CN106265172A - A kind of procyanidin white carbon sunscreen - Google Patents

A kind of procyanidin white carbon sunscreen Download PDF

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Publication number
CN106265172A
CN106265172A CN201610984947.XA CN201610984947A CN106265172A CN 106265172 A CN106265172 A CN 106265172A CN 201610984947 A CN201610984947 A CN 201610984947A CN 106265172 A CN106265172 A CN 106265172A
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procyanidin
sunscreen
white carbon
anthocyanidin
gas
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铁健
柳馨
铁生年
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Qinghai University
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Qinghai University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4913Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to daily cosmetics technical field, particularly relate to a kind of procyanidin white carbon sunscreen.Including following components: procyanidin, anthocyanidin, white carbon, olive oil, suddenly bar oil, dimethicone, glycerol, vitamin, stearic acid, minaline alkanone carboxylic acid sodium, essence, deionized water.One procyanidin white carbon sunscreen of the present invention, stronger to the absorption of ultraviolet and reflectance than the sunscreen product of prior art, good stability, whitening effect, moistening effect are obvious, also can make the skin contraction relaxed, tighten, reduce wrinkle, make skin fine and smooth;Improve gas-phase silica and the value containing procyanidin/anthocyanidin raw material.

Description

A kind of procyanidin white carbon sunscreen
Technical field
The present invention relates to daily cosmetics technical field, particularly relate to a kind of procyanidin white carbon sunscreen.
Background technology
Ultraviolet in sunlight is to cause skin ageing and the principal element forming skin table planar patch.Ultraviolet pair The injury of skin mainly have following some: (1) makes B16 cell increase, and causes pigementation, such as black speck, freckle, chloasma Etc. the increasing of various mottles, increase, deepen.(2) forming hyperplasia, dermal collagen fiber destroys, may result in pachyderma, pine Relaxation, coarse and formation wrinkle.(3) telangiectasis, produces erythema.(4) skin immune function controlling declines, and forms skin carcinoma or cancer Front pathological changes, such as light keratosis, squamous cell carcinoma, melanoma etc..At present, out of doors generally by wiping the side of sunscreen cream to skin Formula prevents the ultraviolet damage to skin, and the action principle of sunscreen cream is to be kept apart with ultraviolet by skin, thus prevents skin Skin is tanned severely.
Procyanidin (Proanthocyanidins is called for short PC) is by different number of flavan-3-alcohol or flavane-3,4-bis- Alcohol is polymerized, and two-tetramer is wherein referred to as Oligomeric Proanthocyanidins, and (Proanthocyanidin Oligomers is called for short OPC), five poly-ten gather for high polymer (Proanthocyanidin Olymers, be called for short PPC), are that one has particular molecule to tie The bioflavonoids of structure.The polyhydroxy structure of procyanidin makes it have special antioxygenic activity and remove the ability of free radical.One As be red-brown powder, feeble QI, puckery, be dissolved in water and most organic solvent, be the most potent freedom found so far Base scavenger, has the strongest activity in vivo.The free radical resisting oxidability of OPC is 50 times of vitamin E, ascorbic 20 times, and absorb the most completely.Owing to procyanidin has chemistry and the physiologically active of uniqueness, skin care item play many recasts With, as defying age, uvioresistant, radioprotective, brighten, moisturizing etc., the skin aging causing many factors has the merit of uniqueness Effect, wherein, sun-proof whitening function is particularly pertinent.
The Semen Vitis viniferae that has now been found that, Lycium ruthenicum Murr., Fructus Lycii, blue berry, seed of Fructus Hippophae, black currant, Fructus Mume, Fructus Mori etc. all contain former flower Blue or green element.Black Fructus Lycii contains the natural pattern glycoside active substances such as substantial amounts of procyanidin (OPC), anthocyanidin.Black Fructus Lycii is Having now been found that the highest plant of (OPC) containing procyanidin, the content of its procyanidin is up to 5.04%, finds up to now The wild fruit that procyanidin (OPC) content is the highest, is also the maximally effective ecosystem Natural antioxidant.The Radix osteomelis schwerinais in Qinghai Fructus Lycii stock number is very big, and quite a few resource cannot utilize.
Anthocyanidin (Anthocyanidin), also known as anthocyanidin, is the water solublity that is widely present in plant of nature one class Natural pigment, belongs to flavonoids.Anthocyanidin is a kind of strong antioxidant, and it can protect human body from free radical The damage of harmful substance.At cosmetic field, anthocyanidin product common trait is good, to microorganism to light, heat, oxidative stability Stable, typically it is dissolved in water and ethanol, insoluble in vegetable oil;In terms of resisting ultraviolet, anthocyanidin is natural sunlight overcover, Ultraviolet damage skin can be stoped.It can also strengthen blood vessel elasticity, improves blood circulation and promotes the smoothness of skin, pressing down Inflammation processed and allergy, improve the pliability in joint.
White carbon is white powder X-ray amorphous silicic acid and the general name of silicate product, is primarily referred to as precipitating dioxy SiClx, aerosil and superfine silicon dioxide gel, also include powder synthetic aluminium silicate and calcium silicates etc..Vapor phase method is white White carbon black is the chloride Silicon chloride. of silicon or trichlorine monomethyl silane generates through pyrohydrolysis in air and hydrogen mixed gas stream The unformed powder of one, spheroidal particle often, surface is with hydroxyl and absorption water, and chemical purity is high, SiO2>=99%.Gas Phase method white carbon can be divided into hydrophilic and hydrophobic type according to whether carry out surface process, can be divided into again according to the size of specific surface Different models.
At cosmetic field, gas-phase silica is inorganic constituents due to it, it is easy to other component compatibility of cosmetics, nothing Malicious, tasteless, there are not the problems referred to above, and from as white, can be coloured simply, the most valuable is gas-phase silica Reflection ultraviolet ability is strong, good stability, does not decomposes, invariant color, also will not rise with other component in formula after being irradiated by ultraviolet Chemical reaction.The upgrading that these outstanding features are sun care preparations of gas-phase silica is had laid a good foundation.
For sun care preparations, it is desirable to strong to ultraviolet screening ability, be desirable to defend ultraviolet medium wave (UVB), The long wave (UVA) harm to human body.Substantially, ultraviolet shielded two aspects that include, one is the absorption to ultraviolet noted earlier, separately On the one hand being the reflection to ultraviolet, at present, the report from the anti ultraviolet agent of ultraviolet reflectance performance angle exploitation compares in the world Rare.In sunscreen product, the most use organic compound are UV absorbent, but exist such as in order to protect as far as possible After sheath skin does not contacts ultraviolet and improves addition, generation skin carcinoma can be increased and produce the problems such as chemical allergy. Current existing sun-proof skin-lightening cosmetic is the product of oiliness mostly, and skin is had local irritation, even has carcinogenesis, and Sun-proof result is the best.
In sum, for solving the problem that above-mentioned prior art exists, the present invention utilizes procyanidin or anthocyanidin with white White carbon black is major function raw material, is prepared for a kind of sunscreen with stronger anti-ultraviolet function.
Summary of the invention
It is an object of the invention to provide a kind of procyanidin white carbon sunscreen.
A kind of procyanidin white carbon sunscreen, including the following components of percentage by weight meter: procyanidin 1~15%, White carbon 1~15%, olive oil 1~10%, suddenly bar oil 1~10%, dimethicone 1~5%, glycerol 1~7%, vitamin E1~5%, stearic acid 1~8%, minaline alkanone carboxylic acid sodium 1~8%, essence 1~2%, surplus is deionized water.
Procyanidin in raw material of the present invention and anthocyanidin are from natural black Fructus Lycii, Semen Vitis viniferae, blue berry, black add Logical sequence, Fructus Mume, Fructus Mori fruit extract gained.Therefore, procyanidin and anthocyanidin can be substituted for each other, and formula is as follows:
A kind of anthocyanidin white carbon sunscreen, including the following components of percentage by weight meter: anthocyanidin 1~15%, Linesless charcoal Black 1~15%, olive oil 1~10%, suddenly bar oil 1~10%, dimethicone 1~5%, glycerol 1~7%, vitamin e1~ 5%, stearic acid 1~8%, minaline alkanone carboxylic acid sodium 1~8%, essence 1~2%, surplus is deionized water.
Further, described white carbon is the white carbon that vapor phase method generates, wherein, dioxide-containing silica >=99%, ferrum Content≤300mg/kg, lead content≤40mg/kg, mercury content≤1mg/kg, arsenic content≤10mg/kg;Gas-phase silica particle diameter It is 20~150nm.
Further, the total number of bacteria≤950CFU/g in described sunscreen, yeast and mold sum≤90CF.
The present invention can be made into suntan lotion or sunscreen cream.
The preparation method of sunscreen of the present invention is:
(1) from black Fructus Lycii, Semen Vitis viniferae, blue berry, black currant, Fructus Mume, Fructus Mori, procyanidin/anthocyanidin is extracted;
(2) prepare dioxide-containing silica >=99%, particle diameter be 20~150nm gas-phase silica;
(3) olive oil, suddenly bar oil, dimethicone, glycerol, vitamin E, stearic acid, minaline alkanone carboxylic acid sodium, perfume (or spice) are taken Essence and deionized water, mix homogeneously, prepare sunscreen substrate;
(4) take procyanidin/anthocyanidin that step (1) prepares, take the gas-phase silica that step (2) prepares, join step Suddenly in the sunscreen substrate that (3) prepare, mix homogeneously, obtain procyanidin white carbon sunscreen.
Procyanidin/anthocyanidin is pure natural, water miscible, and has stronger ultraviolet absorbability;Meanwhile, procyanidin/ Cyanidin cosmetics also has good adhesive ability under waterproof condition to skin, and thick pore can be made to shrink, and makes pine The skin contraction relaxed, tighten, reduce wrinkle, so that skin shows the outward appearance of exquisiteness.Gas-phase silica reflection ultraviolet ability By force, good stability, do not decompose after being irradiated by ultraviolet, invariant color, also will not be with other component chemically reactive in formula.This Bright according to above-mentioned procyanidin/anthocyanidin and the advantageous characteristic of white carbon, invent a kind of procyanidin white carbon sunscreen.
The invention have the advantage that
One procyanidin white carbon sunscreen of the present invention, than the sunscreen product of prior art to the absorption of ultraviolet and anti- Ability of penetrating is strong, good stability, whitening effect, moistening effect obvious, also can make the skin contraction relaxed, tighten, reduces wrinkle, make Skin is fine and smooth;Improve gas-phase silica and the value containing procyanidin/anthocyanidin raw material.
Detailed description of the invention
Following example are used for illustrating the present invention, but are not limited to the scope of the present invention.
Embodiment 1
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment sunscreen cream is:
(1) from black Fructus Lycii, procyanidin is extracted;
(2) prepare dioxide-containing silica 99.8%, particle diameter is the gas-phase silica of 150nm;
(3) olive oil 10g, suddenly bar oil 100g are taken, dimethicone 50g, glycerol 70g, vitamin E 50g, stearic acid 10g, Minaline alkanone carboxylic acid sodium 80g, Flos Rosae Rugosae face cream essence 10g, deionized water 460g, mix homogeneously, prepare sunscreen cream substrate;
(4) take the procyanidin 10g that step (1) prepares, take the gas-phase silica 150g that step (2) prepares, join step Suddenly in the sunscreen cream substrate that (3) prepare, mix homogeneously, obtain procyanidin white carbon sunscreen cream.
Embodiment 2
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment sunscreen cream is:
(1) from extracting proanthocyanidin from grape seeds;
(2) prepare dioxide-containing silica 99.6%, particle diameter is the gas-phase silica of 120nm;
(3) olive oil 60g, suddenly bar oil 50g are taken, dimethicone 30g, glycerol 60g, vitamin E2 0g, stearic acid 60g, Minaline alkanone carboxylic acid sodium 60g, jasmine face cream essence 15g, deionized water 495g, mix homogeneously, prepare sunscreen cream substrate;
(4) take the procyanidin 80g that step (1) prepares, take the gas-phase silica 120g that step (2) prepares, join step Suddenly in the sunscreen cream substrate that (3) prepare, mix homogeneously, obtain procyanidin white carbon sunscreen cream.
Embodiment 3
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment suntan lotion is:
(1) from blue berry, procyanidin is extracted;
(2) prepare dioxide-containing silica 99%, particle diameter is the gas-phase silica of 20nm;
(3) olive oil 100g, suddenly bar oil 60g are taken, dimethicone 20g, glycerol 50g, vitamin E 30g, stearic acid 40g, Minaline alkanone carboxylic acid sodium 40g, Flos Osmanthi Fragrantis face cream essence 20g, deionized water 510g, mix homogeneously, prepare suntan lotion substrate;
(4) take the procyanidin 120g that step (1) prepares, take the gas-phase silica 10g that step (2) prepares, join step Suddenly in the suntan lotion substrate that (3) prepare, mix homogeneously, obtain procyanidin white carbon suntan lotion.
Embodiment 4
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment suntan lotion is:
(1) from black currant, procyanidin is extracted;
(2) prepare dioxide-containing silica 99.3%, particle diameter is the gas-phase silica of 100nm;
(3) olive oil 80g, suddenly bar oil 10g are taken, dimethicone 10g, glycerol 10g, vitamin e1 0g, stearic acid 80g, Minaline alkanone carboxylic acid sodium 50g, Flos Rosae Rugosae face cream essence 10g, deionized water 510g, mix homogeneously, prepare suntan lotion substrate;
(4) take the procyanidin 150g that step (1) prepares, take the gas-phase silica 80g that step (2) prepares, join step Suddenly in the suntan lotion substrate that (3) prepare, mix homogeneously, obtain procyanidin white carbon suntan lotion.
Embodiment 5
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment sunscreen cream is:
(1) from Fructus Mume, anthocyanidin is extracted;
(2) prepare dioxide-containing silica 99.8%, particle diameter is the gas-phase silica of 150nm;
(3) olive oil 10g, suddenly bar oil 100g are taken, dimethicone 50g, glycerol 70g, vitamin E 50g, stearic acid 10g, Minaline alkanone carboxylic acid sodium 80g, jasmine face cream essence 10g, deionized water 460g, mix homogeneously, prepare sunscreen cream substrate;
(4) take the anthocyanidin 10g that step (1) prepares, take the gas-phase silica 150g that step (2) prepares, join step (3) in the sunscreen cream substrate prepared, mix homogeneously, obtain anthocyanidin white carbon sunscreen cream.
Embodiment 6
The present embodiment can be made into suntan lotion or sunscreen cream.
The preparation method of the present embodiment suntan lotion is:
(1) from Fructus Mori, anthocyanidin is extracted;
(2) prepare dioxide-containing silica 99.3%, particle diameter is the gas-phase silica of 100nm;
(3) olive oil 80g, suddenly bar oil 10g are taken, dimethicone 10g, glycerol 10g, vitamin e1 0g, stearic acid 80g, Minaline alkanone carboxylic acid sodium 50g, Flos Osmanthi Fragrantis face cream essence 10g, deionized water 510g, mix homogeneously, prepare suntan lotion substrate;
(4) take the anthocyanidin 150g that step (1) prepares, take the gas-phase silica 80g that step (2) prepares, join step (3) in the suntan lotion substrate prepared, mix homogeneously, obtain anthocyanidin white carbon suntan lotion.
Procyanidin white carbon sunscreen UV transmittance is tested
1, test material
Ultra-violet and visible spectrophotometer, photoelectric analytical balance, dehydrated alcohol analysis, pure absolute ether analytical pure, 1~6 Each 3 parts of the sunscreen sample that embodiment prepares.
2, content of the test
Resistivity available parameter SPF of UVB in sunlight (290~320nm) is represented by sun-proof articles, and spf value is fixed Justice is for assuming not have the people of any sun-proof measure to expose skin after x hour in the sun at the constant uitraviolet intensity next one Skin can redden the sunscreen products consumption 2mg/cm when he uses spf value to be n2Time, his skin just meeting after the time of n × x hour Redden.In this test, the index of SPF is set to 15,30,50.
In sunlight, defence capability parameter PA of UVA (320~400nm) represents, PA protection effect is divided into three grades: PA+ represents effectively can delay 2~4 times of tanned times;PA++ represents quite effective, can delay 4~8 times of tanned times;PA+ ++ represent highly effective, more than 8 times tanned times can be delayed.
Difference sunscreen is coated on substrate so that it is be translucent shape, utilize fiber spectrometer record reflectivity curve and Transmission curve, uses the spectra methods different sun-proof performance of sunscreen of research, and to smear the time after sunscreen as variable, Exploring sunscreen uses the time to affect its sun-proof result.
3, test method
The procyanidin white carbon sunscreen that embodiment 1~6 is prepared, each enforcement take sunscreen weigh 100mg in In the bottle of 50mL capacity, add dehydrated alcohol and absolute ether makes solution by the proportioning concentration of 1:1 as solvent.To make Solution down in the quartz cuvette pond of 1cm × 1cm × 5cm, the ultra-violet and visible spectrophotometer debugged is measured 290 ~the wave-length coverage UV transparent rate of 400nm.
4, result of the test
In procyanidin white carbon sunscreen in measured above-described embodiment 1~6, different parameters value is to UVB and UVA Light transmittance, refer to table 1.
The different embodiment of table 1 UVB and the UVA light transmittance of worth sunscreen
Data show, procyanidin white carbon sunscreen obtained by each embodiment to the light transmittance of ultraviolet at spf value 15 Light transmittance is exactly 5%, and the ultraviolet that it reflected or sponged is just 95%;The light transmittance of spf value 30 is exactly 2.5%, its The ultraviolet reflecting or sponging is just 97.5%;The light transmittance of spf value 50 is exactly 2.35%, and it is reflected or absorbs The ultraviolet fallen is just 97.65%.PA between 10.64~13.33%, can effectively delay the tanned time to UV transparent rate Multiple.
Procyanidin white carbon sunscreen human test tests
1, test method: 1 group of matched group, 6 groups of experimental grouies are set, irradiate a period of time under uviol lamp, then observe survey The change of examination person's red swelling of the skin pain phenomenon carrys out Identification Evaluation test.The procyanidin white carbon prepared with the secondary evaluation present invention The anti-uv-ray of sunscreen.Test group arranges and is shown in Table 2.
Table 2 test group is arranged
2, result of the test: according to above-mentioned test method, the sunscreen 2mg/cm obtained by uniform application embodiment2, pass through Observing the situation of change of tester's red swelling of the skin pain phenomenon, result of the test is as follows:
Table 3 result of the test
3, conclusion (of pressure testing):
Being found the test of procyanidin white carbon sunscreen anti-uv-ray by tester, each embodiment prepares Sunscreen all has the effect absorbed with uv reflectance, and sun-proof result is good, and nuance is only that the consumption difference side of each component Face.

Claims (8)

1. a procyanidin white carbon sunscreen, including the following components of percentage by weight meter: olive oil 1~10%, Huo Ba Oil 1~10%, dimethicone 1~5%, glycerol 1~7%, vitamin e1~5%, stearic acid 1~8%, minaline alkanone carboxylic Acid sodium 1~8%, essence 1~2%, surplus is deionized water, it is characterised in that: possibly together with 1~15% in described sunscreen Procyanidin and 1~the white carbon of 15%.
A kind of procyanidin white carbon sunscreen the most according to claim 1, it is characterised in that: described procyanidin can Substitute with anthocyanidin.
A kind of procyanidin white carbon sunscreen the most according to claim 1, it is characterised in that: described procyanidin is Natural extract.
A kind of procyanidin white carbon sunscreen the most according to claim 2, it is characterised in that: described anthocyanidin is sky So extract.
5. according to a kind of procyanidin white carbon sunscreen described in Claims 1 to 4 any one, it is characterised in that: described White carbon be gas-phase silica, wherein, dioxide-containing silica >=99%, iron content≤300mg/kg, lead content≤40mg/ Kg, mercury content≤1mg/kg, arsenic content≤10mg/kg;Gas-phase silica particle diameter is 20~150nm.
6. according to a kind of procyanidin white carbon sunscreen described in Claims 1 to 4 any one, it is characterised in that: described Sunscreen in total number of bacteria≤950CFU/g, yeast and mold sum≤90CFU/g.
7., according to a kind of procyanidin white carbon sunscreen described in Claims 1 to 4 any one, can be made into sunscreen cream, also Can be made into suntan lotion.
8., according to a kind of procyanidin white carbon sunscreen described in Claims 1 to 4 any one, its preparation method includes:
(1) procyanidin extracts;
(2) preparation of gas-phase silica;
(3) by olive oil, suddenly bar oil, dimethicone, glycerol, vitamin, stearic acid, minaline alkanone carboxylic acid sodium, essence and Deionized water presses formula proportion mixing, makes sunscreen substrate;
(4) procyanidin, gas-phase silica and sunscreen substrate are pressed formula proportion mixing, makes procyanidin white carbon sun-proof Agent.
CN201610984947.XA 2016-11-09 2016-11-09 A kind of procyanidin white carbon sunscreen Pending CN106265172A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
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CN111514066A (en) * 2020-04-22 2020-08-11 复旦大学 Comfortable skin sunscreen coating liquid and preparation method thereof
CN112754950A (en) * 2021-04-01 2021-05-07 郑影 Water-soluble sunscreen emulsion and preparation method thereof

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CN103830123A (en) * 2013-10-02 2014-06-04 铁生年 Sunscreen cream containing microsilicon powder
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CN103520023A (en) * 2013-10-28 2014-01-22 西北农林科技大学 Sunscreen cream rich in grape seed oil and procyanidine
CN104814908A (en) * 2015-03-31 2015-08-05 广西大学 Mask with effects of resisting wrinkle and tendering skin
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107137248A (en) * 2017-04-19 2017-09-08 北海市韩能生物科技有限公司 Cosmetics containing OPC
CN111514066A (en) * 2020-04-22 2020-08-11 复旦大学 Comfortable skin sunscreen coating liquid and preparation method thereof
CN112754950A (en) * 2021-04-01 2021-05-07 郑影 Water-soluble sunscreen emulsion and preparation method thereof

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