CN107540225A - A kind of green glaze modelled after an antique - Google Patents
A kind of green glaze modelled after an antique Download PDFInfo
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- CN107540225A CN107540225A CN201710948790.XA CN201710948790A CN107540225A CN 107540225 A CN107540225 A CN 107540225A CN 201710948790 A CN201710948790 A CN 201710948790A CN 107540225 A CN107540225 A CN 107540225A
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Abstract
The invention provides a kind of green glaze modelled after an antique, it is prepared by the raw material of following parts by weight：9 15 parts of this medicine, 10 16 parts of quartz, 10 14 parts of calcite, 46 parts of lime stone, 37 43 parts of melilite, 0.5 1.5 parts of block tin, 2.5 3.5 parts of Copper Ores, 7 13 parts of wood ash, 3.5 4.5 parts of bone ash.The present invention is compared with prior art, any chemical substance is not added with formula, color development is carried out using a variety of chromonic materials contained in ore, make color development more natural, and pass through scientific and reasonable raw material proportioning and control burning process, the green glaze jade texture and opaque modelled after an antique prepared are strong, high yield rate, up to more than 95%.
Description
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of green glaze modelled after an antique.
Background technology
Pottery is using glaze thickness as this, and in its color or heavy glaze bottom or outstanding glaze or floating glaze table, glaze layer opalescence jade-like stone moisten, be administrations with multiplied departments
Work is intended to drip, and third dimension is extremely strong.Pottery is using transmutation as god, and where natural transmutation is the elite of pottery art, and pottery relies and raise
The name four seas, the rare part for porcelain woods of making a name.With a kind of glaze is applied in firing, once burning till, " it is of the same colour to enter kiln in multicoloured, goes out
Kiln ten thousand is color ".Protean transmutation effect, forms the infinite mystery of colors changing hue, bonus is thoroughly purple, it is purple in it is dark blue, blue or green in reside
In vain, it is general red in white, multicolored imbibition, form a brightening, and have the title of " pottery without right, transmutation is unparalleled ".
The key of pottery is enamel, and transmutation color of the enamel after being fired determines the value of pottery, white
Pottery has bluish white, grey dawn, creamy white, beautiful white etc., and blue pottery has sky blue, acid blue, powder blue, sapphire blue, peacock blue.And Henan
An ancient unit of weight kiln of Yuzhou is northern celadon kiln system, is typically fired using bavin, coal, charcoal and natural gas, glaze caused by different burning process
Color change is also different.And the formula of glaze also influences an important factor for pottery finished product exogenic color, while it is also to cause pottery
Enter that kiln is of the same colour, the color key factor of kiln discharge ten thousand.At present, green glaze glaze colours modelled after an antique jade-like stone profit, the glossiness burnt out is good, but jade matter
Feel poor, color development is unnatural, and yield rate is low.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of color development nature, jade texture and opaque
By force, the green glaze modelled after an antique of high yield rate.
To achieve these goals, the technical solution adopted by the present invention is as follows：
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：This medicine 9-15 parts, quartzy 10-16 parts, calcite 10-
14 parts, lime stone 4-6 parts, melilite 37-43 parts, block tin 0.5-1.5 parts, Copper Ores 2.5-3.5 parts, wood ash 7-13 parts, bone ash
3.5-4.5 part.
Above-mentioned green glaze modelled after an antique, wherein, it is prepared by the raw material of following parts by weight：12 parts of this medicine, quartz 13 parts,
12 parts of calcite, 5 parts of lime stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.
The preparation method of above-mentioned green glaze modelled after an antique, comprises the following steps：
（1）The preparation of glaze slip；
（2）Glazing；
（3）Burn till, 1260-1280 DEG C of firing temperature.
The preparation method of above-mentioned green glaze modelled after an antique, it is characterised in that step（3）In firing process specifically include following step
Suddenly：1. the oxidizing flame stage：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, temperature is ramped up in 3-5h
920-980℃；2. the strong reducing flame stage：Under strongly reducing atmosphere, temperature is set to be ramped up 1120-1180 DEG C in 5-7h；It is 3. weak
The reducing flame stage：Under weakly reducing atmosphere, temperature is set to be ramped up 1260-1280 DEG C in 3.5-4.5h；4. cooling stage：It is natural
Room temperature is cooled to, is made.
The present invention is advantageous in that：
1st, in the present invention, scientific and reasonable allotment melilite, quartz, calcite, lime stone, this medicine, bone ash, wood ash are passed through
Content, and then to control the content of potassium, sodium, calcium, silicon, the shortcomings of glaze paint prepared is without sliver, smoking, sagging.
2nd, the sintering procedure of the green glaze modelled after an antique in the present invention is divided into four-stage：First stage uses oxidizing flame by kiln
Temperature rises to 920-980 DEG C, in the process, the discharge such as organic matter in moisture and glaze in saggar, base substrate and kiln, glaze layer
Start to melt, glaze surface is in unsintered fine granularity, ferrous iron quilt contained in component Copper Ores, this medicine and melilite in glaze
It is oxidized to ferric iron；Kiln in-furnace temperature is risen to 1120-1180 DEG C by second stage using strong reduction flame by 920-980 DEG C,
During this, the raw ore thing in glaze is gradually decomposed and recrystallized, and gradually closure, formation are rough by porous for glaze paint
State, when the temperature of kiln reaches 1120-1180 DEG C, ferric iron starts to be reduced to ferrous iron to turn into ferrous silicon salt in glaze,
In conjunction with the color development of copper ion in Copper Ores, glaze starts to show green；Phase III will be warm in kiln using weak reduction flame
Degree by 1120-1180 DEG C rises to 1260-1280 DEG C, in the process, as temperature raises, glaze layer be fused into thick liquid and by
Upper and lower flowing, the melting of glaze layer make glaze paint flatten, and glaze layer forms vitreous, and can enter ferric reduction reaction
Row is thorough, ensure that the stability of green, and fourth stage is down to room temperature using Temperature fall mode, made to stop burning temperature-fall period
Glaze has a good Crystallization Process, ensure that the stability of green.
3rd, the raw material used in the present invention is mineral matter, is not added with any chemical substance, makes green color development more natural.
4th, the introducing of bone ash and wood ash even more makes the glaze jade texture prepared and opaque strong.
The present invention is not added with any chemical substance compared with prior art, in formula, utilizes a variety of hairs contained in ore
Color substance carries out color development, makes color development more natural, and by scientific and reasonable raw material proportioning and control burning process, prepares
Green glaze jade texture and opaque modelled after an antique are strong, high yield rate, up to more than 95%.
Embodiment
Embodiment 1
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：This medicine 9-15 parts, quartzy 10-16 parts, calcite 10-
14 parts, lime stone 4-6 parts, melilite 37-43 parts, block tin 0.5-1.5 parts, Copper Ores 2.5-3.5 parts, wood ash 7-13 parts, bone ash
3.5-4.5 part.
The preparation method of above-mentioned green glaze modelled after an antique, comprises the following steps：
（1）The preparation of glaze slip：Above-mentioned raw materials are added into appropriate water to mix, ball milling, obtain the glaze slip that mass concentration is 55-57%；
（2）Glazing：Base substrate is immersed into step（1）In take out for a moment in obtained glaze slip, be again dipped into a moment, take out, utilize base
The water imbibition of body, makes glaze slip uniformly be attached to billet surface；
（3）Burn till, 1260-1280 DEG C of firing temperature；
Firing process specifically comprises the following steps：
1. the oxidizing flame stage：Base substrate after glazing is put into kiln after being fitted into saggar, controls the chimney casket plate of ventilation to open, kiln top
Skylight opens, and makes to be under oxidizing atmosphere in kiln, and make kiln temperature be ramped up 920-980 DEG C in 3-5h from room temperature；
2. the strong reducing flame stage：After kiln temperature rises to 920-980 DEG C, closing skylight, the closing or semi-open of flue casket door,
Make to be under strongly reducing atmosphere in kiln, temperature is ramped up 1120-1180 DEG C in 5-7h；
3. the weak reducing flame stage：After kiln temperature rises to 1120-1180 DEG C, under weakly reducing atmosphere, make temperature in 3.5-
4.5h is ramped up 1260-1280 DEG C；
4. cooling stage：After kiln temperature rises to 1260-1280 DEG C, wicket is opened, substantial amounts of oxygen enters in kiln, is in kiln
Oxidizing atmosphere, oxygen is aoxidized to glaze paint, cooling, and glaze colours is formed, and is made.
Using melilite, quartz, calcite, lime stone, this medicine as main component in the present invention, wherein, contain in melilite
Potassium, sodium, there is cosolvent effect, firing time can be shortened, increase the light transmittance of pottery, improve the knot between base substrate and glaze layer
With joint efforts；The predominant amount of quartz is silica, it is possible to increase the melting temperature and viscosity of glaze, reduces the coefficient of expansion of glaze, carries
Mechanical strength, hardness, wearability and the chemical resistance of high glaze, and quartz can be by more lyotrope CaO, Na2O、
K2O, MgO meltings generation transparence quartz glass, make glaze paint bright, improve the glossiness of pottery；Calcite is also known as calcium stone, main
If play the effect of solvent, by increasing capacitance it is possible to increase hardness, abrasion resistance and the corrosion resistance of glaze, reduce the melting temperature of glaze, increase
The glossiness and transparency of glaze colours, the cracking of preventing and treating glaze paint and accumulation；Lime stone main component is CaCO3, it is a kind of solvent, can
The melting temperature and high temperature viscosity of glaze are reduced, promotes the production of body-glaze intermediate layer, is relaxed between base glaze because expansion coefficient difference draws
The stress risen, increases the elasticity, glossiness and transparency of glaze, prevents glaze paint cracking, bald glaze, massed glaze；This medicine is Yuzhou
A kind of natural feldspar, its main component are SiO2, also containing a small amount of Fe elements；In block tin in addition to containing Sn elements, also contain
There are a small amount of Pb elements, Sn elements are a kind of opacifiers and assistant toner, a kind of Pb elements also assistant toner, can make green
Color development is greener；Copper Ores are main colouring agents, are typically made up of, burn till under reducing atmosphere, Fe tri- kinds of elements of Cu, Fe, S2+、
Fe3+、Cu+、Cu2+It is main colour generation ion；Bone ash mainly contains calcium phosphate, is a kind of cosolvent, can reduce the molten of chun glaze
Melt temperature and the coefficient of expansion, increase the opaque of chun glaze；Wood ash is introduced primarily into the elements such as calcium, phosphorus, potassium, is good cosolvent,
There is certain suspension to glaze slip, the melting temperature of glaze and the high temperature viscosity of glaze can be reduced, while there is opaque and to chun glaze
The facilitation of split-phase.This medicine, quartz, calcite, lime stone, melilite, block tin, Copper Ores, wood used in the present invention
Ash, bone ash originate from Yuzhou.
Embodiment 2
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 13 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.
The preparation method of above-mentioned green glaze modelled after an antique, comprises the following steps：
（1）The preparation of glaze slip：Above-mentioned raw materials are added into appropriate water to mix, ball milling, obtain the glaze slip that mass concentration is 56%；
（2）Glazing：Base substrate is immersed into step（1）In take out for a moment in obtained glaze slip, be again dipped into a moment, take out, utilize base
The water imbibition of body, makes glaze slip uniformly be attached to billet surface；
（3）Burn till, 1270 DEG C of firing temperature；
Firing process specifically comprises the following steps：
1. the oxidizing flame stage：Base substrate after glazing is put into kiln after being fitted into saggar, controls the chimney casket plate of ventilation to open, kiln top
Skylight opens, and makes to be under oxidizing atmosphere in kiln, and make kiln temperature be ramped up 950 DEG C in 4h from room temperature；
2. the strong reducing flame stage：After kiln temperature rises to 950 DEG C, skylight is closed, the closing or semi-open of flue casket door, makes kiln
It is interior to be under strongly reducing atmosphere, temperature is ramped up 1150 DEG C in 6h；
3. the weak reducing flame stage：After kiln temperature rises to 1150 DEG C, under weakly reducing atmosphere, temperature is set to be ramped up in 4h
1270℃；
4. cooling stage：After kiln temperature rises to 1270 DEG C, wicket is opened, substantial amounts of oxygen enters in kiln, in oxidation in kiln
Atmosphere, oxygen is aoxidized to glaze paint, cooling, and glaze colours is formed, and is made.
The present invention is not added with any chemical substance compared with prior art, in formula, utilizes a variety of hairs contained in ore
Color substance carries out color development, makes color development more natural, and by scientific and reasonable raw material proportioning and control burning process, prepares
Green glaze jade texture and opaque modelled after an antique are strong, high yield rate, up to more than 97%.
Embodiment 3
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：10 parts of this medicine, 12 parts of quartz, 14 parts of calcite, lime
6 parts of stone, 43 parts of melilite, 0.7 part of block tin, 3.5 parts of Copper Ores, 12 parts of wood ash, 4.5 parts of bone ash.
The preparation method of above-mentioned green glaze modelled after an antique, comprises the following steps：
（1）The preparation of glaze slip：Above-mentioned raw materials are added into appropriate water to mix, ball milling, obtain the glaze slip that mass concentration is 55%；
（2）Glazing：Base substrate is immersed into step（1）In take out for a moment in obtained glaze slip, be again dipped into a moment, take out, utilize base
The water imbibition of body, makes glaze slip uniformly be attached to billet surface；
（3）Burn till, 1260 DEG C of firing temperature；
Firing process specifically comprises the following steps：
1. the oxidizing flame stage：Base substrate after glazing is put into kiln after being fitted into saggar, controls the chimney casket plate of ventilation to open, kiln top
Skylight opens, and makes to be under oxidizing atmosphere in kiln, and make kiln temperature be ramped up 980 DEG C in 3h from room temperature；
2. the strong reducing flame stage：After kiln temperature rises to 980 DEG C, skylight is closed, the closing or semi-open of flue casket door, makes kiln
It is interior to be under strongly reducing atmosphere, temperature is ramped up 1120 DEG C in 7h；
3. the weak reducing flame stage：After kiln temperature rises to 1120 DEG C, under weakly reducing atmosphere, temperature is set to be ramped up in 4.5h
1260℃；
4. cooling stage：After kiln temperature rises to 1260 DEG C, wicket is opened, substantial amounts of oxygen enters in kiln, in oxidation in kiln
Atmosphere, oxygen is aoxidized to glaze paint, cooling, and glaze colours is formed, and is made.
The present invention is not added with any chemical substance compared with prior art, in formula, utilizes a variety of hairs contained in ore
Color substance carries out color development, makes color development more natural, and by scientific and reasonable raw material proportioning and control burning process, prepares
Green glaze jade texture and opaque modelled after an antique are strong, high yield rate, up to more than 95%.
Comparative example 1
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 13 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 35 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.Specific preparation method is the same as embodiment 2.This
Example compared with Example 2, reduces the usage amount of melilite, mainly contains biological cycle in melilite, potassium sodium content in glaze
It is too low, reduce the coefficient of expansion, make the easy sliver of glaze paint burnt out, yield rate only has 86%.
Comparative example 2
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 20 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.Specific preparation method is the same as embodiment 2.This
Example compared with Example 2, adds the dosage of quartz, mainly contains element silicon in quartz, silicone content is too high in glaze, burns out
The easy sliver of glaze paint, yield rate only has 84%.
Comparative example 3
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 13 parts of quartz, 20 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.Specific preparation method is the same as embodiment 2.This
Example compared with Example 2, adds the dosage of calcite, calcium constituent is mainly contained in calcite, and calcium content is too high in glaze, burns
The easy smoking of glaze paint made, yield rate only have 83%.
Comparative example 4
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：20 parts of this medicine, 13 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.Specific preparation method is the same as embodiment 2.This
Example compared with Example 2, adds the dosage of this medicine, element silicon is mainly contained in this medicine, also containing a small amount of ferro element, fires
The easy sagging of glaze gone out, and green is light green, yield rate 85%.
Comparative example 5
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 13 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores.Specific preparation method is the same as embodiment 2.This example compared with Example 2, not
Bone ash, wood ash are added, the glaze jade texture and opaque burnt out is poor, yield rate 60%.
Comparative example 6
A kind of green glaze modelled after an antique, is prepared by the raw material of following parts by weight：12 parts of this medicine, 13 parts of quartz, 12 parts of calcite, lime
5 parts of stone, 40 parts of melilite, 1 part of block tin, 0.5 part of Copper Ores, 10 parts of wood ash, 4 parts of bone ash.Specific preparation method is the same as embodiment 2.
This example compared with Example 2, reduces the content of Copper Ores, and the glaze surface burnt out presents red.
The formula for the green glaze modelled after an antique that 4-25 of the embodiment of the present invention is provided is shown in Table 1-3.
Claims (4)
1. a kind of green glaze modelled after an antique, it is characterised in that it is prepared by the raw material of following parts by weight：This medicine 9-15 parts, quartz
10-16 parts, calcite 10-14 parts, lime stone 4-6 parts, melilite 37-43 parts, block tin 0.5-1.5 parts, Copper Ores 2.5-3.5
Part, wood ash 7-13 parts, bone ash 3.5-4.5 parts.
2. green glaze modelled after an antique as claimed in claim 1, it is characterised in that it is prepared by the raw material of following parts by weight：This
12 parts of medicine, 13 parts of quartz, 12 parts of calcite, 5 parts of lime stone, 40 parts of melilite, 1 part of block tin, 3 parts of Copper Ores, 10 parts of wood ash, bone
4 parts of ash.
3. the preparation method of the green glaze modelled after an antique as described in claim any one of 1-2, it is characterised in that comprise the following steps：
（1）The preparation of glaze slip；
（2）Glazing；
（3）Burn till, 1260-1280 DEG C of firing temperature.
4. the preparation method of green glaze modelled after an antique as claimed in claim 3, it is characterised in that step（3）In firing process specifically wrap
Include following steps：1. the oxidizing flame stage：Base substrate after glazing is put into kiln, is fired under oxidizing atmosphere, makes temperature in 3-5h
It is ramped up 920-980 DEG C；2. the strong reducing flame stage：Under strongly reducing atmosphere, temperature is set to be ramped up 1120-1180 in 5-7h
℃；3. the weak reducing flame stage：Under weakly reducing atmosphere, temperature is set to be ramped up 1260-1280 DEG C in 3.5-4.5h；4. cool down rank
Section：Room temperature is naturally cooled to, is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710948790.XA CN107540225A (en) | 2017-10-12 | 2017-10-12 | A kind of green glaze modelled after an antique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710948790.XA CN107540225A (en) | 2017-10-12 | 2017-10-12 | A kind of green glaze modelled after an antique |
Publications (1)
| Publication Number | Publication Date |
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| CN107540225A true CN107540225A (en) | 2018-01-05 |
Family
ID=60967081
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| CN201710948790.XA Withdrawn CN107540225A (en) | 2017-10-12 | 2017-10-12 | A kind of green glaze modelled after an antique |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109384472A (en) * | 2018-12-12 | 2019-02-26 | 禹州市天宝钧瓷文化有限公司 | A kind of alkaline-resisting enamel |
| CN111268908A (en) * | 2020-03-02 | 2020-06-12 | 福建省德化县昱晟工艺品有限责任公司 | Preparation method of low-temperature peacock green glaze porcelain |
| CN111362726A (en) * | 2020-03-27 | 2020-07-03 | 福建省盛荣生态花卉研究院有限责任公司 | Green glaze and glazing process |
| CN113233764A (en) * | 2021-05-18 | 2021-08-10 | 德化恒瀚艺品有限公司 | Antique white-green glaze material, preparation method thereof and preparation method of antique white-green glaze ceramic product |
-
2017
- 2017-10-12 CN CN201710948790.XA patent/CN107540225A/en not_active Withdrawn
Non-Patent Citations (1)
| Title |
|---|
| 苗松华: "青绿釉系列初探", 《陶瓷研究》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109384472A (en) * | 2018-12-12 | 2019-02-26 | 禹州市天宝钧瓷文化有限公司 | A kind of alkaline-resisting enamel |
| CN111268908A (en) * | 2020-03-02 | 2020-06-12 | 福建省德化县昱晟工艺品有限责任公司 | Preparation method of low-temperature peacock green glaze porcelain |
| CN111362726A (en) * | 2020-03-27 | 2020-07-03 | 福建省盛荣生态花卉研究院有限责任公司 | Green glaze and glazing process |
| CN113233764A (en) * | 2021-05-18 | 2021-08-10 | 德化恒瀚艺品有限公司 | Antique white-green glaze material, preparation method thereof and preparation method of antique white-green glaze ceramic product |
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Application publication date: 20180105 |