CN106276911A - 氮掺杂石墨烯的制造方法及其复合式散热片的制造方法 - Google Patents
氮掺杂石墨烯的制造方法及其复合式散热片的制造方法 Download PDFInfo
- Publication number
- CN106276911A CN106276911A CN201610023641.8A CN201610023641A CN106276911A CN 106276911 A CN106276911 A CN 106276911A CN 201610023641 A CN201610023641 A CN 201610023641A CN 106276911 A CN106276911 A CN 106276911A
- Authority
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- China
- Prior art keywords
- nitrogen
- graphene
- doped graphene
- manufacture method
- solid phase
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- Pending
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 216
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 195
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 51
- 239000002131 composite material Substances 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 55
- 239000007790 solid phase Substances 0.000 claims abstract description 52
- 239000000203 mixture Substances 0.000 claims abstract description 37
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000002243 precursor Substances 0.000 claims abstract description 18
- 239000002002 slurry Substances 0.000 claims abstract description 18
- 229910052751 metal Inorganic materials 0.000 claims abstract description 9
- 239000002184 metal Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 7
- 229920005596 polymer binder Polymers 0.000 claims abstract description 6
- 239000002491 polymer binding agent Substances 0.000 claims abstract description 6
- 239000012298 atmosphere Substances 0.000 claims abstract description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 110
- 229910052757 nitrogen Inorganic materials 0.000 claims description 57
- 239000010409 thin film Substances 0.000 claims description 36
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 24
- 239000011889 copper foil Substances 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 17
- 229910002804 graphite Inorganic materials 0.000 claims description 14
- 239000010439 graphite Substances 0.000 claims description 14
- 229910003480 inorganic solid Inorganic materials 0.000 claims description 13
- 239000010410 layer Substances 0.000 claims description 9
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 8
- 150000001336 alkenes Chemical class 0.000 claims description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 7
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 7
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 7
- 229910002651 NO3 Inorganic materials 0.000 claims description 6
- DLGYNVMUCSTYDQ-UHFFFAOYSA-N azane;pyridine Chemical compound N.C1=CC=NC=C1 DLGYNVMUCSTYDQ-UHFFFAOYSA-N 0.000 claims description 5
- 239000000853 adhesive Substances 0.000 claims description 4
- 230000001070 adhesive effect Effects 0.000 claims description 4
- 239000002356 single layer Substances 0.000 claims description 4
- 239000006258 conductive agent Substances 0.000 claims description 3
- 229910001959 inorganic nitrate Inorganic materials 0.000 claims description 3
- 206010008190 Cerebrovascular accident Diseases 0.000 claims description 2
- 208000006011 Stroke Diseases 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 239000002023 wood Substances 0.000 claims 1
- 238000000576 coating method Methods 0.000 abstract description 15
- 239000011248 coating agent Substances 0.000 abstract description 12
- 238000005245 sintering Methods 0.000 abstract description 3
- 239000000758 substrate Substances 0.000 abstract description 2
- 238000001035 drying Methods 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 77
- 230000000694 effects Effects 0.000 description 21
- 238000002360 preparation method Methods 0.000 description 17
- 229910052799 carbon Inorganic materials 0.000 description 13
- 239000006245 Carbon black Super-P Substances 0.000 description 12
- MTAZNLWOLGHBHU-UHFFFAOYSA-N butadiene-styrene rubber Chemical compound C=CC=C.C=CC1=CC=CC=C1 MTAZNLWOLGHBHU-UHFFFAOYSA-N 0.000 description 11
- 238000010438 heat treatment Methods 0.000 description 11
- 239000002390 adhesive tape Substances 0.000 description 10
- 238000005259 measurement Methods 0.000 description 9
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 8
- 238000010586 diagram Methods 0.000 description 8
- 230000007480 spreading Effects 0.000 description 8
- 238000003892 spreading Methods 0.000 description 8
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 description 7
- 239000010408 film Substances 0.000 description 6
- 229910052760 oxygen Inorganic materials 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 230000008901 benefit Effects 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 230000005855 radiation Effects 0.000 description 5
- 230000000191 radiation effect Effects 0.000 description 5
- 239000004575 stone Substances 0.000 description 5
- 230000008859 change Effects 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 150000001721 carbon Chemical group 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011888 foil Substances 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 239000010931 gold Substances 0.000 description 2
- 229910052737 gold Inorganic materials 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 235000010299 hexamethylene tetramine Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000001931 thermography Methods 0.000 description 2
- 239000000654 additive Substances 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 239000004312 hexamethylene tetramine Substances 0.000 description 1
- 230000002687 intercalation Effects 0.000 description 1
- 238000009830 intercalation Methods 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000011268 mixed slurry Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 150000002829 nitrogen Chemical class 0.000 description 1
- 125000001477 organic nitrogen group Chemical group 0.000 description 1
- 238000013021 overheating Methods 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/08—Materials not undergoing a change of physical state when used
- C09K5/14—Solid materials, e.g. powdery or granular
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/182—Graphene
- C01B32/194—After-treatment
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
- C09D101/286—Alkyl ethers substituted with acid radicals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/34—Arrangements for cooling, heating, ventilating or temperature compensation ; Temperature sensing arrangements
- H01L23/36—Selection of materials, or shaping, to facilitate cooling or heating, e.g. heatsinks
- H01L23/373—Cooling facilitated by selection of materials for the device or materials for thermal expansion adaptation, e.g. carbon
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Nanotechnology (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Computer Hardware Design (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
Description
实施例 | 固相氮源 | C wt.% | O wt.% | N wt.% |
8 | (NH4)2CO3 | 90.57 | 8.21 | 1.14 |
9 | NH4NO3 | 91.78 | 8.22 | 0.04 |
10 | HCO2NH4 | 92.37 | 6.25 | 1.3 |
11 | C3H3N6 | 89.17 | 7.47 | 3.36 |
Claims (19)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
TW104120050A TWI622554B (zh) | 2015-06-22 | 2015-06-22 | Method for producing nitrogen-doped graphene and manufacturing method of composite heat sink |
TW104120050 | 2015-06-22 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN106276911A true CN106276911A (zh) | 2017-01-04 |
Family
ID=57587584
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610023641.8A Pending CN106276911A (zh) | 2015-06-22 | 2016-01-14 | 氮掺杂石墨烯的制造方法及其复合式散热片的制造方法 |
Country Status (3)
Country | Link |
---|---|
US (1) | US10494557B2 (zh) |
CN (1) | CN106276911A (zh) |
TW (1) | TWI622554B (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107227145A (zh) * | 2017-05-04 | 2017-10-03 | 中原大学 | 散热浆料及散热结构的制造方法 |
CN108695515A (zh) * | 2018-03-20 | 2018-10-23 | 中原大学 | 一种二次电池用负极材料的制造方法 |
CN108706578A (zh) * | 2018-07-05 | 2018-10-26 | 新奥石墨烯技术有限公司 | 氮掺杂石墨烯及其制备方法和电容器 |
CN109305917A (zh) * | 2017-07-28 | 2019-02-05 | 中国石油化工股份有限公司 | 一种卤代苯胺的合成方法 |
CN112758919A (zh) * | 2020-12-28 | 2021-05-07 | 西安交通大学 | 一种氮、硫双掺杂石墨烯及其制备方法和采用其制备超级电容器材料的方法 |
Families Citing this family (9)
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US9583358B2 (en) | 2014-05-30 | 2017-02-28 | Samsung Electronics Co., Ltd. | Hardmask composition and method of forming pattern by using the hardmask composition |
KR102287343B1 (ko) | 2014-07-04 | 2021-08-06 | 삼성전자주식회사 | 하드마스크 조성물 및 이를 이용한 패턴의 형성방법 |
KR102287344B1 (ko) | 2014-07-25 | 2021-08-06 | 삼성전자주식회사 | 하드마스크 조성물 및 이를 이용한 패턴의 형성방법 |
KR102384226B1 (ko) * | 2015-03-24 | 2022-04-07 | 삼성전자주식회사 | 하드마스크 조성물 및 이를 이용한 패턴 형성방법 |
KR102463893B1 (ko) | 2015-04-03 | 2022-11-04 | 삼성전자주식회사 | 하드마스크 조성물 및 이를 이용한 패턴의 형성방법 |
US11034847B2 (en) | 2017-07-14 | 2021-06-15 | Samsung Electronics Co., Ltd. | Hardmask composition, method of forming pattern using hardmask composition, and hardmask formed from hardmask composition |
KR102433666B1 (ko) | 2017-07-27 | 2022-08-18 | 삼성전자주식회사 | 하드마스크 조성물, 이를 이용한 패턴의 형성방법 및 상기 하드마스크 조성물을 이용하여 형성된 하드마스크 |
KR102486388B1 (ko) | 2017-07-28 | 2023-01-09 | 삼성전자주식회사 | 그래핀 양자점의 제조방법, 상기 제조방법에 따라 얻어진 그래핀 양자점을 포함한 하드마스크 조성물, 이를 이용한 패턴의 형성방법 및 상기 하드마스크 조성물을 이용하여 형성된 하드마스크 |
TWI646051B (zh) * | 2018-02-07 | 2019-01-01 | 光宇材料股份有限公司 | 氮摻雜碳矽複合材料及其製造方法 |
Citations (3)
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CN102887501A (zh) * | 2011-07-21 | 2013-01-23 | 海洋王照明科技股份有限公司 | 一种掺氮石墨烯的制备方法 |
CN103626158A (zh) * | 2012-08-23 | 2014-03-12 | 中国科学院宁波材料技术与工程研究所 | 氮掺杂石墨烯的制备方法及其应用 |
CN104600320A (zh) * | 2013-10-30 | 2015-05-06 | 上海悦达墨特瑞新材料科技有限公司 | 一种基于石墨烯的功能铜箔及其制备方法 |
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CN101422725B (zh) * | 2007-11-02 | 2010-07-14 | 中国科学院过程工程研究所 | 一种可见光响应的氮掺杂二氧化钛纳米管的制备方法及其应用 |
CN103896254A (zh) * | 2012-12-26 | 2014-07-02 | 海洋王照明科技股份有限公司 | 一种氮掺杂石墨烯的制备方法 |
CN103288075A (zh) * | 2013-05-24 | 2013-09-11 | 大连理工大学 | 氮掺杂石墨烯纳米带及其制备方法 |
CN103803539B (zh) * | 2014-02-17 | 2015-09-09 | 上海交通大学 | 一种氮掺杂氧化石墨烯材料及其制备方法 |
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2015
- 2015-06-22 TW TW104120050A patent/TWI622554B/zh active
-
2016
- 2016-01-14 CN CN201610023641.8A patent/CN106276911A/zh active Pending
- 2016-05-30 US US15/168,097 patent/US10494557B2/en active Active
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107227145A (zh) * | 2017-05-04 | 2017-10-03 | 中原大学 | 散热浆料及散热结构的制造方法 |
CN109305917A (zh) * | 2017-07-28 | 2019-02-05 | 中国石油化工股份有限公司 | 一种卤代苯胺的合成方法 |
CN108695515A (zh) * | 2018-03-20 | 2018-10-23 | 中原大学 | 一种二次电池用负极材料的制造方法 |
CN108706578A (zh) * | 2018-07-05 | 2018-10-26 | 新奥石墨烯技术有限公司 | 氮掺杂石墨烯及其制备方法和电容器 |
CN108706578B (zh) * | 2018-07-05 | 2020-08-11 | 新奥石墨烯技术有限公司 | 氮掺杂石墨烯及其制备方法和电容器 |
CN112758919A (zh) * | 2020-12-28 | 2021-05-07 | 西安交通大学 | 一种氮、硫双掺杂石墨烯及其制备方法和采用其制备超级电容器材料的方法 |
Also Published As
Publication number | Publication date |
---|---|
TWI622554B (zh) | 2018-05-01 |
US20160369149A1 (en) | 2016-12-22 |
TW201700401A (zh) | 2017-01-01 |
US10494557B2 (en) | 2019-12-03 |
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