、钽、钛、镧等合金元素，偶而也还含有铁的一类合金。根据合金中成分不同，它们可以制成焊丝，粉末用于硬面堆焊，热喷涂、喷焊等工艺，也可以制成铸锻件和粉末冶金件。与其它高温合金不同，钴基高温合金不是由与基体牢固结合的有序沉淀相来强化，而是由已被固溶强化的奥氏体fcc基体和基体中分布少量碳化物组成。钴基高温合金中碳化物的热稳定性较好。钴基高温合金是含钴量40～65％的奥氏体高温合金。在730～1100℃条件下具有一定的高温强度、良好的抗热腐蚀和抗氧化能力。适于制作航空喷气发动机、工业燃气轮机、舰船燃气轮机的导向叶片和喷嘴导叶以及柴油机喷嘴等。
强力旋压工艺主要依靠坯料厚度的变薄来实现成形的，坯料外径基本保持不变。通常在进行强力旋压时，旋轮加于坯料的压强要比普通旋压时大得多，坯料的变形情况和普通旋压时大得多，坯料的变形情况和普通旋压时也大不相同。在普通旋压过程中，坯料厚度变化不大，但直径变化很大——由大变小或由小变大。而在强旋压过程中，坯料直径基本保持不变，但厚度变化很大——由厚变薄。因此强力旋压又称为变薄旋压。从工艺过程分析认为：强力旋压属轴向延展，变形区材料处在二向或三向应力状态，因而可产生较高的变形程度。根据旋压件的类型和金属变形机理的差异，强力旋压可分为锥形件强力旋压——剪切旋压和筒形件强力旋压——挤出强旋等两种。强力旋压用于各种、锥体等形体的旋压成型壳体的加工技术，是一种比较成熟的方法和工艺，也叫烫板法。钴合金强力温旋压润滑剂要求能降低强力旋压加工负荷，促进金属在模具中流动，防止模具卡死，减少模具磨损和材料损耗，加快散热，提高强力旋压工件质量和生产效率。
发明内容
本发明要解决的技术问题是提供一种具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性以及粘附性，减少表面擦伤和划痕的钴合金强力温旋压加工工艺润滑剂组合物。
本发明通过如下技术方案解决上述技术问题：
一种钴合金强力温旋压加工工艺润滑剂组合物，采用质量比50％的酯类油(Radialube7251)和50％的MIV90BS基础油复合为复合基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量
基础油 余量
抗氧剂 0.05～0.3％
金属减活剂 0.3～0.6％
油性剂 5～8％
摩擦改进剂 1～2％
极压剂 3～5％
抗磨剂 4～6％
防锈剂 0.08～0.3％
抗氧抗腐剂 0.8～1.5％
增粘剂 4～6％
以上各组分的质量百分比总和是100％。
抗氧剂是采用质量比50％的N-苯基-α-萘胺T591和50％的4，4-亚甲基双(T511)复合。
金属减活剂是采用质量比50％的2-硫基苯并咪唑和50％的噻二唑衍生物复合。
油性剂是硫化棉籽油T404。摩擦改进剂是硫磷酸钼T461。
极压剂是硼化磷胺酯T3011。抗磨剂是硫化异丁烯T321。
防锈剂是质量比50％的石油磺酸钠T702和50％的苯并三氮唑T706复合。
抗氧抗腐剂是二烷基二硫代氨基甲酸硫化氧钼MoPTC。增粘剂是异丁烯T603C。
本发明的优点在于：
本发明的组合物具有良好的冷却性、润滑性(极压抗磨承载性)、扩散性、清洗性、防锈性、抗氧防腐性以及粘附性，减少表面擦伤和划痕；能降低强力旋压加工负荷，促进金属在模具中流动，防止模具卡死，减少模具磨损和材料损耗，加快散热，提高强力旋压工件质量和生产效率。
具体实施方式
实施例1：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例2：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 24.5
闪点(开口)/℃ 277
凝点/℃ -12
粘度指数 142
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 15
氧化安定性(旋转氧弹法，150℃)，min 312
四球机试验，Pb/N 968
烧结负荷，PD/N 6520
梯姆肯，N 301
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 5.6
实施例2产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 22.9
闪点(开口)/℃ 272
凝点/℃ -11
粘度指数 153
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 15
氧化安定性(旋转氧弹法，150℃)，min 309
四球机试验，Pb/N 952
烧结负荷，PD/N 6520
梯姆肯，N 304
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 5.9
实施例1产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 24.9
闪点(开口)/℃ 278
凝点/℃ -12
粘度指数 146
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 15
氧化安定性(旋转氧弹法，150℃)，min 322
四球机试验，Pb/N 951
烧结负荷，PD/N 6480
梯姆肯，N 297
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 5.1

Claims (10)

1.一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于：采用质量比50％的酯类油Radialube7251和50％的MIV90BS基础油复合为复合基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量 基础油 余量 抗氧剂 0.05～0.3％ 金属减活剂 0.3～0.6％ 油性剂 5～8％ 摩擦改进剂 1～2％ 极压剂 3～5％ 抗磨剂 4～6％ 防锈剂 0.08～0.3％ 抗氧抗腐剂 0.8～1.5％ 增粘剂 4～6％
以上各组分的质量百分比总和是100％。
2.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于抗氧剂是采用质量比50％的N-苯基-α-萘胺T591和50％的4,4-亚甲基双T511复合。
3.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于金属减活剂是采用质量比50％的2-硫基苯并咪唑和50％的噻二唑衍生物复合。
4.权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于油性剂是硫化棉籽油T404。
5.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于摩擦改进剂是硫磷酸钼T461。
6.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于极压剂是硼化磷胺酯T3011。
7.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于抗磨剂是硫化异丁烯T321。
8.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于防锈剂是质量比50％的石油磺酸钠T702和50％的苯并三氮唑T706复合。
9.如权利要求1所述的一种钴合金强力温旋压加工工艺润滑剂组合物，其特征在于抗氧抗腐剂是二烷基二硫代氨基甲酸硫化氧钼MoPTC。
10.如权利要求1所述的一种钴合强力温金旋压加工工艺润滑剂组合物，其特征在于增粘剂是异丁烯T603C。
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