CN108455853A - Your porcelain celeste glaze of one kind and preparation method thereof - Google Patents
Your porcelain celeste glaze of one kind and preparation method thereof Download PDFInfo
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- CN108455853A CN108455853A CN201810250468.4A CN201810250468A CN108455853A CN 108455853 A CN108455853 A CN 108455853A CN 201810250468 A CN201810250468 A CN 201810250468A CN 108455853 A CN108455853 A CN 108455853A
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- porcelain
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- Chemical Kinetics & Catalysis (AREA)
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- Organic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses your a kind of porcelain celeste glazes and preparation method thereof, include the component of following parts by weight：11~18 parts of Agate, 6~9 parts of Zijin soil, 35~45 parts of feldspar powder, 9~15 parts of silica flour, side's solution is 16~25 parts right, 3~8 parts of bone ash, 6~15 parts of wood ash, and 10~16 parts of local glaze soil makes 11~18 parts of this medicine by oneself.Eternal division of history into periods glaze colours of celeste glaze is solved, and solves agate and enters glaze, natural transmutation is in Celeste, glaze is for example reddish black, simple and tasteful, smooth exquisiteness, it is converted with light, bright not dazzling, smooth as jade uniqueness, if breast is like ice, cyan is simple and elegant, rich in water colour, the pure exquisiteness of glaze layer, color are green refined plain like emerald, matter U.S.A lies hidden and undeveloped, and gloss is soft, full glaze bind the feet of women branch is burnt, glaze table hacking is gathered, in fish scale, cicada's wings, crab claw, ice crack, sesame flower hacking original feature.
Description
Technical field
The present invention relates to ceramic technology fields, more particularly to your a kind of porcelain celeste glaze and preparation method thereof.
Background technology
Your porcelain is listed in first of five big porcelain (you, official, an ancient unit of weight, brother, fixed) Song Dynasty in China, made by imperial order at that time for imperial palace it is hired
Porcelain.Your china clay matter is fine and smooth, tire bone is hard, glaze colours is moist, and moulding is simple and unsophisticated generous, and glaze such as " the sun shines again after the rain cloud tear ", " thousand peaks are green
Wave kingfisher color comes ", it becomes clear without dazzling, has the characteristics that " pear skin, crab claw, sesame flower ", be known as " like beautiful non-jade winning by common people
It is beautiful ".Your porcelain starts from late period in the Northern Song Dynasty, because kiln site is gained the name at Ruzhou domestic (modern Henan Ruzhou, one band of Baofeng).Due to history original
Cause, prosperous front and back only 20 years of Ruyao, since the firing time is of short duration, spreads treasure so far, less than hundred, more foot is precious
It is expensive.
Traditional ceramic glaze is a kind of silicate, the glaze applied on ware generally with quartz, feldspar, be stained with as raw material,
After the modulation of ground plus water, it is coated on billet surface, is melted through the roasting of certain temperature, when the temperature drops, forming ceramic watch
The glassy thin layer in face.Ceramic glaze layer can increase mechanical strength, thermal stability, the dielectric strength of ware, prevent liquid, gas
Erosion；Simultaneously also add porcelain beauty, convenient for wash wipe, be not infected with by dust the effects that.
Wherein, why unique your enamel is, is to be burnt into because entering glaze with agate with " green such as day, face is such as beautiful, cicada's wings
Line, stars at dawn are dilute, and sesame support pin glaze meets " your porcelain.Agate enter the most important effect of glaze be make glaze gloss it is with nothing left in accumulate (be glaze
Interior air pocket refractive power reflection it is therefore) and glaze in deep and remote profound quiet cyan, therefore your porcelain has reddish black, pea green, pale blue based on celadon
Equal glaze colours.But eternal division of history into periods glaze colours of celeste glaze is current problem to be solved.
Invention content
The object of the present invention is to provide your a kind of porcelain celeste glazes, and thousand to solve celeste glaze in the prior art account for the division of history into periods
Glaze colours, and solve the problems, such as that agate enters glaze, natural transmutation is in Celeste；The present invention also aims to provide your a kind of porcelain day
The preparation method of green glaze.
To achieve the goals above, your a kind of technical solution of porcelain celeste glaze of the invention is：Your a kind of porcelain celeste glaze, packet
Component containing following parts by weight：11~18 parts of Agate, 6~9 parts of Zijin soil, 35~45 parts of feldspar powder, silica flour 9~15
Part, 16~25 parts of calcite, 3~8 parts of bone ash, 6~15 parts of wood ash, 10~16 parts of local glaze soil make 11~18 parts of this medicine by oneself.
A kind of technical solution of preparation method of your the porcelain celeste glaze of the present invention is：It is a kind of as described in claim 1 you
The preparation method of porcelain celeste glaze, comprises the steps of：
1) refining Agate, calcite respectively, eluriate, crushing is particle or powdery；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze, make processing in this medicine and step 1) by oneself
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85~0.90 times of glaze, Ball-milling Time
It is 20~60 hours, obtains glaze slip；
3) a concentration of 60~75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging place
Reason, obtains your porcelain celeste glaze；
4) by your the uniform glazing of porcelain celeste glaze stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, will fired first with oxidizing flame,
15~25 DEG C are increased when oxidizing flame is fired per 10min, recycle reduction flame firing temperature continuation at the uniform velocity risen to 1160~
1300 DEG C, 10~15 DEG C are increased per 10min when being fired with reduction flame, are then protected with reduction flame at 1160~1300 DEG C
Temperature finally stops firing, natural cooling, kiln discharge after 15~18 hours cooling times, obtains your porcelain with your porcelain celeste glaze.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
Burn, in sintering procedure, room temperature is at the uniform velocity warming up to 800 DEG C~1000 DEG C, then cooling, kiln discharge, then to the green body after biscuiting into
Row floating dust is removed, and moisturizing processing is then carried out.
When restoring flame firing and heat preservation firing described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 0.8~1%, carbon monoxide 3~5%.
It is quartzy main siliceous, the wearability of glaze, hardness, whiteness, transparency can be improved.
Feldspar has melting temperature relatively low, and the big melt temperature scope of high temperature viscosity is wider.
Calcite is mainly fluxing raw material, and other raw materials belong to supplement material.
Bone ash is cattle and sheep bone ash and pig bone ash.P elements are mainly contained, glaze jade-like stone can be made to moisten, content one of the bone ash in glaze
As be no more than 5 percent.Bone ash obtains after generally being burnt with sheep bone or ox bone, and pig bone is because of growth period is too short, after bone is burnt,
Lose more, general ten how many pig bones can be obtained one jin after burning, eight jin or so of sheep bone ox bone is one jin available.
Wood ash is based on chestnut ash and mountain weedtree.Potassium element is mainly contained, firing temperature can be reduced in glaze, also there is quality
Effect.Producing for wood ash is easier, and after baked wheaten cake, is removed the impurity such as the firewood to burn incompletely by very thin sieve, is prevented wood
The organic matters such as material are mixed into glaze slip, and at high temperature, combustion gas escapes out out of glaze and destroys glazed structure, and are burnt
Cavity can be also formed afterwards, become flaw.After filtering out impurity, it to be also poured into water stirring, ash pure above is taken after precipitation
Go out, what is precipitated down below is the impurity such as the soil carried secretly on branch, cannot be entered in glaze.
Agate, chemical composition are silica.Agate is used in your porcelain dispensing, can be improved the texture of glaze, be made glaze solid, no
It is apprehensive, it is touched with hand, there is a kind of greasy feeling, glaze jade-like stone profit to have beautiful feeling, and the glaze for being added without agate then seems dry
Dry, enamel is apprehensive, and glass sense is strong.
Make this medicine by oneself：Firing temperature is mainly reconciled to melt.Each constituent in glaze is due to place of production difference, each ingredient
The constituent content of therein also can slightly difference, at this point, make this medicine by oneself by allotment, it is final so that each element in glaze at
Divide and meets the requirements.That is, make by oneself this medicine for element ratio contained by each constituent for allocating in glaze with meet glaze at
Divide and requires.
It is using the advantageous effects of the invention generated：Present invention mainly solves eternal division of history into periods glaze colours of celeste glaze, and
It solving agate and enters glaze, natural transmutation is in Celeste, and glaze is for example reddish black, simple and tasteful, and smooth exquisiteness is converted with light, bright not dazzling,
Like ice, cyan is simple and elegant for smooth as jade uniqueness, such as breast, and rich in water colour, the pure exquisiteness of glaze layer, color is like emerald, and green refined plain, matter U.S.A lies hidden and undeveloped,
Gloss is soft, full glaze bind the feet of women branch is burnt, glaze table hacking is gathered, in fish scale, cicada's wings, crab claw, ice crack, sesame flower hacking original spy
Sign.
Specific implementation mode
With reference to embodiment, further detailed description is done to the present invention.
Embodiment 1：
Your a kind of porcelain celeste glaze, includes the component of following parts by weight：11 parts of Agate, 6 parts of Zijin soil, feldspar powder 35
Part, 9 parts of silica flour, 16~25 parts of calcite, 3 parts of bone ash, 6 parts of wood ash, local 10 parts of glaze soil (are derived from Henan Baofeng glaze
Soil), make 11 parts of this medicine by oneself.
The preparation method of your porcelain celeste glaze, comprises the steps of：
1) refining Agate, calcite respectively, eluriate, crushing is particle or powdery；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze soil, make processing in this medicine and step 1) by oneself
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85 times of glaze, and Ball-milling Time is 20 small
When, obtain glaze slip；
3) a concentration of 60 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To your porcelain celeste glaze；
4) by your the uniform glazing of porcelain celeste glaze stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, will fired first with oxidizing flame,
15 DEG C are increased when oxidizing flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1160 DEG C, with also
10 DEG C are increased when former flame is fired per 10min, is then fired with reduction flame heat preservation at 1160 DEG C, soaking time is according to specific
Situation determines (such as material difference used of getting fire), finally stops firing, natural cooling, kiln discharge after 15 hours cooling times obtains
Your porcelain with your porcelain celeste glaze.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
It burns, in sintering procedure, room temperature is at the uniform velocity warming up to 800 DEG C, then cooling, kiln discharge, then clear to the green body progress floating dust after biscuiting
It removes, then carries out moisturizing processing.
When restoring flame firing and heat preservation firing described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 0.8%, carbon monoxide 3%.
Embodiment 2：
Your a kind of porcelain celeste glaze, includes the composition of following parts by weight：18 parts of Agate, 9 parts of Zijin soil, feldspar powder 45
Part, 15 parts of silica flour, 25 parts of calcite, 8 parts of bone ash, 15 parts of wood ash, local 16 parts of glaze soil (being derived from Henan Baofeng glaze soil),
Make 18 parts of this medicine by oneself.
The preparation method of your porcelain celeste glaze, comprises the steps of：
1) refining Agate, calcite respectively, eluriate, crushing is particle or powdery；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze soil, make processing in this medicine and step 1) by oneself
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.90 times of glaze, and Ball-milling Time is 60 small
When, obtain glaze slip；
3) a concentration of 75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To your porcelain celeste glaze；
4) by your the uniform glazing of porcelain celeste glaze stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, will fired first with oxidizing flame,
25 DEG C are increased when oxidizing flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1300 DEG C, with also
15 DEG C are increased when former flame is fired per 10min, then with reduction flame heat preservation at 1300 DEG C, soaking time is as the case may be
It determines (such as material difference used of getting fire), finally stops firing, natural cooling, kiln discharge after 18 hours cooling times is had
Your porcelain of your porcelain celeste glaze.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
It burns, in sintering procedure, room temperature is at the uniform velocity warming up to 1000 DEG C, then cooling, kiln discharge, then clear to the green body progress floating dust after biscuiting
It removes, then carries out moisturizing processing.
When restoring flame firing and heat preservation firing described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 1%, carbon monoxide 5%.
Claims (4)
1. your a kind of porcelain celeste glaze, which is characterized in that include the component of following parts by weight：11~18 parts of Agate, Zijin soil 6
~9 parts, 35~45 parts of feldspar powder, 9~15 parts of silica flour, 16~25 parts of calcite, 3~8 parts of bone ash, 6~15 parts of wood ash, locally
10~16 parts of glaze soil makes 11~18 parts of this medicine by oneself.
2. a kind of preparation method of your porcelain celeste glaze as described in claim 1, which is characterized in that comprise the steps of：
1) refining Agate, calcite respectively, eluriate, crushing is particle or powdery；
2) by Zijin soil, feldspar powder, silica flour, bone ash, art ash, local glaze soil, make in this medicine and step 1) that treated by oneself
Each building stones proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85~0.90 times of glaze, Ball-milling Time 20
~60 hours, obtain glaze slip；
3) a concentration of 60~75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To your porcelain celeste glaze；
4) by your the uniform glazing of porcelain celeste glaze stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, fired first with oxidizing flame, oxidizing fire
15~25 DEG C are increased when flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1160~1300 DEG C,
10~15 DEG C are increased per 10min when being fired with reduction flame, are then finally stopped with reduction flame heat preservation at 1160~1300 DEG C
It only fires, natural cooling, kiln discharge after 15~18 hours cooling times, obtains your porcelain with your porcelain celeste glaze.
3. the preparation method of your porcelain celeste glaze according to claim 2, which is characterized in that right before glazing in step 4)
Green body is pre-processed, and processing method is：Biscuiting is carried out to molding green body first, in sintering procedure, room temperature at the uniform velocity heats up
To 800 DEG C~1000 DEG C, then cooling, kiln discharge, then floating dust removing is carried out to the green body after biscuiting, then carry out moisturizing processing.
4. the preparation method of your porcelain celeste glaze according to claim 2, which is characterized in that restore fire described in step 5)
When flame is fired and heat preservation is fired, the gas atmosphere in kiln includes the oxygen 0.8~1% of weight percent, and carbon monoxide 3~
5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810250468.4A CN108455853A (en) | 2018-03-16 | 2018-03-16 | Your porcelain celeste glaze of one kind and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810250468.4A CN108455853A (en) | 2018-03-16 | 2018-03-16 | Your porcelain celeste glaze of one kind and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020213A (en) * | 2018-09-21 | 2018-12-18 | 王晟鸣 | A kind of your porcelain sky blue glaze and preparation method thereof, your porcelain |
| CN109400211A (en) * | 2018-12-13 | 2019-03-01 | 禹州市神后镇永春瓷业有限公司 | A kind of celeste glaze and preparation method thereof |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
| CN112608030A (en) * | 2020-12-23 | 2021-04-06 | 湖州钧远木业有限公司 | Reqing glaze for ceramic ornaments and preparation method thereof |
| CN112939464A (en) * | 2021-04-29 | 2021-06-11 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN114133140A (en) * | 2021-12-14 | 2022-03-04 | 德化县艺欣陶瓷工艺有限公司 | Ru-kiln sky-blue glaze and preparation process thereof |
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| CN105293913A (en) * | 2015-09-07 | 2016-02-03 | 龙泉市金宏瓷业有限公司 | Celadon glaze and manufacturing method thereof |
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| CN105293913A (en) * | 2015-09-07 | 2016-02-03 | 龙泉市金宏瓷业有限公司 | Celadon glaze and manufacturing method thereof |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020213A (en) * | 2018-09-21 | 2018-12-18 | 王晟鸣 | A kind of your porcelain sky blue glaze and preparation method thereof, your porcelain |
| CN109020213B (en) * | 2018-09-21 | 2021-08-20 | 王晟鸣 | Ru porcelain sky blue glaze and preparation method thereof, and Ru porcelain |
| CN109400211A (en) * | 2018-12-13 | 2019-03-01 | 禹州市神后镇永春瓷业有限公司 | A kind of celeste glaze and preparation method thereof |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
| CN112608030A (en) * | 2020-12-23 | 2021-04-06 | 湖州钧远木业有限公司 | Reqing glaze for ceramic ornaments and preparation method thereof |
| CN112939464A (en) * | 2021-04-29 | 2021-06-11 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN112939464B (en) * | 2021-04-29 | 2022-06-10 | 张玉凤 | Ru porcelain light azure glaze and preparation method thereof |
| CN114133140A (en) * | 2021-12-14 | 2022-03-04 | 德化县艺欣陶瓷工艺有限公司 | Ru-kiln sky-blue glaze and preparation process thereof |
| CN114133140B (en) * | 2021-12-14 | 2023-09-08 | 德化县艺欣陶瓷工艺有限公司 | Ru-kiln sky-blue glaze and preparation process thereof |
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