CN108191236A - Pea green glaze of your a kind of porcelain and preparation method thereof - Google Patents
Pea green glaze of your a kind of porcelain and preparation method thereof Download PDFInfo
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- CN108191236A CN108191236A CN201810250467.XA CN201810250467A CN108191236A CN 108191236 A CN108191236 A CN 108191236A CN 201810250467 A CN201810250467 A CN 201810250467A CN 108191236 A CN108191236 A CN 108191236A
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- glaze
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- pea green
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
Abstract
The invention discloses pea green glaze of your a kind of porcelain and preparation method thereof, include the component of following parts by weight：13~19 parts of Agate, 7~10 parts of Zijin soil, 35~45 parts of feldspar powder, 8~12 parts of silica flour, 1.6~2.5 parts of bone ash, 10~15 parts of wood ash, 16~19 parts of calcite, 5~9 parts of bloodstone, 7~10 parts of spot fossil, local 10~15 parts of glaze soil, makes 14~19 parts of this medicine by oneself.It present invention mainly solves eternal division of history into periods glaze colours of the pea green glaze of your porcelain, and solves agate and enters glaze, natural transmutation is in pea green, glaze is for example pea green, simple and tasteful, smooth exquisiteness, it is converted with light, smooth as jade uniqueness, such as breast is like ice, cyan is simple and elegant, rich in water colour, the pure exquisiteness of glaze layer, color is like emerald, and green refined plain, matter U.S.A lies hidden and undeveloped, gloss is soft, glaze table hacking gathers, in fish scale, cicada's wings, crab claw, ice crack, sesame flower hacking original feature.
Description
Technical field
The present invention relates to ceramic technology fields more particularly to a kind of pea green glaze of your porcelain and preparation method thereof.
Background technology
Your porcelain is listed in first of five big porcelain (you, official, an ancient unit of weight, brother, fixed) Song Dynasty in China, is made by imperial order at that time hired for imperial palace
Porcelain.Your china clay matter is fine and smooth, tire bone is hard, glaze colours is moistened, and moulding is simple and unsophisticated generous, and glaze such as " the sun shines again after the rain cloud tear ", " thousand peaks are green
Wave kingfisher color comes ", it becomes clear without dazzling, there is " pear skin, crab claw, sesame flower ", be known as " like beautiful non-jade winning by common people
It is beautiful ".Your porcelain starts from late period in the Northern Song Dynasty, gains the name due to kiln site is at Ruzhou domestic (modern Henan Ruzhou, one band of Baofeng).Due to history original
Cause, prosperous front and rear only 20 years of Ruyao, since the firing time is of short duration, spreads treasure so far, less than hundred, more foot is precious
It is expensive.
Traditional ceramic glaze is a kind of silicate, the glaze applied on ware generally with quartz, feldspar, be stained with as raw material,
It after the modulation of ground plus water, coated on billet surface, is melted through the roasting of certain temperature, when the temperature drops, forming ceramic watch
The glassy thin layer in face.Ceramic glaze layer can increase mechanical strength, thermal stability, the dielectric strength of ware, prevent liquid, gas
Erosion；Simultaneously also add porcelain beauty, convenient for wash wipe, be not infected on dirt the effects that.
Wherein, why unique your enamel is, is because entering glaze with agate, has been burnt into " green such as day, face is as beautiful, cicada's wings
Line, stars at dawn are dilute, and sesame support pin glaze meets " your porcelain.Agate enter the most important effect of glaze be make glaze paint gloss it is with nothing left in accumulate (be glaze
Interior air pocket refractive power reflection it is therefore) and glaze in deep and remote profound quiet cyan, therefore your porcelain has pea green, pea green, pale blue based on celadon
Wait glaze colours.But eternal division of history into periods glaze colours of pea green glaze is current problem to be solved.
Invention content
The object of the present invention is to provide a kind of pea green glaze of your porcelain, to solve eternal division of history into periods of pea green glaze of the prior art
Glaze colours, and solve the problems, such as that agate enters glaze, natural transmutation is in pea green；The present invention also aims to provide your a kind of porcelain beans
The preparation method of green glaze.
To achieve these goals, a kind of technical solution of pea green glaze of your porcelain of the invention is：A kind of pea green glaze of your porcelain, packet
Component containing following parts by weight：13~19 parts of Agate, 7~10 parts of Zijin soil, 35~45 parts of feldspar powder, silica flour 8~12
Part, 1.6~2.5 parts of bone ash, 10~15 parts of wood ash, 16~19 parts of calcite, 5~9 parts of bloodstone, 7~10 parts of spot fossil, locally
10~15 parts of glaze soil makes 14~19 parts of this medicine by oneself.
A kind of technical solution of preparation method of pea green glaze of your porcelain of the present invention is：It is a kind of as described in claim 1 you
The preparation method of the pea green glaze of porcelain, comprises the steps of：
1) it is particle or powdery to refine, eluriate, crush Agate, calcite, bloodstone, spot fossil respectively；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze soil, make by oneself in this medicine and step 1) and handle
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85~0.90 times of glaze, Ball-milling Time
It is 20~60 hours, obtains glaze slip；
3) a concentration of 60~75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging place
Reason, obtains the pea green glaze of your porcelain；
4) by the uniform glazing of the pea green glaze of your porcelain stirred evenly on green body；
5) green body of glazing is placed in kiln and be fired, in sintering procedure, fired first with oxidizing flame, oxygen
Change when flame is fired and 15~25 DEG C increased per 10min, recycle reduction flame firing temperature continuation at the uniform velocity risen to 1160~
1300 DEG C, 10~15 DEG C are increased per 10min when being fired with reduction flame, is then protected at 1160~1300 DEG C with reduction flame
Temperature finally stops firing, and natural cooling, kiln discharge after 15~18 hours cooling times obtains your porcelain with the pea green glaze of your porcelain.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
Burn, in sintering procedure, room temperature is at the uniform velocity warming up to 800 DEG C~1000 DEG C, then cooling, kiln discharge, then to the green body after biscuiting into
Row floating dust is removed, and then carries out moisturizing processing.
When flame firing and heat preservation firing are restored described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 0.8~1%, carbon monoxide 3~5%.
It is quartzy main siliceous, the wearability of glaze paint, hardness, whiteness, transparency can be improved.
Feldspar is relatively low with melting temperature, and the big melt temperature scope of high temperature viscosity is wider.
Calcite is mainly fluxing raw material, and other raw materials belong to supplement material.
Bone ash is cattle and sheep bone ash and pig bone ash.P elements are mainly contained, can moisten glaze paint jade-like stone, content one of the bone ash in glaze
As be no more than 5 percent.Bone ash obtains after generally being burnt with sheep bone or ox bone, and pig bone is because of growth period is too short, after bone is burnt,
Lose more, general ten how many pig bones can obtain one jin after burning, eight jin or so of sheep bone ox bone is one jin available.
Wood ash is based on chestnut ash and mountain weedtree.Potassium element is mainly contained, firing temperature can be reduced in glaze, also there is quality
Effect.Producing for wood ash is easier, and after baked wheaten cake, is removed the impurity such as the firewood to burn incompletely by very thin sieve, is prevented wood
The organic matters such as material are mixed into glaze slip, and at high temperature, combustion gas escapes out out of glaze and destroys glazed structure, and are burnt
Cavity can be also formed afterwards, become flaw.After filtering out impurity, stirring is also poured into water, ash pure above is taken after precipitation
Go out, what is precipitated down below is the impurity such as the soil carried secretly on branch, it is impossible into glaze.
Agate, chemical composition are silica.With agate in your porcelain dispensing, the texture of glaze can be improved, make glaze solid, no
It is apprehensive, it is touched with hand, there is a kind of greasy feeling, glaze paint jade-like stone profit has beautiful feeling, and the glaze paint for being added without agate then seems dry
Dry, enamel is apprehensive, and glass sense is strong.
Make this medicine by oneself：Firing temperature is mainly reconciled to melt.Each constituent in glaze is due to place of production difference, each ingredient
The constituent content of therein also can slightly difference, at this point, make this medicine by oneself by allotment, it is final so that each element in glaze into
Divide and meet the requirements.That is, make by oneself this medicine for element ratio contained by each constituent for allocating in glaze with meet glaze into
Divide requirement.
It is using the advantageous effects of the invention generated：Present invention mainly solves eternal division of history into periods glaze of the pea green glaze of your porcelain
Color, and solve agate and enter glaze, natural transmutation is in pea green, and glaze is for example pea green, simple and tasteful, and smooth exquisiteness is converted with light, smooth as jade
Uniqueness, such as breast are like ice, and cyan is simple and elegant, and rich in water colour, the pure exquisiteness of glaze layer, color is like emerald, and green refined plain, matter U.S.A lies hidden and undeveloped, gloss
It is soft, glaze table hacking gathers, in fish scale, cicada's wings, crab claw, ice crack, sesame flower hacking original feature.
Specific embodiment
With reference to embodiment, further detailed description is done to the present invention.
Embodiment 1：
A kind of pea green glaze of your porcelain includes the component of following parts by weight：13 parts of Agate, 7 parts of Zijin soil, feldspar powder 35
Part, 8 parts of silica flour, 1.6 parts of bone ash, 10 parts of wood ash, 16 parts of calcite, 5 parts of bloodstone, 7 parts of spot fossil, local 10 parts of glaze soil
(Henan Baofeng glaze soil), makes 14 parts of this medicine by oneself.
The preparation method of the pea green glaze of your porcelain, comprises the steps of：
1) it is particle or powdery to refine, eluriate, crush Agate, calcite, bloodstone, spot fossil respectively；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze soil, make by oneself in this medicine and step 1) and handle
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85 times of glaze, and Ball-milling Time is small for 20
When, obtain glaze slip；
3) a concentration of 60 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To the pea green glaze of your porcelain；
4) by the uniform glazing of the pea green glaze of your porcelain stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, will fired first with oxidizing flame,
15 DEG C are increased when oxidizing flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1160 DEG C, with also
10 DEG C are increased when former flame is fired per 10min, is then fired at 1160 DEG C with reduction flame heat preservation, soaking time is according to specific
Situation determines (such as material difference used of getting fire), finally stops firing, natural cooling, kiln discharge after 15 hours cooling times obtains
Your porcelain with the pea green glaze of your porcelain.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
It burns, in sintering procedure, room temperature is at the uniform velocity warming up to 800 DEG C, then cooling, kiln discharge, then clear to the green body progress floating dust after biscuiting
It removes, then carries out moisturizing processing.
When flame firing and heat preservation firing are restored described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 0.8%, carbon monoxide 3%.
Embodiment 2：
A kind of pea green glaze of your porcelain includes the component of following parts by weight：19 parts of Agate, 10 parts of Zijin soil, feldspar powder 45
Part, 12 parts of silica flour, 2.5 parts of bone ash, 15 parts of wood ash, 19 parts of calcite, 9 parts of bloodstone, 10 parts of spot fossil, local 15 parts of glaze soil
(Henan Baofeng glaze soil), makes 19 parts of this medicine by oneself.
The preparation method of the pea green glaze of your porcelain, comprises the steps of：
1) it is particle or powdery to refine, eluriate, crush Agate, calcite, bloodstone, spot fossil respectively；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, local glaze soil, make by oneself in this medicine and step 1) and handle
Each building stones afterwards proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.90 times of glaze, and Ball-milling Time is small for 60
When, it obtains to glaze slip；
3) a concentration of 75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To the pea green glaze of your porcelain；
4) by the uniform glazing of the pea green glaze of your porcelain stirred evenly on green body；
5) green body of glazing is placed in kiln and is fired, in sintering procedure, will fired first with oxidizing flame,
25 DEG C are increased when oxidizing flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1300 DEG C, with also
15 DEG C are increased when former flame is fired per 10min, is then kept the temperature at 1300 DEG C with reduction flame, soaking time is as the case may be
It determines (such as material difference used of getting fire), finally stops firing, natural cooling, kiln discharge after 18 hours cooling times is had
Your porcelain of the pea green glaze of your porcelain.
Green body is pre-processed before glazing in step 4), processing method is：Element is carried out to molding green body first
It burns, in sintering procedure, room temperature is at the uniform velocity warming up to 1000 DEG C, then cooling, kiln discharge, then clear to the green body progress floating dust after biscuiting
It removes, then carries out moisturizing processing.
When flame firing and heat preservation firing are restored described in step 5), the gas atmosphere in kiln includes weight percent
Oxygen 1%, carbon monoxide 5%.
Claims (4)
1. a kind of pea green glaze of your porcelain, it is characterised in that：Include the component of following parts by weight：13~19 parts of Agate, Zijin soil 7
~10 parts, 35~45 parts of feldspar powder, 8~12 parts of silica flour, 1.6~2.5 parts of bone ash, 10~15 parts of wood ash, calcite 16~19
Part, 5~9 parts of bloodstone, 7~10 parts of spot fossil, local 10~15 parts of glaze soil make 14~19 parts of this medicine by oneself.
2. a kind of preparation method of the pea green glaze of your porcelain as described in claim 1, it is characterised in that：It comprises the steps of：
1) it is particle or powdery to refine, eluriate, crush Agate, calcite, bloodstone, spot fossil respectively；
2) by Zijin soil, feldspar powder, silica flour, bone ash, wood ash, on local glaze, make in this medicine and step 1) that treated by oneself
Each building stones proportionally uniformly mix, and add water carry out ball milling, and amount of water is 0.85~0.90 times of glaze, Ball-milling Time 20
~60 hours, obtain glaze slip；
3) a concentration of 60~75 Baume degrees of glaze slip is adjusted, then by the glaze slip after adjusting successively by except iron, aging processing, obtaining
To the pea green glaze of your porcelain；
4) by the uniform glazing of the pea green glaze of your porcelain stirred evenly on green body；
5) green body of glazing is placed in kiln and be fired, in sintering procedure, fired first with oxidizing flame, oxidizing fire
15~25 DEG C are increased when flame is fired per 10min, recycles reduction flame that firing temperature continuation is at the uniform velocity risen to 1160~1300 DEG C,
10~15 DEG C are increased per 10min when being fired with reduction flame, is then kept the temperature with reduction flame at 1160~1300 DEG C, finally stopped
It only fires, natural cooling, kiln discharge after 15~18 hours cooling times, obtains your porcelain with the pea green glaze of your porcelain.
3. the preparation method of the pea green glaze of your porcelain according to claim 2, it is characterised in that：It is right before glazing in step 4)
Green body is pre-processed, and processing method is：Biscuiting is carried out to molding green body first, in sintering procedure, room temperature at the uniform velocity heats up
To 800 DEG C~1000 DEG C, then then cooling, kiln discharge, then carry out floating dust removing to the green body after biscuiting carry out moisturizing processing.
4. the preparation method of the pea green glaze of your porcelain according to claim 2, it is characterised in that：Fire is restored described in step 5)
When flame is fired and heat preservation is fired, the gas atmosphere in kiln includes the oxygen 0.8~1% of weight percent, and carbon monoxide 3~
5%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810250467.XA CN108191236A (en) | 2018-03-16 | 2018-03-16 | Pea green glaze of your a kind of porcelain and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810250467.XA CN108191236A (en) | 2018-03-16 | 2018-03-16 | Pea green glaze of your a kind of porcelain and preparation method thereof |
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| CN108191236A true CN108191236A (en) | 2018-06-22 |
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| CN201810250467.XA Pending CN108191236A (en) | 2018-03-16 | 2018-03-16 | Pea green glaze of your a kind of porcelain and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108483918A (en) * | 2018-06-19 | 2018-09-04 | 刘冬青 | Pseudo-classic glaze of your a kind of porcelain and preparation method thereof |
| CN109437565A (en) * | 2018-12-19 | 2019-03-08 | 禹州市正玉钧窑有限公司 | A kind of radix curcumae glaze |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
Citations (1)
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| CN105293913A (en) * | 2015-09-07 | 2016-02-03 | 龙泉市金宏瓷业有限公司 | Celadon glaze and manufacturing method thereof |
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2018
- 2018-03-16 CN CN201810250467.XA patent/CN108191236A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105293913A (en) * | 2015-09-07 | 2016-02-03 | 龙泉市金宏瓷业有限公司 | Celadon glaze and manufacturing method thereof |
Non-Patent Citations (3)
| Title |
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| 布莱恩•泰勒 凯特•杜迪: "《釉料及陶瓷颜色配制手册》", 31 October 2015, 上海科学技术出版社 * |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108483918A (en) * | 2018-06-19 | 2018-09-04 | 刘冬青 | Pseudo-classic glaze of your a kind of porcelain and preparation method thereof |
| CN109437565A (en) * | 2018-12-19 | 2019-03-08 | 禹州市正玉钧窑有限公司 | A kind of radix curcumae glaze |
| CN109437565B (en) * | 2018-12-19 | 2021-10-01 | 禹州市正玉钧窑有限公司 | Jade and gold glaze |
| CN110668843A (en) * | 2019-11-15 | 2020-01-10 | 汝州市宣和坊汝瓷有限公司 | Ru jade glaze and preparation method thereof |
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Application publication date: 20180622 |