CN106235378B - A kind of application of filler flavouring additives in cigarette - Google Patents
A kind of application of filler flavouring additives in cigarette Download PDFInfo
- Publication number
- CN106235378B CN106235378B CN201610915735.6A CN201610915735A CN106235378B CN 106235378 B CN106235378 B CN 106235378B CN 201610915735 A CN201610915735 A CN 201610915735A CN 106235378 B CN106235378 B CN 106235378B
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- China
- Prior art keywords
- flavouring additives
- cigarette
- filler
- flavouring
- wall material
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
1%~30% wall material is added in heating stirring in distilled water by mass percentage, obtains wall material solution by a kind of application of filler flavouring additives in cigarette；The flavoring substances that will be equivalent to wall material mass percent 1%~50% are slowly added into wall material solution, and stir 4h under conditions of 50 DEG C, 500~2000r/min, by flavoring substances inclusion into the cavity of wall material, obtain inclusion solution；The spray-dried obtained flavouring additives of solution will be included, in the preparation process of cigarette paper or in papermaking-method reconstituted tobaccos preparation process, will be added flavouring additives as filler.Flavouring additives are made by embedding in flavoring substances by the present invention, and simple production process is easy to spread.Flavouring additives are applied in the form of filler in cigarette by the present invention, can reduce the volatility of flavoring substances, and front and back end concentration is more uniform consistent when aspirating flue gas, improves the suction quality of cigarette.
Description
Technical field
The invention belongs to cigarette packing technique fields, and in particular to the preparation of filler flavouring additives and in cigarette
Using.
Background technology
Flavouring humectation is one of nine key special subjects that the key technology of promotion cigarette quality and industry determine.Cigarette
Type of aroma and style decide the class and grade of cigarette product, cigarette " flavouring " class essence and flavoring agent object to a certain extent
Matter can make cigarette flavor amount get a promotion, cigarette note is increased or enriched, the quality generation directly influence on cigarette.
However spices and essence substance has volatility mostly, there are high volatility, the residence time is short, the shelf-life is short, essence release is uneven
The problems such as even, make cigarette smoke release concentration there are front and rear section it is inconsistent the drawbacks of, so as to influence the raising of cigarette smoking quality
And the application range in cigarette.
Essence spice for cigarette can be embedded in using microcapsule embedded technology in the hollow cavity of wall material, protects the substance
While can also improve its stability, reduce volatility, and it made to be slowly released in the case where cigarette burns and sucks state or external force effect
Fragrance component, reaching essence and flavoring agent substance, flavouring effect is good, protects fragrant lasting, the uniform effect of release, and it is better to assign cigarette
Aspirate sensory experience.Filler can improve cigarette paper, the gas permeability of reconstituted tobacco chip base, opacity, whiteness, tensile property
With the indexs such as evenness.By can also impart to its certain functional character to filler modified.Publication No. CN103711029A's
Patent describes a kind of loaded modified CaCO3 fillers, prepares flavouring humectation cigarette paper using common papermaking process, makes fragrance alcohol
It is thick, lasting, improve the quality of cigarette.The filler modified methods of CaCO3 described in it are to be carried on flavor components by emulsifier
Modified CaCO3Filler surface, but protection and slow releasing function are not played to flavoring substances.Publication No. CN103362033A's is special
Profit discloses a kind of cigarette paper, and the cigarette paper is that fragrant extract will be caused to be prepared into the microcapsules with slow-release function, then
Addition obtains during two pressures of cigarette copy paper.Flavor matter accounts for the 5% of beta-cyclodextrin quality wherein in microcapsules, and
0.1% microencapsulation causes fragrant mixed liquor addition quality only to account for the 0.1% of cigarette paper quality.Cause perfume (or spice) extract described in it is in cigarette
Addition in paper is range-restricted larger, and the allotment that may influence flavouring formula uses.
Existing cigarette filler aromatizing technology application effect is undesirable, and microcapsules flavoring technology is in cigarette paper, reconstituted tobacco
In research it is less.
The content of the invention
The purpose of the present invention is making up the deficiencies in the prior art, improve the use limitation of flavoring substances, a kind of volume is provided
Application of the cigarette with flavouring filler auxiliary agent in cigarette.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of application of filler flavouring additives in cigarette, the filler are prepared as follows with flavouring additives：
(1) wall material that mass percent is 1%~30% is added in into heating stirring in distilled water；The wall material is α-ring
One or more of dextrin, beta-cyclodextrin, gamma-cyclodextrin, hydroxypropyl-β-cyclodextrin, Sulfobutyl ether β _ cyclodextrin；
(2) flavoring substances that wall material mass percent is 1%~50% be will be equivalent to and be slowly added into step (1) preparation
In solution, and 4h is stirred under conditions of 50 DEG C, 500~2000r/min, by flavoring substances inclusion into the cavity of wall material, obtained
To inclusion solution；The flavoring substances include but not limited to tobacco absolute oil, advanced this perfume of tobacco, tree moss absolute, rhodamine toner
Oil, orange oil, peppermint oil, lemon oil, spearmint oil, cognac green oil, dorinone, alpha, beta-lonone, Megastigmatrienone, virtue
One or more of camphor tree alcohol, isoamyl butyrate, lactone, β-carypohyllene, leaf-alcohol, pungent certain herbaceous plants with big flowers acid glyceride；
(3) the spray-dried obtained solid powdery flavouring additives not soluble in water of solution will be included；
In the preparation process of cigarette paper or in papermaking-method reconstituted tobaccos preparation process, using flavouring additives as filler into
Row addition.
Flavouring additives feed postition in the preparation process of cigarette paper is, using papermaking process by flavouring additives,
CaCO3, wood pulp cellulose, hemp compare flavouring additives according to quality：CaCO3：Wood pulp cellulose：Hemp is (10~35%)：
(5~40%)：(40~75%)：(0~45%) ratio mixes, and is prepared into pulp suspension, then manufactures paper with pulp to obtain cigarette paper.Increase
Feed postition of the fragrant auxiliary agent in papermaking-method reconstituted tobaccos preparation process is that flavouring additives are added to reconstituted tobacco chip base of manufacturing paper with pulp
Tobacco slurry in and be uniformly mixed, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain；Flavouring additives account for the quality percentage of chip base oven dry weight
Than for 5~20%.
Compared with prior art, the invention has the characteristics that：
(1) flavouring additives are made by embedding in flavoring substances, simple production process is easily promoted.
(2) compared with traditional flavoring mode, flavouring additives is applied in the form of filler in cigarette, increasing can be reduced
The volatility of Studies of The Aromatic Substances, front and back end concentration is more uniform consistent when aspirating flue gas, improves the suction quality of cigarette.
(3) by the way that the flavouring additives of filler are prepared, expand it and apply model in cigarette paper, reconstituted tobacco
It encloses, new form and new developing direction is provided for the filler of cigarette paper, reconstituted tobacco.
Specific embodiment
To more fully understand the present invention, with reference to embodiment, the invention will be further described, but the reality of the present invention
It is without being limited thereto to apply mode.
Implementation column 1
2% beta-cyclodextrin is added in into heating stirring in distilled water by mass percentage, beta-cyclodextrin solution is obtained, by phase
It is slowly added into when in the peppermint oil of beta-cyclodextrin mass percent 1% in beta-cyclodextrin solution, and in 50 DEG C, 800r/min
Under the conditions of stir 4h, by flavoring substances peppermint oil inclusion into the cavity of beta-cyclodextrin, obtain inclusion solution；It will inclusion solution warp
Powdered flavouring additives not soluble in water are made in spray drying.
The flavouring additives of preparation use regular-size cigarette paper papermaking process, by flavouring additives, CaCO3, wood pulp cellulose, hemp it is fine
Dimension compares flavouring additives according to quality:CaCO3:Wood pulp cellulose:Hemp=15%：10%：40%：45%, which is prepared into paper pulp, hangs
Supernatant liquid, obtained cigarette paper of then manufacturing paper with pulp.
Implementation column 2
By mass percent be 3% gamma-cyclodextrin in distilled water heating stirring, obtain gamma-cyclodextrin solution；By phase
When in orange oil, the isoamyl butyrate of gamma-cyclodextrin mass percent 25%, (quality compares orange oil：Isoamyl butyrate=80%：
20%) it is slowly added into gamma-cyclodextrin solution, and 4h is stirred under conditions of 50 DEG C, 1000r/min, by orange oil and fourth
Isoamyl valerate is included into the cavity of gamma-cyclodextrin, obtains inclusion solution；It is spray-dried obtained not soluble in water that solution will be included
Flavouring additives.
The flavouring additives of preparation use regular-size cigarette paper papermaking process, by flavouring additives, CaCO3, wood pulp cellulose, hemp it is fine
Dimension is according to mass ratio 10%：5%：75%：10% is prepared into pulp suspension, then manufactures paper with pulp to obtain cigarette paper.
Implementation column 3
By mass percent be 30% hydroxypropyl-β-cyclodextrin in distilled water heating stirring, obtain hydroxy propyl-Beta-ring
Dextrin solution；Will be equivalent to hydroxypropyl-β-cyclodextrin mass percent 20% advanced perfume (or spice) of tobacco and lemon oil (tobacco is advanced
This perfume：The mass ratio of lemon oil is 80%：20%) it is slowly added into hydroxypropyl-β-cyclodextrin solution, and in 50 DEG C, 500r/
4h is stirred under conditions of min, obtains inclusion solution, after reaction spray-dried obtained flavouring additives.
By the flavouring additives of preparation, the tobacco slurry for being added to reconstituted tobacco chip base of manufacturing paper with pulp by the 5% of chip base oven dry weight
In, it is uniformly mixed, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Implementation column 4
By mass percent be 20% Sulfobutyl ether β _ cyclodextrin in distilled water heating stirring, obtain sulphur butyl-β-ring
Dextrin solution；It will be equivalent to the cognac green oil, leaf-alcohol, pungent certain herbaceous plants with big flowers acid glyceride of Sulfobutyl ether β _ cyclodextrin mass percent 50%
In mass ratio 40%：10%：It is slowly added into after 50% mixing in Sulfobutyl ether β _ cyclodextrin solution, and in 50 DEG C, 1000r/
4h is stirred under conditions of min, obtains inclusion solution；Spray-dried obtained flavouring additives after reaction.
By the flavouring additives of preparation, the tobacco slurry for being added to reconstituted tobacco chip base of manufacturing paper with pulp by the 20% of chip base oven dry weight
In, it is uniformly mixed, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Implementation column 5
10% beta-cyclodextrin is added in into heating stirring in distilled water by mass percentage, obtains beta-cyclodextrin solution, it will
Gross mass is equivalent to the tobacco absolute oil of beta-cyclodextrin mass percent 5% and spearmint oil is slowly added into beta-cyclodextrin solution
In, and 4h is stirred under conditions of 50 DEG C, 1200r/min, tobacco absolute oil and spearmint oil are included to the sky to beta-cyclodextrin
In chamber, inclusion solution is obtained；The spray-dried obtained flavouring additives of solution will be included.
By the flavouring additives of preparation, the tobacco slurry for being added to reconstituted tobacco chip base of manufacturing paper with pulp by the 10% of chip base oven dry weight
In, it is uniformly mixed, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Flavoring substances used in the present invention can also be alpha, beta-lonone, Megastigmatrienone, linalool, lactone substance
Deng.
Claims (3)
1. application of a kind of filler flavouring additives in cigarette, which is characterized in that the filler is with flavouring additives by following step
It is rapid to prepare：
(1) wall material that mass percent is 1%~30% is added in into heating stirring in distilled water；The wall material is α-ring paste
One or more of essence, beta-cyclodextrin, gamma-cyclodextrin, hydroxypropyl-β-cyclodextrin, Sulfobutyl ether β _ cyclodextrin；
(2) it will be equivalent to the solution that the flavoring substances that wall material mass percent is 1%~50% are slowly added into step (1) preparation
In, and 4h is stirred under conditions of 50 DEG C, 500~2000r/min, by flavoring substances inclusion into the cavity of wall material, wrapped
Close solution；The flavoring substances include tobacco absolute oil, tree moss absolute, Rosa Damascana, orange oil, peppermint oil, lemon oil, stay
Blue sesame oil, cognac green oil, dorinone, alpha, beta-lonone, Megastigmatrienone, linalool, isoamyl butyrate, lactone, β-
One or more of carypohyllene, leaf-alcohol, pungent certain herbaceous plants with big flowers acid glyceride；
(3) the spray-dried obtained solid powdery flavouring additives not soluble in water of solution will be included；
In the preparation process of cigarette paper or in papermaking-method reconstituted tobaccos preparation process, add flavouring additives as filler
Add.
A kind of 2. application of the filler flavouring additives according to claim 1 in cigarette, which is characterized in that flavouring additives
Feed postition is in the preparation process of cigarette paper, using papermaking process by flavouring additives, CaCO3, wood pulp cellulose, hemp it is fine
Dimension compares flavouring additives according to quality：CaCO3：Wood pulp cellulose：Hemp is (10~35%)：(5~40%)：(40~
75%)：(0~45%) ratio mixes, and is prepared into pulp suspension, then manufactures paper with pulp to obtain cigarette paper.
A kind of 3. application of the filler flavouring additives according to claim 1 in cigarette, which is characterized in that flavouring additives
Feed postition in papermaking-method reconstituted tobaccos preparation process is the tobacco that flavouring additives are added to reconstituted tobacco chip base of manufacturing paper with pulp
It in slurry and is uniformly mixed, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain；Flavouring additives account for the mass percent of chip base oven dry weight for 5~
20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610915735.6A CN106235378B (en) | 2016-10-20 | 2016-10-20 | A kind of application of filler flavouring additives in cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610915735.6A CN106235378B (en) | 2016-10-20 | 2016-10-20 | A kind of application of filler flavouring additives in cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106235378A CN106235378A (en) | 2016-12-21 |
| CN106235378B true CN106235378B (en) | 2018-06-01 |
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| CN201610915735.6A Active CN106235378B (en) | 2016-10-20 | 2016-10-20 | A kind of application of filler flavouring additives in cigarette |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108929776B (en) * | 2018-07-09 | 2021-04-30 | 浙江大学 | Long-acting fragrance-releasing nano particle and preparation method thereof |
| CN110710707A (en) * | 2018-07-11 | 2020-01-21 | 湖南中烟工业有限责任公司 | Method for preparing composite low-temperature cigarette with stable nicotine release |
| CN109797443B (en) * | 2019-01-30 | 2020-06-09 | 湖北中烟工业有限责任公司 | Preparation method and application of mint-flavor fiber felt used in non-combustible tobacco by heating |
| CN111838740B (en) * | 2020-09-09 | 2022-05-13 | 吉林烟草工业有限责任公司 | Method for improving aroma quality of paper-making reconstituted tobacco applied to papermaking forming section |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3550598A (en) * | 1967-08-15 | 1970-12-29 | James H Mcglumphy | Reconstituted tobacco containing adherent encapsulated flavors and other matter |
| CN103362033A (en) * | 2013-07-31 | 2013-10-23 | 广州市澳键丰泽生物科技有限公司 | Cigarette paper |
| CN103396886A (en) * | 2013-07-26 | 2013-11-20 | 湖北中烟工业有限责任公司 | Compound microcapsule wall material and application thereof in essence microcapsules for cigarettes |
| CN103451999A (en) * | 2013-09-06 | 2013-12-18 | 湖北中烟工业有限责任公司 | Method for preparing colorful recombined tobacco leaf paper by microencapsulation of coating liquid |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103711029A (en) * | 2013-12-20 | 2014-04-09 | 华南理工大学 | Method for manufacturing aroma-increasing moisture retention cigarette paper |
| CN105661626A (en) * | 2016-03-25 | 2016-06-15 | 河南中烟工业有限责任公司 | Composite biological agent microcapsule capable of improving sensory quality of tobacco |
| CN105925375A (en) * | 2016-06-23 | 2016-09-07 | 云南中烟工业有限责任公司 | Compound essence for cigarette as well as preparation method and purpose thereof |
-
2016
- 2016-10-20 CN CN201610915735.6A patent/CN106235378B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3550598A (en) * | 1967-08-15 | 1970-12-29 | James H Mcglumphy | Reconstituted tobacco containing adherent encapsulated flavors and other matter |
| CN103396886A (en) * | 2013-07-26 | 2013-11-20 | 湖北中烟工业有限责任公司 | Compound microcapsule wall material and application thereof in essence microcapsules for cigarettes |
| CN103362033A (en) * | 2013-07-31 | 2013-10-23 | 广州市澳键丰泽生物科技有限公司 | Cigarette paper |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103451999A (en) * | 2013-09-06 | 2013-12-18 | 湖北中烟工业有限责任公司 | Method for preparing colorful recombined tobacco leaf paper by microencapsulation of coating liquid |
| CN103711029A (en) * | 2013-12-20 | 2014-04-09 | 华南理工大学 | Method for manufacturing aroma-increasing moisture retention cigarette paper |
| CN105661626A (en) * | 2016-03-25 | 2016-06-15 | 河南中烟工业有限责任公司 | Composite biological agent microcapsule capable of improving sensory quality of tobacco |
| CN105925375A (en) * | 2016-06-23 | 2016-09-07 | 云南中烟工业有限责任公司 | Compound essence for cigarette as well as preparation method and purpose thereof |
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| CN106235378A (en) | 2016-12-21 |
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