CN107419593A - A kind of sweet odor type cigarette paper and preparation method thereof - Google Patents

A kind of sweet odor type cigarette paper and preparation method thereof Download PDF

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Publication number
CN107419593A
CN107419593A CN201710943652.2A CN201710943652A CN107419593A CN 107419593 A CN107419593 A CN 107419593A CN 201710943652 A CN201710943652 A CN 201710943652A CN 107419593 A CN107419593 A CN 107419593A
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CN
China
Prior art keywords
porous
cigarette paper
odor type
parts
type cigarette
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Pending
Application number
CN201710943652.2A
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Chinese (zh)
Inventor
倪朝敏
王晓辉
李雪梅
徐济仓
李松
伊奥尔
王迪
李迎华
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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Filing date
Publication date
Application filed by China Tobacco Yunnan Industrial Co Ltd filed Critical China Tobacco Yunnan Industrial Co Ltd
Priority to CN201710943652.2A priority Critical patent/CN107419593A/en
Publication of CN107419593A publication Critical patent/CN107419593A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/21Macromolecular organic compounds of natural origin; Derivatives thereof
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63Inorganic compounds
    • D21H17/67Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/675Oxides, hydroxides or carbonates
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H27/00Special paper not otherwise provided for, e.g. made by multi-step processes
    • D21H27/10Packing paper

Abstract

The invention discloses a kind of sweet odor type cigarette paper and preparation method thereof.The present invention chooses porous material as fragrance carrier, take the mode of vacuum perfuming, by the propolis after atomization, honey extract spice solution appendix into porous material cavity, then the ethanol solution of the ethyl cellulose by atomization is sprayed in porous material particle surface again, film layer is formed after solvent volatilization completely, obtains the powder material rich in spices.The porous material of appendix spices is added in cigarette paper in a manner of filler, sweet odor type cigarette paper is made, the loss and volatilization of fragrance matter in spices can be efficiently reduced, the sweet sense of cigarette smoke can be improved simultaneously, promote the production of body fluid sense and comfortableness and fragrance it is rich, and can also be consistent the style and features of sucking of section before and after cigarette.

Description

A kind of sweet odor type cigarette paper and preparation method thereof
Technical field
The invention belongs to cigarette paper production technical field, and in particular to it is a kind of with rich in propolis, honey extract it is porous Material is sweet odor type cigarette paper of filler and preparation method thereof.
Background technology
Cigarette paper is also referred to as obbbin, for wrapping up cigarette shreds, compared with other cigarette supplementaries, it is maximum the characteristics of be exactly to participate in Pipe tobacco burns, and physical change not only occurs during cigarette smoking in it, and chemical change occurs, to cigarette smoking product Matter has a great influence, it is possible thereby to an important composition of cigarette leaf group is regarded as, so shadow of the cigarette paper for cigarette odor-absorbing Sound has critical effect.
Flavouring humectation is carried out to cigarette by essence and flavoring agent, the suction quality of cigarette can be effectively lifted, except pipe tobacco Outside perfuming and filter stick perfuming, cigarette paper perfuming or load perfume are again a kind of relatively effective technological means.Such as:Patent of invention 《A kind of delicate fragrance type cigarette paper and preparation method thereof》(CN105200857A)Disclosed cigarette paper is that delicate fragrance type is added in paper pulp Microcapsules, obtained cigarette paper can effectively enrich cigarette flavor, increase delicate fragrance fragrance;Patent of invention《Contain vanilla High-grade cigarette paper of extract and preparation method thereof》(CN103343487A)Disclosed cigarette paper is that fragrant pod is added in coating fluid Blue extract, obtained cigarette paper can effectively augment sweetness cream it is fragrant, fragrant and sweet, beans are fragrant, strengthen cigarette perfume;Patent of invention 《A kind of preparation of peppermint type cigarette tissue》(CN101487203A)Disclosed cigarette paper selection addition molecule encapsulated menthol green wood Material, obtained cigarette paper can ensure that peppermint refrigerant sense is remained the same from beginning to end when cigarette is aspirated.
The technological means that cigarette paper perfuming is taken at present mainly has:1)Spices is directly appended in a manner of coating fluid In cigarette paper;2nd, molecule encapsulated or embedding are carried out to spices using cyclodextrin and its derivative, the body of paste for including spices are made, Then it is added in a manner of coating fluid in cigarette paper;3)Molecule encapsulated is carried out to spices using cyclodextrin and its derivative Or embedding, then by drying of dusting, the powder for including spices is made, cigarette paper is then added in a manner of filler In;4)Spices is embedded as wall material using suitable high polymer material, then by method processing physically or chemically, system For into comprising perfume microcapsule powder, then it is added in a manner of filler in cigarette paper.
Had certain effect although above-mentioned cigarette paper perfuming technology has in terms of flavouring humectation, but still several aspects be present Deficiency:1st, for technological means 1, it is mainly reflected in that spices fragrant loss when cigarette paper produces is excessive, and perfumery on cigarette paper Matter fragrance remaining time is not grown;2)For technological means 2, in terms of being mainly reflected in the selectivity that cyclodextrin embeds to spices, especially into Point complicated spices, it is difficult to its all components is uniformly immobilized in cyclodextrin cavity, secondly, the embedding rate of cyclodextrin is not yet Greatly, the amount of flavorants of embedding is smaller;3)For technological means 3, and it is mainly reflected in the selectivity or embedding rate of cyclodextrin embedding Not high two aspects, and cyclodextrin and spices embedding Main Basiss is a kind of molecular separating force, such a active force is weaker, so depositing In loss fragrant to a certain degree;4)For technological means 4, the negative effect of polymer confrontation cigarette odor-absorbing is mainly reflected in, and And when cigarette paper produces, high score subclass wall material easily by the corrosion of water, causes part perfume loss, so as to reduce using effect.
The present invention is directed to the deficiency of existing cigarette paper perfuming technology, selects porous class inorganic material to carry out appendix spices first, Then water-insoluble macromolecular material is overlying on porous material surface again, forms envelope, prevent spices fragrance matter in cigarette paper Loss in production and library procedure, and can effectively extend the retention time of Studies of The Aromatic Substances.
The content of the invention
It is an object of the invention to overcome the shortcomings of existing perfuming cigarette technology, the embedding rate of fragrance material is improved, is reduced The loss amount of Studies of The Aromatic Substances, extend the retention time of Studies of The Aromatic Substances, there is provided a kind of sweet odor type cigarette paper and preparation method thereof.
To achieve these goals, the present invention has the technical scheme to be:Using porous calcium carbonate, porous magnesia, porous oxygen Change the porous inorganic materials such as aluminium powder as fragrance carrier, using the porous of porous material, high adsorption, pass through vacuum perfuming Mode, first by the propolis extract after atomization, honey extract appendix in porous material cavity;Then again in porous material The ethanol solution of ethyl cellulose of the particle surface spraying by atomization, water-insoluble film is formed after ethanol volatilization completely Layer, so as to effectively prevent the volatilization of fragrance matter, reduce the loss of Studies of The Aromatic Substances;The porous material of spices finally be will be enriched in fill out The mode of material is added in cigarette paper, and preparation gained cigarette paper can improve the sweet sense of cigarette smoke, promote the production of body fluid sense and comfortableness It and fragrance is rich, and can also be consistent the style and features of sucking of section before and after cigarette.
The preparation method of sweet odor type cigarette paper comprises the following steps:
1)Porous material carries fragrant:Under conditions of vacuum is -0.07 ~ -0.08MPa, wriggling revolution speed is adjusted to 160 ~ 180 Rev/min, the atomizing pressure of pressure-air is adjusted to 0.2 ~ 0.3MPa, then by propolis extract or honey in a manner of vacuum perfuming The mixture of extract or the two arbitrary proportion is added to porous calcium carbonate powder or porous oxidation magnesium dust or Woelm Alumina In the cavity of the mixture porous material of the mixture or three's arbitrary proportion of powder or both wherein any arbitrary proportions, and add Fragrant addition is the 20 ~ 35% of porous material weight, obtains carrying fragrant porous material;
2)Porous material overlay film:Fragrant process conditions are carried by above-mentioned porous material(It is -0.07 ~ -0.08MPa's i.e. in vacuum Under the conditions of, wriggling revolution speed is adjusted to 160 ~ 180 revs/min, the atomizing pressure of pressure-air is adjusted to 0.2 ~ 0.3MPa, then with true The mode of empty perfuming)It will be molten the ethyl cellulose ethanol formed will to be mixed by 12 ~ 25 parts of ethyl celluloses and 75 ~ 85 parts of absolute ethyl alcohols Liquid is sprayed on the porous material surface for being loaded with spices, and ethyl cellulose ethanol solution addition is the 2 ~ 5% of porous material weight, Obtain porous calcium carbonate and carry face powder end;
3)The preparation of sweet odor type cigarette paper:The porous material comprising spices obtained by prepared by step 2 is in a manner of filler It is added in wood pulp cellulose slurries, its addition accounts for the 20 ~ 30% of cigarette paper dry weight, by being sufficiently mixed, forms uniform paper pulp Suspension, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Described propolis extract, honey extract are commercially available prod, have tempting, quiet and tastefully laid out sweet fragrance, simultaneous There is the simple and elegant fragrance of a flower, can be with the mutual harmony of this perfume of tobacco, its chemical composition included, such as limonene, cloves alkene, Chinese cassia tree Acid, benzoic acid, benzyl carbinol, vanillic aldehyde etc., it is the important flavor matter of cigarette flavor.
The ethyl cellulose of described porous material surface spraying, has excellent film forming, it is in porous material surface Water-insoluble film layer is formed, sealing can be played a part of to the spices in porous material cavity, and thermal decomposition product is similar In the thermal decomposition product of wood pulp cellulose, cigarette odor-absorbing will not be had a negative impact.
The porous inorganic materials such as described porous calcium carbonate, porous magnesia, porous oxidation aluminium powder burn in cigarette paper When, it will not also have an impact the material of cigarette odor-absorbing.
Compared with prior art, the present invention has advantages below:
1st, it is fragrant by being carried to porous material, the addition of spices can be improved, while namely improve adding for spices in cigarette paper Dosage, and porous material carries perfume (or spice) and perfume composition uniformity can be embedded in cavity.
2nd, by the way that to carrying fragrant porous material overlay film, the loss and volatilization of spices can be significantly decreased, while can carry The sweet sense of high cigarette smoke, promote the production of body fluid sense and comfortableness and fragrance it is rich, when extending the reservation of cigarette paper fragrance material Between.
3rd, material therefor of the present invention does not have a negative impact to cigarette odor-absorbing, and can also make sucking for section before and after cigarette Style and features are consistent.
Embodiment
For a better understanding of the present invention, with reference to embodiment, the invention will be further described, but the present invention Embodiment not limited to this.In the examples where no specific technique or condition is specified, according to document in the art described by skill Art or condition are carried out according to product description.Agents useful for same or the unreceipted production firm person of instrument, are that can pass through purchase Buy the conventional products of acquisition.
Embodiment 1:
1st, porous material carries fragrant:It is -0.075MPa in vacuum, wriggling revolution speed is 170 revs/min, pressure-air atomizing pressure Under conditions of 0.2MPa, in a manner of vacuum perfuming, propolis extract is added in porous calcium carbonate powder cavity first, Propolis extract addition is the 26% of porous material weight, obtains carrying fragrant porous material;
2nd, porous material overlay film:It will be mixed and formed by 15 parts of ethyl celluloses and 85 parts of absolute ethyl alcohols by above-mentioned 1 process conditions Ethyl cellulose solution be sprayed on and carry fragrant porous material surface, ethyl cellulose solution addition is carries fragrant porous material weight 5%, obtain porous calcium carbonate carry face powder end;
3rd, the preparation of sweet odor type cigarette paper:The porous calcium carbonate for preparing gained is carried into face powder end and is added to wood in a manner of filler In pulp fibres slurries, its addition accounts for the 25% of cigarette paper dry weight, afterwards, by being sufficiently mixed, forms uniform pulp suspension Liquid, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Embodiment 2:
1st, porous material carries fragrant:It is -0.08MPa in vacuum, wriggling revolution speed is 160 revs/min, and pressure-air atomizing pressure is Under conditions of 0.25MPa, in a manner of vacuum perfuming, honey extract is added in porous magnesia powder cavity first, Propolis extract addition is the 28% of porous material weight, obtains carrying fragrant porous material;
2nd, porous material overlay film:It will be mixed and formed by 20 parts of ethyl celluloses and 80 parts of absolute ethyl alcohols by above-mentioned 1 process conditions Ethyl cellulose solution be sprayed on and carry fragrant porous material surface, ethyl cellulose solution addition is porous material weight 3%, obtain porous calcium carbonate and carry face powder end;
3rd, the preparation of sweet odor type cigarette paper:The porous calcium carbonate for preparing gained is carried into face powder end and is added to wood in a manner of filler In pulp fibres slurries, its addition accounts for the 20% of cigarette paper dry weight, afterwards, by being sufficiently mixed, forms uniform pulp suspension Liquid, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Embodiment 3:
1st, porous material carries fragrant:It is -0.07MPa in vacuum, wriggling revolution speed is 180 revs/min, and pressure-air atomizing pressure is Under conditions of 0.3MPa, in a manner of vacuum perfuming, it will be mixed first by 60 parts of honey extracts and 40 parts of propolis essence extracts The spices of composition is added in Woelm Alumina powder cavity, and its addition is the 35% of porous material weight, and it is fragrant porous to obtain load Material;
2nd, porous material overlay film:It will be mixed and formed by 12 parts of ethyl celluloses and 88 parts of absolute ethyl alcohols by above-mentioned 1 process conditions Ethyl cellulose solution be sprayed on and carry fragrant porous material surface, its addition is the 5% of porous material weight, obtains porous carbonic acid Calcium carries face powder end;
3rd, the preparation of sweet odor type cigarette paper:The porous calcium carbonate for preparing gained is carried into face powder end and is added to wood in a manner of filler In pulp fibres slurries, its addition accounts for the 30% of cigarette paper dry weight, afterwards, by being sufficiently mixed, forms uniform pulp suspension Liquid, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Embodiment 4:
1st, porous material carries fragrant:It is -0.075MPa in vacuum, wriggling revolution speed is 175 revs/min, pressure-air atomizing pressure , will be by 30 parts of honey extracts and 70 parts of propolis essence extract mixing structures in a manner of vacuum perfuming under conditions of 0.25MPa Into spices be added in the mixed-powder cavity being made up of 60 parts of porous calcium carbonates and the mixing of 40 parts of porous magnesias, spices adds Dosage is the 35% of porous material weight, obtains carrying fragrant porous material;
2nd, porous material overlay film:It will be mixed and formed by 25 parts of ethyl celluloses and 75 parts of absolute ethyl alcohols by above-mentioned 1 process conditions Ethyl cellulose solution be sprayed on and carry fragrant porous material surface, its addition is the 4% of porous material weight, obtains porous carbon Sour calcium carries face powder end;
3rd, the preparation of sweet odor type cigarette paper:The porous calcium carbonate for preparing gained is carried into face powder end and is added to wood in a manner of filler In pulp fibres slurries, its addition accounts for the 28% of cigarette paper dry weight, afterwards, by being sufficiently mixed, forms uniform pulp suspension Liquid, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Embodiment 5:
1st, porous material carries fragrant:It is -0.07MPa in vacuum, wriggling revolution speed is 165 revs/min, and pressure-air atomizing pressure is Under conditions of 0.2MPa, in a manner of vacuum perfuming, by propolis essence extract be added to by 50 parts of porous calcium carbonates, 30 parts it is porous In the mixed-powder cavity that magnesia and 20 parts of Woelm Alumina mixing are formed, its addition is the 30% of porous material weight, is obtained Face powder end is carried to porous calcium carbonate;
2nd, porous material overlay film:It will be mixed and formed by 22 parts of ethyl celluloses and 78 parts of absolute ethyl alcohols by above-mentioned 1 process conditions Ethyl cellulose solution be sprayed on and carry fragrant porous material surface, its addition is the 5% of porous material weight, obtains porous carbon Sour calcium carries face powder end;
3rd, the preparation of sweet odor type cigarette paper:The porous calcium carbonate for preparing gained is carried into face powder end and is added to wood in a manner of filler In pulp fibres slurries, its addition accounts for the 30% of cigarette paper dry weight, afterwards, by being sufficiently mixed, forms uniform pulp suspension Liquid, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
Cigarette is made in the cigarette paper roll prepared by embodiment 1~5 respectively, using online normal cigarette as reference examples, is carried out Sensory evaluation, smoking result are shown in Table 1:
The cigarette sensory evaluating smoking's result of table 1
Remarks:In addition to cigarette paper differs, remaining pipe tobacco and auxiliary material are completed identical for reference examples and the cigarette of embodiment 1~5.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (6)

  1. A kind of 1. preparation method of sweet odor type cigarette paper, it is characterised in that:Carry out according to the following steps:
    1)Porous material carries fragrant:Under conditions of vacuum is -0.07 ~ -0.08MPa, wriggling revolution speed is adjusted to 160 ~ 180 Rev/min, the atomizing pressure of pressure-air is adjusted to 0.2 ~ 0.3MPa, then by propolis extract or honey in a manner of vacuum perfuming The mixture of extract or the two arbitrary proportion is added to porous calcium carbonate powder or porous oxidation magnesium dust or Woelm Alumina In the cavity of the mixture porous material of the mixture or three's arbitrary proportion of powder or both wherein any arbitrary proportions, and add Fragrant addition is the 20 ~ 35% of porous material weight, obtains carrying fragrant porous material;
    2)Porous material overlay film:Fragrant process conditions are carried by above-mentioned porous material, i.e., are -0.07 ~ -0.08MPa's in vacuum Under the conditions of, wriggling revolution speed is adjusted to 160 ~ 180 revs/min, the atomizing pressure of pressure-air is adjusted to 0.2 ~ 0.3MPa, then with true The mode of empty perfuming, it is molten that the ethyl cellulose ethanol formed will be mixed by 12 ~ 25 parts of ethyl celluloses and 75 ~ 85 parts of absolute ethyl alcohols Liquid is sprayed on the porous material surface for being loaded with spices, and ethyl cellulose ethanol solution addition is the 2 ~ 5% of porous material weight, Obtain porous calcium carbonate and carry face powder end;
    3)The preparation of sweet odor type cigarette paper:The porous material comprising spices obtained by prepared by step 2 is in a manner of filler It is added in wood pulp cellulose slurries, its addition accounts for the 20 ~ 30% of cigarette paper dry weight, by being sufficiently mixed, forms uniform paper pulp Suspension, then by manufacturing paper with pulp to obtain sweet odor type cigarette paper.
  2. 2. the preparation method of sweet odor type cigarette paper according to claim 1, it is characterised in that described ethyl cellulose Ethanol solution, be made up of 12 ~ 25 parts of ethyl celluloses and the mixing of 75 ~ 85 parts of absolute ethyl alcohols.
  3. 3. the preparation method of sweet odor type cigarette paper according to claim 1, it is characterised in that described propolis extract Mixing with honey extract is by 30-60 part honey extracts and the mixing of 40-70 part propolis essences extract.
  4. 4. the preparation method of sweet odor type cigarette paper according to claim 1, it is characterised in that described porous material by 50 parts of porous calcium carbonates, 30 parts of porous magnesias and 20 parts of Woelm Alumina mixing are formed.
  5. 5. the preparation method of sweet odor type cigarette paper according to claim 1, it is characterised in that described porous material by 60 parts of porous calcium carbonates and 40 parts of porous magnesia mixing are formed.
  6. 6. the sweet odor type cigarette paper that a kind of preparation method of sweet odor type cigarette paper with described in claim 1 is prepared.
CN201710943652.2A 2017-10-11 2017-10-11 A kind of sweet odor type cigarette paper and preparation method thereof Pending CN107419593A (en)

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CN110924234A (en) * 2019-11-25 2020-03-27 浙江华丰纸业科技有限公司 Printing two-section cigarette paper and preparation method thereof
CN111418875A (en) * 2020-05-11 2020-07-17 河南中烟工业有限责任公司 Preparation method of cigar-flavor cigarette paper

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Publication number Priority date Publication date Assignee Title
CN110924234A (en) * 2019-11-25 2020-03-27 浙江华丰纸业科技有限公司 Printing two-section cigarette paper and preparation method thereof
CN111418875A (en) * 2020-05-11 2020-07-17 河南中烟工业有限责任公司 Preparation method of cigar-flavor cigarette paper

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Application publication date: 20171201