CN107043214A - Brownish black floor iron red colored crystalline point ceramic glaze and the method using its preparation ceramics - Google Patents
Brownish black floor iron red colored crystalline point ceramic glaze and the method using its preparation ceramics Download PDFInfo
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- CN107043214A CN107043214A CN201710169357.6A CN201710169357A CN107043214A CN 107043214 A CN107043214 A CN 107043214A CN 201710169357 A CN201710169357 A CN 201710169357A CN 107043214 A CN107043214 A CN 107043214A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6567—Treatment time
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
- C04B2235/661—Multi-step sintering
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Abstract
A kind of method that ceramics are prepared the invention discloses brownish black floor iron red colored crystalline point ceramic glaze and using it, it is related to ceramic commodity preparation field, the brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition is 40 55 parts of albites, 15 25 parts of burning talcums, 5 15 parts of bone ashes, 15 parts of quartz, 13 parts of kaolin, 35 parts of magnesium carbonate and 5 10 parts of iron oxide.Brownish black floor iron red colored crystalline point glaze in the present invention, its glaze colours entire body is sedate brownish black, tiny rust crystalline temperature appears in base substrate bottom, because crystalline temperature is made up of numerous scattered fine droplets, due to certain optical principle, watched by tea medium, it may appear that rust is changed into golden visual effect, it is great to play entertaining, the sentiment that increase people drink tea.
Description
Technical field
The present invention relates to the preparation field of ceramic commodity, a kind of brownish black floor iron red colored crystalline point pottery is more particularly related to
Glaze and the method using its preparation ceramics.
Background technology
Chinese porcelain is with a long history, and species is various, is the culture of China's successive dynasties, the witness of civilization and progress and crystallization, in being located in
There is a very important status in former Henan in the Beijing enamel history of the whole nation, and the flat-top Mountain area in Henan ancient times fires it is ceramic once
Through brilliant a period of time, reach that government porcelain kiln stands in great numbers, the grand occasion that common cave spreads all over.
Why flat-top Mountain area can possess the ceramic history of radiance, as long as its odjective cause is due to flat-top Mountain area
There are the raw material of advantageous firing ceramics.One side's water and soil brings up a side people, and side's water and soil also fires side's porcelain, profit
With the native resource of region, burn out with innovative new porcelain kind, do not continue the mission of the magnificent Ceramics Culture in region still,
It is immediately following era change, it is necessary to the requirement constantly brought forth new ideas.
Modern life rhythm is fast, and operating pressure is big, the characteristics of starting to praise highly the tea culture cultivated the moral character and nourished the nature gradually, therefore,
Need to research and develop the ceramics of new glaze colours, make people while drinking tea, increase sight and play entertaining.
The content of the invention
The present invention provides a kind of brownish black floor iron red colored crystalline point ceramic glaze and the method using its preparation ceramics, its glaze
Color entire body is sedate brownish black, and tiny rust crystalline temperature appears in base substrate bottom, because crystalline temperature is by numerous scattered
Fine droplet composition, due to certain optical principle, watched by tea medium, it may appear that rust is changed into golden vision
Effect, it is great to play entertaining, the sentiment that increase people drink tea.
Specifically, the present invention provides brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition is
40-55 parts of albites, 15-25 parts burn talcum, 5-15 parts of bone ashes, 1-5 parts of quartz, 1-3 parts of kaolin, 3-5 parts of magnesium carbonate and 5-
10 parts of iron oxide.
A kind of method that utilization brownish black floor iron red colored crystalline point glaze prepares ceramics, comprises the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：Weigh respectively 40-55 parts of albites, 15-25 parts burn talcum, 5-15 part bone ashes, 1-5 parts it is quartzy,
1-3 parts of kaolin, 3-5 parts of magnesium carbonate and 5-10 parts of iron oxide, mixing are put into ball mill, and addition water and silicon into ball mill
Sour sodium mixing and ball milling 30-40min, wherein, the weight ratio of mixed material, water and sodium metasilicate is 1:0.7:0.003, by ball milling
Slurry crosses 250 mesh sieves, and the slurry progress of sieving is old, produces glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome,
By swinging glaze method glazing, ceramic idiosome uniform rotation 3-5 is enclosed, made after the whole uniform glazings of ceramic idiosome surfaces externally and internally, will be surplus
Remaining glaze slip is poured out, will be standby after the ceramic idiosome natural air drying for having applied glaze slip；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 140-160 DEG C/h heating
Speed is risen to after 910-970 DEG C from room temperature, and adjustment heating rate is 30-50 DEG C/h, temperature is continued to rise to 1200-1300 DEG C
After be incubated 40min, when stopping heating and being naturally cooling to 50-150 DEG C, open wicket；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red
Crystalline temperature ceramic product.
Preferably, in step S2, mixed material in ball mill, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:
0.003。
It is preferred that, the rotating speed of ball mill is 65r/min.
It is preferred that, in step S2, by old 3 days of mixed slurry.
It is preferred that, in step S2, tail over as 0.5-0.8%.
It is preferred that, in step S3, ceramic idiosome inner surface glazing glazed thickness is 1-2mm.
It is preferred that, in step S4, kiln temperature fluctuation range is between ± 5 DEG C in insulating process.
In the present invention, brownish black floor iron red colored crystalline point glaze, its glaze colours entire body is sedate brownish black, tiny iron oxide red
Color crystalline temperature appears in base substrate bottom, and outward appearance is steady generous and simple and tasteful, because crystalline temperature is by numerous scattered small liquid
Drop composition, is watched by tea medium, it may appear that rust is changed into golden visual effect, i.e., with " chance tea Cheng Jin " spy
Point, can greatly increase ornamental and interest when sampling tea.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
Embodiment 1
The embodiment of the present invention 1 provides a kind of brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition
Talcum, 15 parts of bone ashes, 4 parts of quartz, 3 parts of kaolin, 3 parts of magnesium carbonate and 10 parts of iron oxide are burnt for 45 parts of albites, 20 parts.
Specifically, preparing the method for ceramics using brownish black floor iron red colored crystalline point glaze, comprise the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：Weigh respectively 45 parts of albites, 20 parts burn talcum, 15 parts of bone ashes, 4 parts of quartz, 3 parts of kaolin,
3 parts of magnesium carbonate and 10 parts of iron oxide, mixing are put into ball mill, and addition water and sodium metasilicate, mixing and ball milling into ball mill
30min, wherein, mixed material, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:0.003, drum's speed of rotation is 65r/
Min, 250 mesh sieves are crossed by the slurry of ball milling, are tailed over as 0.6%, by the slurry of sieving it is well mixed after carry out old 3 days, i.e.,
Obtain glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome,
By swinging glaze method glazing, ceramic idiosome uniform rotation 3 is enclosed, makes all uniform glazings, and glaze layer of ceramic idiosome surfaces externally and internally
Thickness, will be standby after the ceramic idiosome natural air drying for having applied glaze slip for after 1mm, remaining glaze slip is poured out；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 140 DEG C/h heating rate
Rise to after 920 DEG C, adjustment heating rate is 35 DEG C/h, continues to rise to temperature and 40min is incubated after 1220 DEG C, stop from room temperature
When heating and being naturally cooling to 60 DEG C, open wicket, wherein, in insulating process kiln temperature fluctuation range between ± 5 DEG C,；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red
Crystalline temperature ceramic product.
Embodiment 2
The embodiment of the present invention 2 provides a kind of brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition
Talcum, 15 parts of bone ashes, 3 parts of quartz, 3 parts of kaolin, 3 parts of magnesium carbonate and 8 parts of iron oxide are burnt for 50 parts of albites, 18 parts.
Specifically, preparing the method for ceramics using brownish black floor iron red colored crystalline point glaze, comprise the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：Weigh respectively 50 parts of albites, 18 parts burn talcum, 15 parts of bone ashes, 3 parts of quartz, 3 parts of kaolin,
3 parts of magnesium carbonate and 8 parts of iron oxide, mixing are put into ball mill, and addition water and sodium metasilicate, mixing and ball milling into ball mill
35min, wherein, mixed material, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:0.003, drum's speed of rotation is 280r/
Min, 250 mesh sieves are crossed by the slurry of ball milling, are tailed over as 0.7%, by the slurry of sieving it is well mixed after carry out old 3 days, i.e.,
Obtain glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome,
By swinging glaze method glazing, ceramic idiosome uniform rotation 3 is enclosed, makes all uniform glazings, and glaze layer of ceramic idiosome surfaces externally and internally
Thickness, will be standby after the ceramic idiosome natural air drying for having applied glaze slip for after 1.5mm, remaining glaze slip is poured out；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 150 DEG C/h heating rate
Rise to after 940 DEG C, adjustment heating rate is 40 DEG C/h, continues to rise to temperature and 40min is incubated after 1240 DEG C, stop from room temperature
When heating and being naturally cooling to 70 DEG C, open wicket, wherein, in insulating process kiln temperature fluctuation range between ± 5 DEG C,；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red
Crystalline temperature ceramic product.
Embodiment 3
The embodiment of the present invention 3 provides a kind of brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition
Talcum, 10 parts of bone ashes, 5 parts of quartz, 2 parts of kaolin, 5 parts of magnesium carbonate and 8 parts of iron oxide are burnt for 55 parts of albites, 15 parts.
Specifically, preparing the method for ceramics using brownish black floor iron red colored crystalline point glaze, comprise the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：Weigh respectively 55 parts of albites, 15 parts burn talcum, 10 parts of bone ashes, 5 parts of quartz, 2 parts of kaolin,
5 parts of magnesium carbonate and 8 parts of iron oxide, mixing are put into ball mill, and addition water and sodium metasilicate, mixing and ball milling into ball mill
40min, wherein, mixed material, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:0.003, drum's speed of rotation is 65r/
Min, 250 mesh sieves are crossed by the slurry of ball milling, are tailed over as 0.8%, by the slurry of sieving it is well mixed after carry out old 3 days, i.e.,
Obtain glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome,
By swinging glaze method glazing, ceramic idiosome uniform rotation 5 is enclosed, makes all uniform glazings, and glaze layer of ceramic idiosome surfaces externally and internally
Thickness, will be standby after the ceramic idiosome natural air drying for having applied glaze slip for after 2mm, remaining glaze slip is poured out；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 160 DEG C/h heating rate
Rise to after 960 DEG C, adjustment heating rate is 50 DEG C/h, continues to rise to temperature and 40min is incubated after 1280 DEG C, stop from room temperature
When heating and being naturally cooling to 80 DEG C, open wicket, wherein, in insulating process kiln temperature fluctuation range between ± 5 DEG C,；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red
Crystalline temperature ceramic product.
Embodiment 4
The embodiment of the present invention 4 provides a kind of brownish black floor iron red colored crystalline point glaze, according to parts by weight, its raw material composition
Talcum, 5 parts of bone ashes, 1 part of quartz, 1 part of kaolin, 5 parts of magnesium carbonate and 5 parts of iron oxide are burnt for 40 parts of albites, 25 parts.
Specifically, preparing the method for ceramics using brownish black floor iron red colored crystalline point glaze, comprise the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：40 parts of albites, 25 parts of burning talcums, 5 parts of bone ashes, 1 part of quartz, 1 part of kaolin, 5 are weighed respectively
Part magnesium carbonate and 5 parts of iron oxide, mixing are put into ball mill, and addition water and sodium metasilicate, mixing and ball milling into ball mill
30min, wherein, mixed material, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:0.003, drum's speed of rotation is 65r/
Min, 250 mesh sieves are crossed by the slurry of ball milling, are tailed over as 0.5%, by the slurry of sieving it is well mixed after carry out old 3 days, i.e.,
Obtain glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome,
By swinging glaze method glazing, ceramic idiosome uniform rotation 3 is enclosed, makes all uniform glazings, and glaze layer of ceramic idiosome surfaces externally and internally
Thickness, will be standby after the ceramic idiosome natural air drying for having applied glaze slip for after 1mm, remaining glaze slip is poured out；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 150 DEG C/h heating rate
Rise to after 970 DEG C, adjustment heating rate is 30 DEG C/h, continues to rise to temperature and 40min is incubated after 1300 DEG C, stop from room temperature
When heating and being naturally cooling to 150 DEG C, open wicket, wherein, in insulating process kiln temperature fluctuation range between ± 5 DEG C,；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red
Crystalline temperature ceramic product.
, but those skilled in the art once know basic creation although preferred embodiments of the present invention have been described
Property concept, then can make other change and modification to these embodiments.So, appended claims are intended to be construed to include excellent
Select embodiment and fall into having altered and changing for the scope of the invention.
Obviously, those skilled in the art can carry out the essence of various changes and modification without departing from the present invention to the present invention
God and scope.So, if these modifications and variations of the present invention belong to the scope of the claims in the present invention and its equivalent technologies
Within, then the present invention is also intended to comprising including these changes and modification.
Claims (8)
1. a kind of brownish black floor iron red colored crystalline point ceramic glaze, it is characterised in that according to parts by weight, its raw material, which is constituted, is
40-55 parts of albites, 15-25 parts burn talcum, 5-15 parts of bone ashes, 1-5 parts of quartz, 1-3 parts of kaolin, 3-5 parts of magnesium carbonate and 5-
10 parts of iron oxide.
2. the method that the brownish black floor iron red colored crystalline point ceramic glaze described in a kind of utilization claim 1 prepares ceramics, it is special
Levy and be, comprise the following steps：
S1, preparation ceramic idiosome：Feldspathic china idiosome pug is chosen, draws embryo to repair embryo after shaping and is drying to obtain ceramic idiosome；
It is prepared by S2, glaze slip：40-55 parts of albites, 15-25 parts of burning talcums, 5-15 parts of bone ashes, 1-5 parts of quartz, 1-3 are weighed respectively
Part kaolin, 3-5 parts of magnesium carbonate and 5-10 parts of iron oxide, mixing are put into ball mill, and addition water and silicic acid into ball mill
Sodium mixing and ball milling 30-40min, wherein, the weight ratio of mixed material, water and sodium metasilicate is 1:0.7:0.003, by the material of ball milling
250 mesh sieves were starched, the slurry progress of sieving is old, produce glaze slip；
S3, by ready drying of ceramic idiosome moisturizing and dedusting is wiped, the glaze slip prepared is poured into ceramic idiosome, passed through
Glaze method glazing is swung, ceramic idiosome uniform rotation 3-5 is enclosed, is made after the whole uniform glazings of ceramic idiosome surfaces externally and internally, by remaining glaze
Slurry is poured out, will be standby after the ceramic idiosome natural air drying for having applied glaze slip；
S4, the ceramic idiosome loading of kiln dried after glazing is fired, control kiln temperature is with 140-160 DEG C/h heating rate
Risen to from room temperature after 910-970 DEG C, adjustment heating rate is 30-50 DEG C/h, temperature is continued to rise to after 1200-1300 DEG C and protect
Warm 40min, when stopping heating and being naturally cooling to 50-150 DEG C, opens wicket；
S5, kiln temperature are down to after room temperature, are taken out the ceramic idiosome after firing in kiln, are produced brownish black floor iron red colored crystalline
Point ceramic product.
3. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that step
In rapid S2, mixed material in ball mill, abrading-ball, the weight ratio of water and sodium metasilicate are 1:2:0.7:0.003.
4. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that institute
The rotating speed for stating ball mill is 65r/min.
5. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that step
In rapid S2, by old 3 days of mixed slurry.
6. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that step
In rapid S2, tail over as 0.5-0.8%.
7. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that step
In rapid S3, ceramic idiosome inner surface glazing glazed thickness is 1-2mm.
8. the method that brownish black floor iron red colored crystalline point glaze according to claim 2 prepares ceramics, it is characterised in that step
In rapid S4, kiln temperature fluctuation range is between ± 5 DEG C in insulating process.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108069609A (en) * | 2017-12-04 | 2018-05-25 | 李经文 | Reddish brown rust coloured glaze and preparation method thereof |
| CN109179997A (en) * | 2018-11-26 | 2019-01-11 | 福建省德化县鸿芳陶瓷有限公司 | A kind of high temperature transmutation TianXing glaze ceramic glaze and its high temperature transmutation TianXing glaze ceramics preparation process |
| CN111792846A (en) * | 2020-07-08 | 2020-10-20 | 佛山市东鹏陶瓷有限公司 | Oxidation-resistant porcelain glazed tile and preparation method thereof |
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| CN104529548A (en) * | 2015-01-23 | 2015-04-22 | 广东省大埔陶瓷工业研究所 | Red-spot crystalline glaze and preparation method of ceramic adopting same |
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| WO2013037091A1 (en) * | 2011-09-16 | 2013-03-21 | 广东蒙娜丽莎新型材料集团有限公司 | Glazed material and ceramic sheet and manufacturing process therefor |
| CN104529548A (en) * | 2015-01-23 | 2015-04-22 | 广东省大埔陶瓷工业研究所 | Red-spot crystalline glaze and preparation method of ceramic adopting same |
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