CN106520321A - 一种钴合金旋压加工工艺润滑剂组合物 - Google Patents

一种钴合金旋压加工工艺润滑剂组合物 Download PDF

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CN106520321A
CN106520321A CN201610963568.2A CN201610963568A CN106520321A CN 106520321 A CN106520321 A CN 106520321A CN 201610963568 A CN201610963568 A CN 201610963568A CN 106520321 A CN106520321 A CN 106520321A
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lubricant composition
cobalt alloy
processing technology
pressing processing
rotary pressing
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黄福川
张姗姗
肖锋
唐弓斌
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Guangxi University
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Abstract

本发明公开了一种钴合金旋压加工工艺润滑剂组合物，采用50％的酯类Radialube7251和50％的MIV750基础油复合作为基础油，配合多种复合添加剂。包括：抗氧剂、金属减活剂、油性剂、摩擦改进剂、极压剂、抗磨剂、防锈剂、抗氧防腐剂、增粘剂等。本发明的组合物具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性，减少表面擦伤和刮伤以及粘附性强。

Description

一种钴合金旋压加工工艺润滑剂组合物
技术领域
本发明一种钴合金旋压加工工艺润滑剂组合物属于金属加工润滑剂领域。
背景技术
钴基高温合金是高温合金中的一种，它是以钴作为主要成分，含有相当数量的镍、铬、钨和少量的钼、铌、钽、钛、镧等合金元素，偶而也还含有铁的一类合金。根据合金中成分不同，它们可以制成焊丝，粉末用于硬面堆焊，热喷涂、喷焊等工艺，也可以制成铸锻件和粉末冶金件。与其它高温合金不同，钴基高温合金不是由与基体牢固结合的有序沉淀相来强化，而是由已被固溶强化的奥氏体fcc基体和基体中分布少量碳化物组成。钴基高温合金中碳化物的热稳定性较好。钴基高温合金是含钴量40～65％的奥氏体高温合金。在730～1100℃条件下具有一定的高温强度、良好的抗热腐蚀和抗氧化能力。适于制作航空喷气发动机、工业燃气轮机、舰船燃气轮机的导向叶片和喷嘴导叶以及柴油机喷嘴等。
旋压技术起源于古代制陶工艺。他是一种综合了锻造、挤压、拉件、弯曲、环轧、横轧和滚挤等工艺特点的少无切削加工的先进工艺。通常将金属简坯、平板毛坯或预制坯用尾顶顶紧在旋压机模上，由主轴带动芯棒和坯料旋转；同时旋压轮从毛坯一侧将材料挤压在旋转的芯模上，使材料产生逐点连续的塑性变形，从而获得各种母线形状的空心旋转体零件。根据旋压加工过程中的毛坯厚度变化情况，把旋压工艺分为普通旋压和强力旋压两种，即普通旋压和强力旋压。
普通旋压简称普旋。普旋过程中毛坯的厚度基本保持不变，成形主要依靠坯料沿圆周的收缩及沿半径方向上伴长不变形来实现。其主要特征是在成形过程中，可以明显看出坯料外径的变化。普通旋压的基本方式有：拉深旋压(拉旋)、缩径旋压(缩旋)和扩径旋压(扩旋)等三种。钴合金旋压加工工艺润滑剂要求能降低旋压加工负荷，促进金属在模具中流动，防止模具卡死，减少模具磨损和材料损耗，加快散热，提高旋压工件质量、残屑回收率和生产效率。
发明内容
本发明要解决的技术问题是提供一种具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性，减少表面擦伤和刮伤以及粘附性强的钴合金旋压加工工艺润滑剂组合物。
本发明通过如下技术方案解决上述技术问题：
一种钴合金旋压加工工艺润滑剂组合物，采用质量比50％的酯类Radialube7251和50％的MIV750基础油复合为基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量
基础油 余量
抗氧剂 0.06～0.2％
金属减活剂 0.05～0.5％
油性剂 4～6％
摩擦改进剂 2～3％
极压剂 2～4％
抗磨剂 4～6％
防锈剂 0.06～0.5％
抗氧抗腐剂 0.5～1.2％
增粘剂 2～5％
以上各组分的质量百分比总和是100％。
抗氧剂是采用质量比50％的4，4-亚甲基双T511和50％的二烷基二苯胺T534复合。
金属减活剂是苯三唑衍生物T551。油性剂是硫化烯烃棉籽油T405A。
摩擦改进剂是硫磷酸钼。极压剂是酸性亚磷酸二丁酸T304。
抗磨剂是氯化石蜡T501。
防锈剂是质量比50％的石油磺酸钠T702和50％的2-硫基苯并三氮唑复合。
抗氧抗腐剂是二烷基二硫代氨基甲酸硫化氧钼MoPTC。增粘剂是乙丙共聚物T603C。
本发明的优点在于：
本发明的组合物具有良好的冷却性、润滑性、扩散性、清洗性、防锈性、抗氧防腐性，减少表面擦伤和刮伤以及粘附性强，能降低旋压加工负荷，促进金属在模具中流动，防止模具卡死，减少模具磨损和材料损耗，加快散热，提高旋压工件质量、残屑回收率和生产效率。
具体实施方式
实施例1：
将以下各组分按下列质量百分比调和而成：
组分 质量百分比含量
质量比50％的酯类(Radialube7251)和50％的MIV750基础油复合 余量
质量比50％的4，4-亚甲基双(T511)和50％的二烷基二苯胺(T534)复合 0.15％
苯三唑衍生物(T551) 0.1％
硫化烯烃棉籽油(T405A) 5.0％
硫磷酸钼 2.5％
酸性亚磷酸二丁酸(T304) 3.0％
氯化石蜡(T501) 4.5％
质量比50％的石油磺酸钠(T702)和50％的2-硫基苯并三氮唑复合 0.1％
二烷基二硫代氨基甲酸硫化氧钼(MoPTC) 1.1％
乙丙共聚物(T603C) 2.45％
以上各组分质量百分比含量总和为100％。
实施例2：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3：
将以下各组分按下列质量百分比调和而成：
以上各组分质量百分比含量总和为100％。
实施例3产品的主要技术指标
项目 指标
40℃运动粘度/(mm2﹒s-1) 166.8
闪点(开口)/℃ 262
凝点/℃ -18
粘度指数 98
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-40-6)/min 13
四球机试验，Pb/N 935
烧结负荷，PD/N 6105
梯姆肯，N 325
FZG，级 13
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 8.5
实施例2产品的主要技术指标
项目 指标
40℃运动粘度/(mm2﹒s-1) 167.4
闪点(开口)/℃ 275
凝点/℃ -20
粘度指数 96
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-40-6)/min 13
四球机试验，Pb/N 921
烧结负荷，PD/N 5990
梯姆肯，N 309
FZG，级 13
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 8.2
实施例1产品的主要技术指标
项目 指标
40℃运动粘度/(mm2﹒s-1) 165.9
闪点(开口)/℃ 267
凝点/℃ -18
粘度指数 102
腐蚀(铜片、100℃、3h)/级 1
抗乳化度82℃(40-40-6)/min 12
四球机试验，Pb/N 945
烧结负荷，PD/N 6015
梯姆肯，N 331
FZG，级 13
水分，％ 痕迹
机械杂质，％ 无
蒸发损失(Noack法,250℃,1h)(m),％ 8.8

Claims (10)

1.一种钴合金旋压加工工艺润滑剂组合物，其特征在于：采用质量比50％的酯类油Radialube7251和50％的MIV750基础油复合为复合基础油，配合多种复合添加剂，其各自质量百分数的成分组成：
组分 质量百分比含量 基础油 余量 抗氧剂 0.06～0.2％ 金属减活剂 0.05～0.5％ 油性剂 4～6％ 摩擦改进剂 2～3％ 极压剂 2～4％ 抗磨剂 4～6％ 防锈剂 0.06～0.5％ 抗氧抗腐剂 0.5～1.2％ 增粘剂 2～5％
以上各组分的质量百分比总和是100％。
2.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于抗氧剂是采用质量比50％的4，4-亚甲基双T511和50％的二烷基二苯胺T534复合。
3.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于金属减活剂是苯三唑衍生物T551。
4.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于油性剂是硫化烯烃棉籽油T405A。
5.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于摩擦改进剂是硫磷酸钼。
6.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于极压剂是酸性亚磷酸二丁酸T304。
7.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于抗磨剂是氯化石蜡T501。
8.权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于防锈剂是质量比50％的石油磺酸钠T702和50％的2-硫基苯并三氮唑复合。
9.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于抗氧抗腐剂是二烷基二硫代氨基甲酸硫化氧钼MoPTC。
10.如权利要求1所述的一种钴合金旋压加工工艺润滑剂组合物，其特征在于增粘剂是乙丙共聚物T603C。
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Publication number Priority date Publication date Assignee Title
CN104862035A (zh) * 2015-06-05 2015-08-26 广西大学 冷旋压钛合金管润滑剂组合物

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Publication number Priority date Publication date Assignee Title
CN104862035A (zh) * 2015-06-05 2015-08-26 广西大学 冷旋压钛合金管润滑剂组合物

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