CN105925375A - Compound essence for cigarette as well as preparation method and purpose thereof - Google Patents
Compound essence for cigarette as well as preparation method and purpose thereof Download PDFInfo
- Publication number
- CN105925375A CN105925375A CN201610462742.5A CN201610462742A CN105925375A CN 105925375 A CN105925375 A CN 105925375A CN 201610462742 A CN201610462742 A CN 201610462742A CN 105925375 A CN105925375 A CN 105925375A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- wall material
- tobacco
- essence
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to the technical field of application of compound essences for cigarettes to cigarette fields, and discloses a compound essence for a cigarette. The compound essence for the cigarette comprises a wall material, a core material and an emulsifying agent, wherein the wall material is a mixture of sodium alginate and guar gum; the core material is a mixture of neohesperidin dihydrochalcone, leaf alcohol and leaf alcohol glycoside; the emulsifying agent is propylene glycol fatty acid ester. The invention also discloses a preparation method of the compound essence for the cigarette and a purpose of the compound essence for the cigarette for increasing the aroma of the cigarette; the compound essence for the cigarette can be used for restraining the biting smell of smoke and keeping the stability and the durability of the aroma of the cigarette, and the uniformity and the consistency, with the passage of time, of the release of the aroma.
Description
Technical field
The invention belongs to the technical field that compound flavouring essence for tobacco is applied in cigarette field, be specifically related to a kind of compound
Flavouring essence for tobacco, its preparation method and the application in cigarette.
Background technology
Tobacco product generally will use perfuming method, reaches to improve cigarette fragrance characteristic, cover miscellaneous taste and imparting
The purpose of cigarette individual style, thus become a part indispensable in tobacco industry.Updating formula,
While developing novel flavouring essence for tobacco, the stability of cigarette flavor and persistent problem, Research Center is looked forward in one's power especially
Industry scientific research personnel's focus of attention.The boiling point of most of perfume materials is relatively low, highly volatile, during long-term storage
Loss is serious, and owing to cigarette belongs to the handling characteristics that high temperature burns and sucks, the flue gas of heat can make the spices in cigarette carry
Front release, causes early stage strong, and what the later stage was boring releases fragrant non-uniform phenomenon, reduces product consumption quality.
Microcapsules technology is to improve the important means of essence stability, uses naturally occurring or synthetic macromolecular compound
Constitute continuous film (wall or foreign minister) completely to be coated with by perfume material to be protected (core or internal phase), can
Effectively to stop the volatilization of fragrant composition to be scattered and disappeared, isolation simultaneously contacts with extraneous, also slow down chemical change and causes
Rotten, improve the stability of fragrance material.But microcapsule embedded essence product, burning and sucking cigarette
Cheng Zhong, owing to flue-gas temperature is higher, still can not prevent the release in advance of fragrance component, releases fragrant homogeneity question also
It is to solve.
Summary of the invention
The present invention, for overcoming loss in fragrance material high temperature working processes serious, causes releasing fragrant non-uniform phenomenon, very
Lose fragrance to during storing because of volatilization, or unstable chemcial property is easy to be oxidized rotten and propose, this
Invention uses compound flavouring essence for tobacco, and for cigarette flavouring, suppression flue gas acid, and cigarette can be kept fragrant
The stability of gas, persistence and/or the uniformity consistency of fragrance release.
A first aspect of the present invention relates to a kind of compound flavouring essence for tobacco, including wall material, core and emulsifying agent；
Described wall material is the mixture of sodium alginate and guar gum；Described core be neohesperidin dihydrochalcone,
Leaf-alcohol and the mixture of leaf-alcohol glucosides；Described emulsifying agent is methyl glycol fatty acid ester.
In the preferred version of a first aspect of the present invention, described sodium alginate accounts for the 40wt%～50 of described wall material
Wt%, described guar gum accounts for 50wt%～60wt% of described wall material；
Described neohesperidin dihydrochalcone is 1～3 weight portions, and leaf-alcohol is 5～15 weight portions, and leaf-alcohol glucosides is
2～4 weight portions；
Described wall material is 1:1～1:1.5 with the weight ratio of described core.
A second aspect of the present invention relates to the preparation method of described compound flavouring essence for tobacco, comprises the steps:
(1) it is mixed to get mixture after weighing described wall material, described core and described emulsifying agent in proportion；Institute
The amount stating emulsifying agent accounts for wall material and 1.0wt%～2.0wt% of core gross weight；
(2) add water stirring by the mixture that step (1) obtains, and is configured to 30wt%～40wt% aqueous dispersions；
(3) aqueous dispersions step (2) obtained homogeneous under 60～70 DEG C and 25～35MPa, obtains all
Even aqueous dispersions；
(4) uniform aqueous dispersions step (3) obtained is spray-dried and i.e. obtains described composite smoke perfume
Essence.Preferably, the EAT of described spray drying is 150～250 DEG C, and outlet temperature is 60～90 DEG C
A third aspect of the present invention relates to described compound flavouring essence for tobacco for the purposes to cigarette flavouring.
A fourth aspect of the present invention relates to described compound flavouring essence for tobacco for suppressing flue gas acid and keeping volume
The stability of cigarette fragrance, persistence and/or the purposes of fragrance release uniformity consistency in time.
The beneficial effects of the present invention is:
1, using the stable type flavouring essence for tobacco that the present invention produces, during the long-term storage of cigarette, fragrance is held
Continuous permanent, there is not the change of perceptibility, good stability in flavouring essence quality.During burning and sucking, from start to
Terminating, fragrance is the most uniform and stable, releases fragrant uniform.And fragrance is waved during the cigarette adding common essence is deposited
Send out loss, occur flavouring essence quality to deteriorate, during burning and sucking, owing to flue-gas temperature is high, make essence quickly volatilize,
Give off a strong fragrance before formation, after the boring phenomenon of fragrance.
2, the neohesperidin dihydrochalcone that the present invention adds, is a kind of to have debitter and flavor improvement
Functional sweetener, uses in cigarette, can suppress the acid of flue gas, increase taste of the sweet end, improve
Flue gas quality.
3, the leaf-alcohol that the present invention adds, has the blue or green fragrant of strong fresh blade of grass, and fresh tea leaf and apple green grass or young crops are fragrant,
Extension is strong, has special herbal and leaf smell after dilution, and taste is gentle, belongs to delicate fragrance type rare spice,
It is mainly used as the front taste agent of various floral type tobacco, it is provided that fresh top note.
4, the present invention uses neohesperidin dihydrochalcone and leaf-alcohol, leaf-alcohol glucosides compound use, and uses
Microcapsule embedded it is added in cigarette tobacco as stability fragrance precursor stable composition technology, can be in combustion
Smell delicate fragrance during suction, no impurity taste, most importantly inhibit flue gas acid, and long-term storage cigarette fragrance is steady
Fixed, when burning and sucking, fragrance release is uniformly.The present invention will set up Premium Brands to improving cigarette quality, have important
Meaning.
Accompanying drawing explanation
Nothing.
Detailed description of the invention
The compound flavouring essence for tobacco using the present invention adds in cigarette shreds, with the cigarette adding common flavouring essence for tobacco
Comparing, choose 6 professionals and carry out scoring of smokeing panel test, appraisal result is as shown in table 2, standards of grading such as table 1
Shown in.
Table 1 Score index and standards of grading
Table 2 appraisal result
As can be seen from Table 2, compared with the control, the present invention is combined the perfume (or spice) that flavouring essence for tobacco adds in cigarette shreds
Gas value is high, perfume quantity foot, and fragrance is pure, it is suppressed that acid, has sweet rose fragrance.Burn and suck process
In, from lighting cigarette suction, to last after-flame, fragrance is persistently uniform, and each item rating is superior to control group, takes
Obtained unexpected effect.
Using the compound flavouring essence for tobacco of the present invention, during cigarette long-term storage, fragrance is still stable lasting,
The cigarette of long-term storage, during burning and sucking, fragrance is uniform and stable from the beginning to the end, releases fragrant uniform.And common cigarette
With essence, then volatile aroma loss during cigarette is deposited, forms above fragrance dense during burning and sucking, after
The phenomenon that fragrance is boring, and during burning and sucking, owing to flue-gas temperature is high, make essence volatilization loss fast, also deposit
Dense at above fragrance, after the boring phenomenon of fragrance.
Use the compound flavouring essence for tobacco of the present invention, compound essence ratio uniform can be made, also to a certain degree improving
The stability of essence.Significantly improve the aroma quality of cigarette.The present invention will promote improving cigarette quality
The development of tobacco business, significant.
Claims (5)
1. a compound flavouring essence for tobacco, including wall material and core；It is characterized in that, described wall material is alginic acid
Sodium and the mixture of guar gum；Described core is neohesperidin dihydrochalcone, leaf-alcohol and the mixing of leaf-alcohol glucosides
Thing.
Compound flavouring essence for tobacco the most according to claim 1, it is characterised in that described sodium alginate accounts for described
40wt%～50wt% of wall material, described guar gum accounts for 50wt%～60wt% of described wall material；
Described neohesperidin dihydrochalcone is 1～3 weight portions, and leaf-alcohol is 5～15 weight portions, and leaf-alcohol glucosides is
2～4 weight portions；
Described wall material is 1:1～1:1.5 with the weight ratio of described core.
The preparation method of a kind of compound flavouring essence for tobacco the most according to claim 2, it is characterised in that include as
Lower step:
(1) weigh described wall material and described core in proportion, and be mixed to get mixture after emulsifying agent, its
Described in emulsifying agent be methyl glycol fatty acid ester, the amount of emulsifying agent account for wall material and the 1.0wt% of core gross weight～
2.0wt%；
(2) add water stirring by the mixture that step (1) obtains, and is configured to 30wt%～40wt% aqueous dispersions；
(3) aqueous dispersions step (2) obtained homogeneous under 60～70 DEG C and 25～35MPa, obtains all
Even aqueous dispersions；
(4) uniform aqueous dispersions step (3) obtained is spray-dried and i.e. obtains described composite smoke perfume
Essence.
Compound flavouring essence for tobacco the most according to claim 1 is for the purposes of cigarette flavouring.
Compound flavouring essence for tobacco the most according to claim 1 is used for suppressing flue gas acid and keeping cigarette fragrant
The stability of gas, persistence and/or the purposes of fragrance release uniformity consistency in time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462742.5A CN105925375B (en) | 2016-06-23 | 2016-06-23 | Composite tobacco essence, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462742.5A CN105925375B (en) | 2016-06-23 | 2016-06-23 | Composite tobacco essence, preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105925375A true CN105925375A (en) | 2016-09-07 |
| CN105925375B CN105925375B (en) | 2020-04-03 |
Family
ID=56831238
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610462742.5A Active CN105925375B (en) | 2016-06-23 | 2016-06-23 | Composite tobacco essence, preparation method and application thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN105925375B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106235378A (en) * | 2016-10-20 | 2016-12-21 | 云南瑞升烟草技术（集团）有限公司 | The preparation method of a kind of filler flavouring auxiliary agent and the application in Medicated cigarette thereof |
| CN106565450A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Novel chalcone compound extracted from Campanumoea javanica, and preparation method and application thereof |
| CN106565449A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Preparation method and applications of chalcone compound capable of increasing cigarette smoking sweetness |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408620A (en) * | 2013-08-15 | 2013-11-27 | 西南化工研究设计院有限公司 | Neohesperidin synthesis technology |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
-
2016
- 2016-06-23 CN CN201610462742.5A patent/CN105925375B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103408620A (en) * | 2013-08-15 | 2013-11-27 | 西南化工研究设计院有限公司 | Neohesperidin synthesis technology |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106565450A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Novel chalcone compound extracted from Campanumoea javanica, and preparation method and application thereof |
| CN106565449A (en) * | 2016-10-14 | 2017-04-19 | 云南中烟工业有限责任公司 | Preparation method and applications of chalcone compound capable of increasing cigarette smoking sweetness |
| CN106565450B (en) * | 2016-10-14 | 2019-02-19 | 云南中烟工业有限责任公司 | A kind of novel Chalcone Compounds, preparation method and the usage extracted from Bai Yun Shen |
| CN106565449B (en) * | 2016-10-14 | 2019-02-19 | 云南中烟工业有限责任公司 | A kind of preparation method and application for the chalcone compounds can increase cigarette smoking sweet tea sense |
| CN106235378A (en) * | 2016-10-20 | 2016-12-21 | 云南瑞升烟草技术（集团）有限公司 | The preparation method of a kind of filler flavouring auxiliary agent and the application in Medicated cigarette thereof |
| CN106235378B (en) * | 2016-10-20 | 2018-06-01 | 云南瑞升烟草技术（集团）有限公司 | A kind of application of filler flavouring additives in cigarette |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105925375B (en) | 2020-04-03 |
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