CN106348599A - Vermilion glaze and preparation method thereof - Google Patents
Vermilion glaze and preparation method thereof Download PDFInfo
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- CN106348599A CN106348599A CN201610833801.5A CN201610833801A CN106348599A CN 106348599 A CN106348599 A CN 106348599A CN 201610833801 A CN201610833801 A CN 201610833801A CN 106348599 A CN106348599 A CN 106348599A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/10—Frit compositions, i.e. in a powdered or comminuted form containing lead
Abstract
The invention belongs to the technical field of Jun porcelain glaze and particularly relates to vermilion glaze and a preparation method thereof. The vermilion glaze is prepared from, by weight, 80-100 parts of SiO2, 10-15 parts of Al2O3, 60-80 parts of Pb3O4, 20-30 parts of Na2B4O7, 3-8 parts of Na2O, 4-8 parts of K2O, 5-8 parts of ZnO, 4-10 parts of B2O3, 10-15 parts of CdSe and 10-15 parts of CdS. The preparation method of the vermillion glaze has wide application scope and is easy to understand and plays a good role in production cost reduction and technician training. The vermilion glaze is new-colored glaze and is progress in the innovation of colored glaze.
Description
Technical field
The invention belongs to pottery glaze technical field is and in particular to a kind of bright red glaze and preparation method thereof.
Background technology
China's pottery has a long history, and is the outstanding representative of human civilization progress, spread all over now we life each
Field, improves our quality of life.With the progress of technique, the quality of pottery is also lifted constantly, various on market
Pottery system various in style tinkling of jades meet the eye on every side, its practicality and dicoration are all stronger, but are from making more than the dicoration of existing pottery
To innovate in type, its color is also relatively single few, colored glaze still awaits innovating hyperchromic, to meet creation and decoration demand.Red
Color is one of favorite color of the whole mankind, because redness signifies the sun, life, good harvest, luckiness, complies with one's wishes etc. that all are fine
Things.Vermilion, the favorite color of this Chinese people, it is noble, magnificent, ardent, it have rich culture intension and
The lofty moral stature.But vermeil pottery is at present also fewer, be badly in need of a kind of stable bright red colour glaze of research and development and its
Preparation method, to meet the needs of people.
Content of the invention
For the deficiencies in the prior art, the present invention proposes a kind of bright red glaze and preparation method thereof, in order to make up existing skill
The deficiency of art.
The technical scheme is that and be achieved in that: a kind of bright red glaze, it is by the raw material system of following parts by weight
Standby: sio280 to 100 parts, al2o310 to 15 parts, pb3o460 to 80 parts, na2b4o720 to 30 parts, na2O 3 to 8
Part, k25 to 8 parts of 4 to 8 parts of o, zno, b2o34 to 10 parts, 10 to 15 parts of 10 to 15 parts of cdse, cds.
It is to be prepared from by the raw material of following parts by weight: sio290 parts, al2o312 parts, pb3o475 parts,
na2b4o725 parts, na26 parts of o, k26 parts of 5 parts of o, zno, b2o38 parts, 12 parts of 12 parts of cdse, cds.
Its preparation method is as follows:
1) choose the sio of above-mentioned weight portion2, al2o3, pb3o4, na2b4o7, na2O, k2O, zno, b2o3, mix homogeneously,
Obtain compound；
2) compound is crossed after 80 mesh sieves, melting 1 to 1 .5 hour at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching, obtain block glaze；
3) by block glaze after wet ball grinding, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/ml, by glaze
Slurry imposes on billet surface, after the moisture being dried to glaze slip is less than 1%, respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C
Alternately fire 2 times, each firing time is 20 to 30 minutes, after cooling, obtain mixing glaze；
4) choose cdse, the cds of above-mentioned weight portion, make their mix homogeneously, then they are entered ball milling 20h, obtain cadmium selenium
Glaze；
5) by obtained mixing glaze in step 3) and step 4) and cadmium selenium glaze mix homogeneously, obtain bright red glaze.
Described drying is to dry at 80 to 160 DEG C.
Described melting is carried out in box siliconits resistance furnace.
Described it is cooled to naturally cool to room temperature with stove.
The present invention has following beneficial effect: the range of application of the preparation method of described bright red glaze disclosed by the invention
Wide and it can be readily appreciated that goodish effect is all played in the reduction to production cost and the training to technical staff；Zhu of the present invention
In preparation process, fusion process adopts stagewise to red glaze, and sintering procedure is alternately fired using high and low temperature, by this shape
The melting of formula and fire each component of guarantee and effectively combine, and then obtain the preferably bright red glaze of the uniformity；Present invention bright red glaze
Add a new color for colored glaze, the innovation for colored glaze enhances a step again.
Specific embodiment
A kind of bright red glaze, it is to be prepared from by the raw material of following parts by weight: sio280 to 100 parts, al2o310
To 15 parts, pb3o460 to 80 parts, na2b4o720 to 30 parts, na23 to 8 parts of o, k25 to 8 parts of 4 to 8 parts of o, zno, b2o34 to
10 parts, 10 to 15 parts of 10 to 15 parts of cdse, cds.It is to be prepared from by the raw material of following parts by weight: sio290 parts,
al2o312 parts, pb3o475 parts, na2b4o725 parts, na26 parts of o, k26 parts of 5 parts of o, zno, b2o38 parts, 12 parts of cdse, cds
12 parts.Its preparation method is as follows: 1) chooses the sio of above-mentioned weight portion2, al2o3, pb3o4, na2b4o7, na2O, k2O, zno
, b2o3, mix homogeneously, obtain compound；2) compound is crossed after 80 mesh sieves, melting 1 to 1 .5 hour at 900 to 1000 DEG C,
Then at 1300 to 1500 DEG C, melting 2 hours, then water quenching, obtain block glaze；3) by block glaze through wet ball grinding
Afterwards, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/ml, glaze slip is imposed on billet surface, is dried to glaze slip
Moisture be less than 1% after, alternately fire at 1000 to 1100 DEG C and 1200 to 1250 DEG C 2 times respectively, each firing time is
20 to 30 minutes, after cooling, obtain mixing glaze；4) choose cdse, the cds of above-mentioned weight portion, make their mix homogeneously, then
They are entered ball milling 20h, obtains cadmium selenium glaze；5) by obtained mixing glaze in step 3) and step 4) and cadmium selenium glaze
Mix homogeneously, obtains bright red glaze.Described drying is to dry at 80 to 160 DEG C.Described melting is in box siliconits electricity
Carry out in resistance stove.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 1: take sio280 kg, al2o310 kg, pb3o460 kg, na2b4o720 kg, na2O 3 kg, k2o 4
Kg, zno 5 kg, b2o34 kg, make their mix homogeneously, obtain compound；Compound is crossed after 80 mesh sieves, at 900 to 1000 DEG C
Lower melting 1 to 1 .5 hour, then at 1300 to 1500 DEG C, melting 2 hours, then water quenching, obtain block glaze；By bulk
After wet ball grinding, remove impurity of sieving obtains glaze slip to glaze, and the concentration of glaze slip is 1 .5 to 1.8g/ml, and glaze slip is imposed on base substrate table
Face, after the moisture being dried to glaze slip is less than 1%, alternately fires 2 times respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C,
Firing time is 20 to 30 minutes every time, after cooling, obtains mixing glaze；Choose cdse10 kg, cds 10 kg, so that them is mixed
Close uniformly, then they are entered ball milling 20h, obtain cadmium selenium glaze；Obtained mixing glaze and cadmium selenium glaze are mixed all
Even, obtain bright red glaze.Described drying is to dry at 80 to 160 DEG C.Described melting is in box siliconits resistance furnace
Carry out.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 2: take sio2100 kg, al2o315 kg, pb3o480 kg, na2b4o730 kg, na2O 8 kg, k2o
8 kg, zno 8 kg, b2o310 kg, make their mix homogeneously, obtain compound；Compound is crossed after 80 mesh sieves, 900 to
Melting 1 to 1 .5 hour at 1000 DEG C, then at 1300 to 1500 DEG C, melting 2 hours, then water quenching, obtain block glaze；
By block glaze after wet ball grinding, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/ml, and glaze slip is imposed on
Billet surface, after the moisture being dried to glaze slip is less than 1%, alternately burns respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C
System 2 times, each firing time is 20 to 30 minutes, after cooling, obtains mixing glaze；Choose cdse15 kg, cds 15 kg, make
Then they entered ball milling 20h, obtain cadmium selenium glaze by their mix homogeneously；By obtained mixing glaze and cadmium selenium glaze
Mix homogeneously, obtains bright red glaze.Described drying is to dry at 80 to 160 DEG C.Described melting is in box siliconits electricity
Carry out in resistance stove.Described it is cooled to naturally cool to room temperature with stove.
Embodiment 3: take sio290 kg, al2o312 kg, pb3o475 kg, na2b4o725 kg, na2O 6 kg, k2o 5
Kg, zno 6 kg, b2o38 kg, make their mix homogeneously, obtain compound；Compound is crossed after 80 mesh sieves, at 900 to 1000 DEG C
Lower melting 1 to 1 .5 hour, then at 1300 to 1500 DEG C, melting 2 hours, then water quenching, obtain block glaze；By bulk
After wet ball grinding, remove impurity of sieving obtains glaze slip to glaze, and the concentration of glaze slip is 1 .5 to 1.8g/ml, and glaze slip is imposed on base substrate table
Face, after the moisture being dried to glaze slip is less than 1%, alternately fires 2 times respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C,
Firing time is 20 to 30 minutes every time, after cooling, obtains mixing glaze；Choose cdse12 kg, cds 12 kg, so that them is mixed
Close uniformly, then they are entered ball milling 20h, obtain cadmium selenium glaze；Obtained mixing glaze and cadmium selenium glaze are mixed all
Even, obtain bright red glaze.Described drying is to dry at 80 to 160 DEG C.Described melting is in box siliconits resistance furnace
Carry out.Described it is cooled to naturally cool to room temperature with stove.
Claims (6)
1. a kind of bright red glaze is it is characterised in that it is to be prepared from by the raw material of following parts by weight: sio280 to 100
Part, al2o310 to 15 parts, pb3o460 to 80 parts, na2b4o720 to 30 parts, na23 to 8 parts of o, k24 to 8 parts of o, zno 5 to 8
Part, b2o34 to 10 parts, 10 to 15 parts of 10 to 15 parts of cdse, cds.
2. bright red glaze according to claim 1 is it is characterised in that it is to be prepared from by the raw material of following parts by weight
: sio290 parts, al2o312 parts, pb3o475 parts, na2b4o725 parts, na26 parts of o, k26 parts of 5 parts of o, zno, b2o38 parts,
12 parts of 12 parts of cdse, cds.
3. a kind of preparation method of bright red glaze as claimed in claim 1 or 2 is it is characterised in that its preparation method is as follows:
1) choose the sio of above-mentioned weight portion2, al2o3, pb3o4, na2b4o7, na2O, k2O, zno, b2o3, mix homogeneously,
Obtain compound；
2) compound is crossed after 80 mesh sieves, melting 1 to 1 .5 hour at 900 to 1000 DEG C, then at 1300 to 1500 DEG C,
Melting 2 hours, then water quenching, obtain block glaze；
3) by block glaze after wet ball grinding, remove impurity of sieving obtains glaze slip, and the concentration of glaze slip is 1 .5 to 1.8g/ml, by glaze
Slurry imposes on billet surface, after the moisture being dried to glaze slip is less than 1%, respectively at 1000 to 1100 DEG C and 1200 to 1250 DEG C
Alternately fire 2 times, each firing time is 20 to 30 minutes, after cooling, obtain mixing glaze；
4) choose cdse, the cds of above-mentioned weight portion, make their mix homogeneously, then they are entered ball milling 20h, obtain cadmium selenium
Glaze；
5) by obtained mixing glaze in step 3) and step 4) and cadmium selenium glaze mix homogeneously, obtain bright red glaze.
4. rust red glaze according to claim 3 preparation method it is characterised in that described drying be 80 to
Dry at 160 DEG C.
5. the preparation method of rust red glaze according to claim 3 is it is characterised in that described melting is in box silicon
Carry out in kryptol stove.
6. the preparation method of rust red glaze according to claim 3 is it is characterised in that described being cooled to is natural with stove
It is cooled to room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610833801.5A CN106348599A (en) | 2016-09-20 | 2016-09-20 | Vermilion glaze and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610833801.5A CN106348599A (en) | 2016-09-20 | 2016-09-20 | Vermilion glaze and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106348599A true CN106348599A (en) | 2017-01-25 |
Family
ID=57858275
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610833801.5A Pending CN106348599A (en) | 2016-09-20 | 2016-09-20 | Vermilion glaze and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106348599A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108840566A (en) * | 2018-08-17 | 2018-11-20 | 湖南德兴瓷业有限公司 | Red glaze of low temperature and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101786795A (en) * | 2009-12-31 | 2010-07-28 | 深圳市永丰源实业有限公司 | Enamel glaze and preparation process thereof |
-
2016
- 2016-09-20 CN CN201610833801.5A patent/CN106348599A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101786795A (en) * | 2009-12-31 | 2010-07-28 | 深圳市永丰源实业有限公司 | Enamel glaze and preparation process thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108840566A (en) * | 2018-08-17 | 2018-11-20 | 湖南德兴瓷业有限公司 | Red glaze of low temperature and preparation method thereof |
| CN108840566B (en) * | 2018-08-17 | 2021-06-22 | 湖南德兴瓷业有限公司 | Low-temperature red glaze and preparation method thereof |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170125 |
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| WD01 | Invention patent application deemed withdrawn after publication |