CN106520341A - 一种钨合金强力温旋压加工工艺润滑剂组合物 - Google Patents

一种钨合金强力温旋压加工工艺润滑剂组合物 Download PDF

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CN106520341A
CN106520341A CN201610966163.4A CN201610966163A CN106520341A CN 106520341 A CN106520341 A CN 106520341A CN 201610966163 A CN201610966163 A CN 201610966163A CN 106520341 A CN106520341 A CN 106520341A
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tungsten alloy
processing technology
agent
pressing processing
rotary pressing
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黄福川
王玥
潘发存
胡雄风
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Guangxi University
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Abstract

本发明公开了一种钨合金强力温旋压加工工艺润滑剂组合物，采用质量比50％的茂金属聚α‑烯烃基础油和50％的酯类油Radialube7251复合作为基础油，配合多种复合添加剂。包括：抗氧剂、金属减活剂、油性剂、极压剂、抗磨剂、防锈剂、抗氧抗腐剂、填充剂、摩擦改进剂等。本发明的组合物具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性；有良好的热氧化安定性、减摩极压抗磨、粘附性，足够的油膜强度和厚度。

Description

一种钨合金强力温旋压加工工艺润滑剂组合物
技术领域
本发明一种钨合金强力温旋压加工工艺润滑剂组合物属于金属加工润滑剂领域。
背景技术
钨合金是以钨为基加入其他元素组成的合金。在金属中，钨的熔点最高，高温强度和抗蠕变性能以及导热、导电和电子发射性能都好，比重大，除大量用于制造硬质合金和作合金添加剂外，钨及其合金广泛用于电子、电光源工业，也在航天、铸造、武器等部门中用于制作火箭喷管、压铸模具、穿甲弹芯、触点、发热体和隔热屏等。
强力旋压工艺主要依靠坯料厚度的变薄来实现成形的，坯料外径基本保持不变。通常在进行强力旋压时，旋轮加于坯料的压强要比普通旋压时大得多，坯料的变形情况和普通旋压时大得多，坯料的变形情况和普通旋压时也大不相同。在普通旋压过程中，坯料厚度变化不大，但直径变化很大——由大变小或由小变大。而在强旋压过程中，坯料直径基本保持不变，但厚度变化很大——由厚变薄。因此强力旋压又称为变薄旋压。从工艺过程分析认为：强力旋压属轴向延展，变形区材料处在二向或三向应力状态，因而可产生较高的变形程度。根据旋压件的类型和金属变形机理的差异，强力旋压可分为锥形件强力旋压——剪切旋压和筒形件强力旋压——挤出强旋等两种。强力旋压用于各种、锥体等形体的旋压成型壳体的加工技术，是一种比较成熟的方法和工艺，也叫烫板法。
钨合金强力温旋压润滑要求有良好的热氧化安定性、减摩极压抗磨、粘附性，足够的油膜强度和厚度，以克服温旋压加工过程中的下压力大，材料强度高，延展性差，变形困难，模具损害大的问题。
发明内容
本发明要解决的技术问题是提供一种具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性、氧化安定性以及粘附性，减少表面擦伤和划痕的钨合金强力温旋压加工工艺润滑剂组合物。
本发明通过如下技术方案解决上述技术问题：降低强力温旋压加工负荷，促进金属在模具中流动，防止模具卡死，减少模具磨损和材料损耗，加快散热，提高强力温旋压工件质量和生产效率。
一种钨合金强力温旋压加工工艺润滑剂组合物，采用质量比50％的茂金属聚α-烯烃基础油和50％的酯类油(Radialube7251)复合为复合基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量
基础油 余量
抗氧剂 0.06～0.3％
金属减活剂 0.05～0.2％
油性剂 4～8％
极压剂 3～5％
抗磨剂 4～6％
防锈剂 0.06～0.3％
抗氧抗腐剂 0.8～1.5％
填充剂 4～6％
摩擦改进剂 1～3％
以上各组分的质量百分比总和是100％。
抗氧剂是采用质量比50％的二烷基苯胺T534和50％的硫化烷基酚T504复合。
金属减活剂是采用质量比50％的苯三唑衍生物T551和50％的噻重氮复合。
油性剂是硫化猪油。
摩擦极压剂是酸性亚磷酸二丁酯T304。
抗磨剂是硫化异丁烯T321。
防锈剂是质量比50％的石油磺酸钠T702和50％的苯并三氮唑T706复合。
抗氧抗腐剂是二烷基二硫代氨基甲酸钨。
填充剂是全精炼石蜡70号。
摩擦改进剂是硫磷酸钼T461。
本发明的优点在于：
本发明的组合物具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性；有良好的热氧化安定性、减摩极压抗磨、粘附性，足够的油膜强度和厚度，以克服温旋压加工过程中的下压力大，材料强度高，延展性差，变形困难，模具损害大的问题。
具体实施方式
实施例1：
将以下各组分按下列质量百分比调和而成：
组分 质量百分比含量
质量比50％的茂金属聚α-烯烃基础油和酯类油(Radialube7251)复合 余量
质量比50％的二烷基苯胺(T534)和50％的硫化烷基酚(T504)复合 0.1％
质量比50％的苯三唑衍生物(T551)和50％的噻重氮复合 0.1％
硫化猪油 5.0％
酸性亚磷酸二丁酯(T304) 3.0％
硫化异丁烯(T321) 5.0％
质量比50％的石油磺酸钠(T702)和50％的苯并三氮唑(T706)复合 0.1％
二烷基二硫代氨基甲酸钨 1.1％
全精炼石蜡70号 5.0％
硫磷酸钼(T461) 2.3％
以上各组分质量百分比含量总和为100％。
实施例2：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 33.6
闪点(开口)/℃ 276
凝点/℃ -35
粘度指数 156
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 13
氧化安定性(旋转氧弹法，150℃)，min 382
四球机试验，Pb/N 921
烧结负荷，PD/N 6580
梯姆肯，N 306
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 7.6
实施例2产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 31.9
闪点(开口)/℃ 271
凝点/℃ -35
粘度指数 161
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 11
氧化安定性(旋转氧弹法，150℃)，min 372
四球机试验，Pb/N 916
烧结负荷，PD/N 6515
梯姆肯，N 298
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 8.2
实施例1产品的主要技术指标
项目 指标
100℃运动粘度/(mm2﹒s-1) 32.6
闪点(开口)/℃ 271
凝点/℃ -35
粘度指数 166
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-37-3)/min 12
氧化安定性(旋转氧弹法，150℃)，min 379
四球机试验，Pb/N 913
烧结负荷，PD/N 6525
梯姆肯，N 301
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 8.6

Claims (9)

1.一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于是：采用质量比50％的茂金属聚α-烯烃基础油和50％的酯类油Radialube7251为基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量 基础油 余量 抗氧剂 0.06～0.3％ 金属减活剂 0.05～0.2％ 油性剂 4～8％ 极压剂 3～5％ 抗磨剂 4～6％ 防锈剂 0.06～0.3％ 抗氧抗腐剂 0.8～1.5％ 填充剂 4～6％ 摩擦改进剂 1～3％
以上各组分的质量百分比总和是100％。
2.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于抗氧剂是采用质量比50％的二烷基苯胺T534和50％的硫化烷基酚T504复合。
3.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于金属减活剂是采用质量比50％的苯三唑衍生物T551和50％的噻重氮复合。
4.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于油性剂是硫化猪油。
5.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于摩擦极压剂是酸性亚磷酸二丁酯T304。
6.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于抗磨剂是硫化异丁烯T321。
7.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于防锈剂是质量比50％的石油磺酸钠T702和50％的苯并三氮唑T706复合。
8.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于抗氧抗腐剂是二烷基二硫代氨基甲酸钨。
9.如权利要求1所述的一种钨合金强力温旋压加工工艺润滑剂组合物，其特征在于填充剂是全精炼石蜡70号；摩擦改进剂是硫磷酸钼T461。
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Publication number Priority date Publication date Assignee Title
CN104974833A (zh) * 2015-07-20 2015-10-14 广西大学 旋转冷锻钛合金润滑剂组合物

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Publication number Priority date Publication date Assignee Title
CN104974833A (zh) * 2015-07-20 2015-10-14 广西大学 旋转冷锻钛合金润滑剂组合物

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丰华: "《石油加工助剂及石油产品添加剂加工配制与生产应用最新工艺技术操作手册（第一卷）》", 30 June 2006, 中国科技文化出版社 *

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