CN106235378A - The preparation method of a kind of filler flavouring auxiliary agent and the application in Medicated cigarette thereof - Google Patents
The preparation method of a kind of filler flavouring auxiliary agent and the application in Medicated cigarette thereof Download PDFInfo
- Publication number
- CN106235378A CN106235378A CN201610915735.6A CN201610915735A CN106235378A CN 106235378 A CN106235378 A CN 106235378A CN 201610915735 A CN201610915735 A CN 201610915735A CN 106235378 A CN106235378 A CN 106235378A
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- CN
- China
- Prior art keywords
- auxiliary agent
- flavouring auxiliary
- filler
- flavouring
- paper
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
The preparation method of a kind of filler flavouring auxiliary agent and the application in Medicated cigarette thereof, add heated and stirred in distilled water by the wall material of 0.1%~30% by mass percentage, obtain wall material solution;The flavoring substances that will be equivalent to wall material mass percent 1%~50% is slowly added in wall material solution, and stirs 4h under conditions of 50 DEG C, 500~2000r/min, by flavoring substances inclusion to the cavity of wall material, obtains inclusion solution;By spray-dried for inclusion solution prepared flavouring auxiliary agent.Flavoring substances is prepared flavouring auxiliary agent by embedding by the present invention, and production technology is simple, it is easy to promote.Flavouring auxiliary agent is applied in Medicated cigarette by the present invention with the form of filler, can reduce the volatility of flavoring substances, and when making flue gas aspirate, front and back end concentration is more uniform unanimously, improves the suction quality of Medicated cigarette.
Description
Technical field
The invention belongs to Medicated cigarette packing technique field, be specifically related to the preparation of filler flavouring auxiliary agent and in Medicated cigarette
Application.
Background technology
Flavouring humectation is an up the key technology of cigarette quality, is also one of nine key special subjects determining of industry.Medicated cigarette
Type of aroma and style decide class and the grade of Medicated cigarette product, Medicated cigarette " flavouring " class essence and flavoring agent thing to a certain extent
Matter, can make cigarette flavor amount get a promotion, Medicated cigarette note is increased or abundant, and the quality of Medicated cigarette is produced directly impact.
But spices and essence material has volatility mostly, exist high volatility, the holdup time is short, the shelf-life is short, essence release inequality
The problem such as even, the drawback that before and after making cigarette smoke release concentration exist, section is inconsistent, thus affect the raising of cigarette smoking quality
And the range of application in Medicated cigarette.
Use microcapsule embedded technology to be embedded in the cavity of wall material by essence spice for cigarette, protect the same of this material
Time also can improve its stability, reduce volatility, and make it slowly release fragrance under Medicated cigarette burns and sucks state or External Force Acting
Composition, flavouring is effective, protect perfume persistently, discharge uniform effect to make essence and flavoring agent material reach, and gives Medicated cigarette and preferably aspirates
Sensory experience.Filler can improve cigarette paper, the breathability of reconstituted tobacco chip base, opacity, whiteness, tensile property and even
The indexs such as degree.By can also impart to its certain functional character to filler modified.The China of Publication No. CN103711029A
Patent describes a kind of loaded modified CaCO3 filler, uses common papermaking process to prepare flavouring humectation cigarette paper, makes fragrance alcohol
Thick, lasting, improve the quality of Medicated cigarette.Its filler modified method of described CaCO3 is to be carried on by mulser by flavor components
Modified CaCO3Filling surface, but flavoring substances is not played protection and slow releasing function.In Publication No. CN103362033A
State's patent discloses a kind of cigarette paper, and its described cigarette paper is will to cause the microcapsule that fragrant extract is prepared as having slow-release function,
Then add during two pressures of Medicated cigarette copy paper and obtain.Wherein in microcapsule, flavor matter accounts for the 5% of beta-schardinger dextrin-quality, and
0.1% micro encapsulation causes fragrant mixed liquor interpolation quality and only accounts for the 0.1% of cigarette paper quality.Its described cause perfume (or spice) extract is at Medicated cigarette
Interpolation in paper is range-restricted relatively big, and the allotment that may affect flavouring formula uses.
Existing Medicated cigarette filler aromatizing technology application effect is undesirable, and microcapsule perfuming technology is at cigarette paper, reconstituted tobacco
In research less.
Summary of the invention
It is an object of the invention to make up the deficiencies in the prior art, improve the use limitation of flavoring substances, it is provided that Yi Zhongjuan
The cigarette preparation method of flavouring filler and the application in Medicated cigarette.
For achieving the above object, the present invention adopts the following technical scheme that
The preparation method of a kind of filler flavouring auxiliary agent, comprises the steps:
(1) by mass percentage the wall material of 0.1%~30% is added heated and stirred in distilled water, obtain wall material solution;
(2) flavoring substances that will be equivalent to wall material mass percent 1%~50% is slowly added in wall material solution, and
Stir 4h under conditions of 50 DEG C, 500~2000r/min, by flavoring substances inclusion to the cavity of wall material, obtain inclusion solution;
(3) by spray-dried for inclusion solution prepared flavouring auxiliary agent.
Wall material described in above-mentioned steps (1) is alpha-cyclodextrin, beta-schardinger dextrin-, gamma-cyclodextrin, HP-β-CD, sulphur
One or more in fourth group-beta-cyclodextrin, resin and silica gel.Flavoring substances described in step (2) includes but not limited to Nicotiana tabacum L.
Class absolute oil, senior this perfume of Nicotiana tabacum L., tree moss absolute, Flos Rosae Rugosae quintessence oil, oleum Citri sinensis, Oleum menthae, Fructus Citri Limoniae oil, Oleum Menthae Rotundifoliae, cognac are green
Oil, dorinone, alpha, beta-lonone, Megastigmatrienone, linalool, isoamyl butyrate, lactone, β-caryophyllene, folic alcohol, Xin Kui
One or more in acid glyceride.Described flavouring auxiliary agent is water-fast solid powdery material.
The filler flavouring auxiliary agent that the present invention prepares application in Medicated cigarette, is in the preparation process of cigarette paper
Or in papermaking-method reconstituted tobaccos preparation process, flavouring auxiliary agent is added as filler.Described cigarette paper includes Medicated cigarette
Paper, filter stick formation paper, cigarette tipping paper.
Flavouring auxiliary agent feed postition in cigarette paper preparation process can be use papermaking process by flavouring auxiliary agent,
CaCO3, wood pulp cellulose, hemp according to quality than flavouring auxiliary agent: CaCO3: wood pulp cellulose: hemp is (10~35%):
(5~40%): (40~75%): (0~45%) ratio mixes, and is prepared as pulp suspension, and then manufacturing paper with pulp obtains cigarette paper.Increase
Fragrant auxiliary agent feed postition in papermaking-method reconstituted tobaccos preparation process can also reproduce cigarette for adding to manufacture paper with pulp by flavouring auxiliary agent
In the tobacco slurry of blade base and mix homogeneously, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain;Flavouring auxiliary agent accounts for the matter of chip base oven dry weight
Amount percentage ratio is 5~20%.
Compared with prior art, the invention have the advantages that
(1) by embedding, flavoring substances being prepared flavouring auxiliary agent, production technology is simple, it is easy to promote;
(2) comparing with traditional perfuming mode, flavouring auxiliary agent is applied in Medicated cigarette by the present invention with the form of filler, permissible
Reducing the volatility of flavoring substances, when making flue gas aspirate, front and back end concentration is more uniform unanimously, improves the suction quality of Medicated cigarette;
(3) by preparing the flavouring auxiliary agent of filler, flavouring auxiliary agent can be expanded in cigarette paper, reconstituted tobacco
Range of application, the filler for cigarette paper, reconstituted tobacco provides new form and new developing direction.
Detailed description of the invention
For being more fully understood that the present invention, below in conjunction with embodiment, the invention will be further described, but the reality of the present invention
The mode of executing is not limited to this.
Implement row 1
By mass percentage the beta-schardinger dextrin-of 2% is added heated and stirred in distilled water, obtain beta-schardinger dextrin-solution, by phase
In the Oleum menthae in beta-schardinger dextrin-mass percent 1% is slowly added into beta-schardinger dextrin-solution, and at 50 DEG C, 800r/min
Under the conditions of stir 4h, by flavoring substances Oleum menthae inclusion to the cavity of beta-schardinger dextrin-, obtain inclusion solution;By inclusion solution warp
It is spray-dried and prepares water-fast powder flavouring auxiliary agent.
The flavouring auxiliary agent of preparation uses regular-size cigarette paper papermaking process, by flavouring auxiliary agent, CaCO3, wood pulp cellulose, Fructus Cannabis fine
Tie up according to quality than flavouring auxiliary agent: CaCO3: wood pulp cellulose: hemp=15%:10%:40%:45% is prepared as paper pulp and hangs
Supernatant liquid, prepared cigarette paper of then manufacturing paper with pulp.
Implement row 2
By gamma-cyclodextrin heated and stirred in distilled water that mass percent is 3%, obtain gamma-cyclodextrin solution;By phase
When in the oleum Citri sinensis of gamma-cyclodextrin mass percent 25%, isoamyl butyrate (quality is than oleum Citri sinensis: isoamyl butyrate=80%:
20%) be slowly added in gamma-cyclodextrin solution, and 50 DEG C, stir 4h under conditions of 1000r/min, by oleum Citri sinensis and fourth
Isoamyl valerate inclusion, in the cavity of gamma-cyclodextrin, obtains inclusion solution;By spray-dried for inclusion solution prepared water insoluble
Flavouring auxiliary agent.
The flavouring auxiliary agent of preparation uses regular-size cigarette paper papermaking process, by flavouring auxiliary agent, CaCO3, wood pulp cellulose, Fructus Cannabis fine
Dimension is prepared as pulp suspension according to mass ratio 10%:5%:75%:10%, and then manufacturing paper with pulp obtains cigarette paper.
Implement row 3
By HP-β-CD heated and stirred in distilled water that mass percent is 30%, obtain hydroxy propyl-Beta-ring
Dextrin solution;(Nicotiana tabacum L. is senior to will be equivalent to senior perfume (or spice) of Nicotiana tabacum L. of HP-β-CD mass percent 20% and Fructus Citri Limoniae oil
This perfume: the mass ratio of Fructus Citri Limoniae oil is 80%:20%) it is slowly added in HP-β-CD solution, and at 50 DEG C, 500r/
Stirring 4h under conditions of min, obtain inclusion solution, reaction prepares flavouring auxiliary agent through spray drying after terminating.
By the flavouring auxiliary agent of preparation, by the 5% of the chip base oven dry weight tobacco slurry adding reconstituted tobacco chip base of manufacturing paper with pulp to
In, mix homogeneously, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Implement row 4
By resin heated and stirred in distilled water that mass percent is 0.1%, obtain resin solution;Will be equivalent to resin
Senior this perfume of Nicotiana tabacum L. of mass percent 8%, tree moss absolute, Flos Rosae Rugosae quintessence oil, pungent certain herbaceous plants with big flowers acid glyceride 20%:10% in mass ratio:
10%:60% is slowly added in resin solution, and 50 DEG C, stir 4h under conditions of 2000r/min, obtain inclusion solution,
Reaction prepares flavouring auxiliary agent through spray drying after terminating.
The flavouring auxiliary agent of preparation uses regular-size cigarette paper papermaking process, by flavouring auxiliary agent, CaCO3, wood pulp cellulose, Fructus Cannabis fine
Dimension is prepared as pulp suspension according to mass ratio 35%:10%:45%:10%, manufactures paper with pulp and obtains cigarette tipping paper.
Implement row 5
By Sulfobutyl ether β _ cyclodextrin heated and stirred in distilled water that mass percent is 20%, obtain sulphur butyl-β-ring
Dextrin solution;Will be equivalent to the cognac green oil of Sulfobutyl ether β _ cyclodextrin mass percent 50%, folic alcohol, pungent certain herbaceous plants with big flowers acid glyceride
It is slowly added in Sulfobutyl ether β _ cyclodextrin solution after the mixing of 40%:10%:50% in mass ratio, and at 50 DEG C, 1000r/
Stir 4h under conditions of min, obtain inclusion solution;Reaction prepares flavouring auxiliary agent through spray drying after terminating.
By the flavouring auxiliary agent of preparation, by the 20% of the chip base oven dry weight tobacco slurry adding reconstituted tobacco chip base of manufacturing paper with pulp to
In, mix homogeneously, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Implement row 6
By alpha-cyclodextrin that mass percent is 5%, silica gel heated and stirred in distilled water of 10%, obtain alpha-cyclodextrin
With the mixed solution of silica gel, will be equivalent to alpha-cyclodextrin and the dorinone of silica gel gross mass percentage ratio 20%, β-caryophyllene by
Be slowly added in silica gel solution after mass ratio 50%:50% mixing, and 50 DEG C, stir 4h under conditions of 1500r/min,
To inclusion solution;Reaction prepares flavouring auxiliary agent through spray drying after terminating.
The flavouring auxiliary agent of preparation uses regular-size cigarette paper papermaking process, by flavouring auxiliary agent, CaCO3, wood pulp cellulose is according to matter
Amount is prepared as pulp suspension than 10%:40%:50%, manufactures paper with pulp and obtains filter stick formation paper.
Implement row 7
By mass percentage the beta-schardinger dextrin-of 10% is added heated and stirred in distilled water, obtain beta-schardinger dextrin-solution, will
Gross mass is equivalent to the tobacco absolute oil of beta-schardinger dextrin-mass percent 5% and Oleum Menthae Rotundifoliae is slowly added into beta-schardinger dextrin-solution
In, and 50 DEG C, stir 4h under conditions of 1200r/min, by the sky of tobacco absolute oil and Oleum Menthae Rotundifoliae inclusion to beta-schardinger dextrin-
In chamber, obtain inclusion solution;By spray-dried for inclusion solution prepared flavouring auxiliary agent.
By the flavouring auxiliary agent of preparation, by the 10% of the chip base oven dry weight tobacco slurry adding reconstituted tobacco chip base of manufacturing paper with pulp to
In, mix homogeneously, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain.
Flavoring substances used by the present invention can also is that alpha, beta-lonone, Megastigmatrienone, linalool, lactone material
Deng.
Claims (8)
1. the filler preparation method of flavouring auxiliary agent, it is characterised in that comprise the steps:
(1) by mass percentage the wall material of 0.1%~30% is added heated and stirred in distilled water, obtain wall material solution;
(2) flavoring substances that will be equivalent to wall material mass percent 1%~50% is slowly added in wall material solution, and 50
DEG C, 500~2000r/min under conditions of stir 4h, by flavoring substances inclusion to the cavity of wall material, obtain inclusion solution;
(3) by spray-dried for inclusion solution prepared flavouring auxiliary agent.
The preparation method of a kind of filler flavouring auxiliary agent the most according to claim 1, it is characterised in that above-mentioned steps (1)
Described wall material is alpha-cyclodextrin, beta-schardinger dextrin-, gamma-cyclodextrin, HP-β-CD, Sulfobutyl ether β _ cyclodextrin, resin
With one or more in silica gel.
The preparation method of a kind of filler flavouring auxiliary agent the most according to claim 1, it is characterised in that above-mentioned steps (2)
Described flavoring substances includes but not limited to tobacco absolute oil, senior this perfume of Nicotiana tabacum L., tree moss absolute, Flos Rosae Rugosae quintessence oil, oleum Citri sinensis, thin
Lotus oil, Fructus Citri Limoniae oil, Oleum Menthae Rotundifoliae, cognac green oil, dorinone, alpha, beta-lonone, Megastigmatrienone, linalool, butanoic acid are different
One or more in pentyl ester, lactone, β-caryophyllene, folic alcohol, pungent certain herbaceous plants with big flowers acid glyceride.
The preparation method of a kind of filler flavouring auxiliary agent the most according to claim 1, it is characterised in that described flavouring auxiliary agent
For water-fast solid powdery material.
5. the filler flavouring auxiliary agent prepared such as any one of Claims 1 to 4 application in Medicated cigarette, its feature exists
In, in the preparation process of cigarette paper or in papermaking-method reconstituted tobaccos preparation process, flavouring auxiliary agent is added as filler
Add.
The filler flavouring auxiliary agent the most according to claim 5 application in Medicated cigarette, it is characterised in that described Medicated cigarette is used
Paper includes cigarette paper, filter stick formation paper, cigarette tipping paper.
7. according to the flavouring auxiliary agent application in Medicated cigarette of the filler described in claim 5 or 6, it is characterised in that flavouring auxiliary agent
Feed postition in cigarette paper preparation process is, uses papermaking process by flavouring auxiliary agent, CaCO3, wood pulp cellulose, Fructus Cannabis fine
Tie up according to quality than flavouring auxiliary agent: CaCO3: wood pulp cellulose: hemp is (10~35%): (5~40%): (40~
75%): (0~45%) ratio mixes, and is prepared as pulp suspension, and then manufacturing paper with pulp obtains cigarette paper.
The filler flavouring auxiliary agent the most according to claim 7 application in Medicated cigarette, it is characterised in that flavouring auxiliary agent is being made
Feed postition in paper method reconstituted tobacco preparation process is that flavouring auxiliary agent adds to the tobacco slurry of reconstituted tobacco chip base of manufacturing paper with pulp
In and mix homogeneously, papermaking-method reconstituted tobaccos of manufacturing paper with pulp to obtain;Flavouring auxiliary agent account for the mass percent of chip base oven dry weight be 5~
20%.
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CN201610915735.6A CN106235378B (en) | 2016-10-20 | 2016-10-20 | A kind of application of filler flavouring additives in cigarette |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108929776A (en) * | 2018-07-09 | 2018-12-04 | 浙江大学 | A kind of long-acting incense-releasing nanoparticle and preparation method thereof |
CN109797443A (en) * | 2019-01-30 | 2019-05-24 | 湖北中烟工业有限责任公司 | For heating the preparation method and application of the mint aroma fibrofelt in not burning tobacco |
CN110710707A (en) * | 2018-07-11 | 2020-01-21 | 湖南中烟工业有限责任公司 | Method for preparing composite low-temperature cigarette with stable nicotine release |
CN111838740A (en) * | 2020-09-09 | 2020-10-30 | 吉林烟草工业有限责任公司 | Method for improving aroma quality of paper-making reconstituted tobacco applied to papermaking forming section |
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CN103711029A (en) * | 2013-12-20 | 2014-04-09 | 华南理工大学 | Method for manufacturing aroma-increasing moisture retention cigarette paper |
CN105661626A (en) * | 2016-03-25 | 2016-06-15 | 河南中烟工业有限责任公司 | Composite biological agent microcapsule capable of improving sensory quality of tobacco |
CN105925375A (en) * | 2016-06-23 | 2016-09-07 | 云南中烟工业有限责任公司 | Compound essence for cigarette as well as preparation method and purpose thereof |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108929776A (en) * | 2018-07-09 | 2018-12-04 | 浙江大学 | A kind of long-acting incense-releasing nanoparticle and preparation method thereof |
CN108929776B (en) * | 2018-07-09 | 2021-04-30 | 浙江大学 | Long-acting fragrance-releasing nano particle and preparation method thereof |
CN110710707A (en) * | 2018-07-11 | 2020-01-21 | 湖南中烟工业有限责任公司 | Method for preparing composite low-temperature cigarette with stable nicotine release |
CN109797443A (en) * | 2019-01-30 | 2019-05-24 | 湖北中烟工业有限责任公司 | For heating the preparation method and application of the mint aroma fibrofelt in not burning tobacco |
CN111838740A (en) * | 2020-09-09 | 2020-10-30 | 吉林烟草工业有限责任公司 | Method for improving aroma quality of paper-making reconstituted tobacco applied to papermaking forming section |
CN111838740B (en) * | 2020-09-09 | 2022-05-13 | 吉林烟草工业有限责任公司 | Method for improving aroma quality of paper-making reconstituted tobacco applied to papermaking forming section |
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