CN106135276A - A kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof - Google Patents

A kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof Download PDF

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Publication number
CN106135276A
CN106135276A CN201610474730.4A CN201610474730A CN106135276A CN 106135276 A CN106135276 A CN 106135276A CN 201610474730 A CN201610474730 A CN 201610474730A CN 106135276 A CN106135276 A CN 106135276A
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Prior art keywords
parts
bta
sodium molybdate
semen sojae
sojae atricolor
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CN201610474730.4A
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Chinese (zh)
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赵思璐
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Individual
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Priority to CN201610474730.4A priority Critical patent/CN106135276A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16Heavy metals; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N53/00Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof, including the raw material of following weight portion: Kadethrin, 45~55 parts;Primulagenin, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist BTA and sodium molybdate totally 6~8 parts, the weight ratio of BTA and sodium molybdate is 5~7:1.The compositions that the present invention provides can prevent and treat Semen sojae atricolor red spider, the pesticide of preventing and treating Semen sojae atricolor red spider can be developed into, prevention effect is relevant with the weight ratio of synergist BTA and sodium molybdate in raw material, and when the weight ratio of BTA and sodium molybdate is 5~7:1, prevention effect is best.And, it is little that the present composition sprays dose, is difficult to residual.

Description

A kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof.
Background technology
Kadethrin is a kind of crops pesticide, and herbicidal performance is remarkable simultaneously.
Semen sojae atricolor red spider is Tetranychus cinnabarinus, belongs to Arachnoidea Acarina Tetranychidae.Within 2007, affected by high temperature and drought, big bean red In Heilongjiang Province, big occurring area reaches 1.2 hundred million mu to Aranea, causes Semen sojae atricolor Severe Reduction.According to investigations, in recent years, Semen sojae atricolor red spider Cause harm and have gone up as main status, typically make Semen sojae atricolor underproduction 20-30%, serious plot underproduction 70-90%..
Have not yet to see Kadethrin and work in coordination with the report preventing and treating Semen sojae atricolor red spider with primulagenin.
Summary of the invention
It is an object of the invention to provide the compositions of a kind of preventing and treating Semen sojae atricolor red spider containing Kadethrin and primulagenin And the application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Semen sojae atricolor red spider, including the raw material of following weight portion: Kadethrin, 45~55 parts;Report Vernalin, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist BTA and sodium molybdate totally 6~8 Part, the weight ratio of BTA and sodium molybdate is 5~7:1.
Further, the compositions of described preventing and treating Semen sojae atricolor red spider includes the raw material of following weight portion: Kadethrin, 50 Part;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and sodium molybdate totally 7 parts, BTA It is 6:1 with the weight ratio of sodium molybdate.
Further, the compositions of described preventing and treating Semen sojae atricolor red spider includes the raw material of following weight portion: Kadethrin, 45 Part;Primulagenin, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and sodium molybdate totally 6 parts, BTA It is 5:1 with the weight ratio of sodium molybdate.
Further, the compositions of described preventing and treating Semen sojae atricolor red spider includes the raw material of following weight portion: Kadethrin, 55 Part;Primulagenin, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and sodium molybdate totally 8 parts, BTA It is 7:1 with the weight ratio of sodium molybdate.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Semen sojae atricolor red spider, can develop into the pesticide of preventing and treating Semen sojae atricolor red spider.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Semen sojae atricolor red spider
Parts by weight of raw materials compares:
Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and molybdenum Totally 7 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 6:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Semen sojae atricolor red spider
Parts by weight of raw materials compares:
Kadethrin, 45 parts;Primulagenin, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and molybdenum Totally 6 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 5:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Semen sojae atricolor red spider
Parts by weight of raw materials compares:
Kadethrin, 55 parts;Primulagenin, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and molybdenum Totally 8 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 7:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Semen sojae atricolor red spider
Parts by weight of raw materials compares:
Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and molybdenum Totally 7 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 5:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Semen sojae atricolor red spider
Parts by weight of raw materials compares:
Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and molybdenum Totally 7 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 7:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, BTA and sodium molybdate is 4:1
Parts by weight of raw materials compares:
Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and molybdenum Totally 7 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 4:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, BTA and sodium molybdate is 8:1
Parts by weight of raw materials compares:
Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and molybdenum Totally 7 parts of sodium of acid, the weight ratio of BTA and sodium molybdate is 8:1.
Preparation method:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1~7 preventing and treating effective percentage to Semen sojae atricolor red spider (%).
Test sets chemicals treatment group 1~7 and blank group, and chemicals treatment group 1~7 is sprayed embodiment 1~7 respectively and prepared Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 20g/hm in terms of Kadethrin2.Plot area is 50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
Preventing and treating effective percentage (%)
Embodiment 1 97
Embodiment 4 93
Embodiment 5 92
Embodiment 6 65
Embodiment 7 62
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Semen sojae atricolor red spider, can develop into preventing and treating Semen sojae atricolor The pesticide of red spider, prevention effect is relevant with the weight ratio of synergist BTA and sodium molybdate in raw material, benzo three When the weight ratio of nitrogen azoles and sodium molybdate is 5~7:1, prevention effect is best.If without primulagenin, the present composition Preventing and treating effective percentage less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent, Essence and protection domain without deviating from technical solution of the present invention.

Claims (5)

1. the compositions preventing and treating Semen sojae atricolor red spider, it is characterised in that include the raw material of following weight portion: Kadethrin, 45 ~55 parts;Primulagenin, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist BTA and molybdic acid Totally 6~8 parts of sodium, the weight ratio of BTA and sodium molybdate is 5~7:1.
The compositions of preventing and treating Semen sojae atricolor red spider the most according to claim 1, it is characterised in that include the former of following weight portion Material: Kadethrin, 50 parts;Primulagenin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and sodium molybdate are altogether 7 parts, the weight ratio of BTA and sodium molybdate is 6:1.
The compositions of preventing and treating Semen sojae atricolor red spider the most according to claim 1, it is characterised in that include the former of following weight portion Material: Kadethrin, 45 parts;Primulagenin, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and sodium molybdate are altogether 6 parts, the weight ratio of BTA and sodium molybdate is 5:1.
The compositions of preventing and treating Semen sojae atricolor red spider the most according to claim 1, it is characterised in that include the former of following weight portion Material: Kadethrin, 55 parts;Primulagenin, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and sodium molybdate are altogether 8 parts, the weight ratio of BTA and sodium molybdate is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves Kadethrin, primulagenin and synergist BTA G & W;
Step S2, by sodium molybdate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
CN201610474730.4A 2016-06-22 2016-06-22 A kind of compositions preventing and treating Semen sojae atricolor red spider and preparation method thereof Pending CN106135276A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102057942A (en) * 2011-01-13 2011-05-18 江苏省农业科学院 Emamectin benzoate and kadethrine compound insecticide
CN103109846A (en) * 2013-03-13 2013-05-22 山东省农业科学院中心实验室 Dichlorovos kadethrine compounded pesticide

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102057942A (en) * 2011-01-13 2011-05-18 江苏省农业科学院 Emamectin benzoate and kadethrine compound insecticide
CN103109846A (en) * 2013-03-13 2013-05-22 山东省农业科学院中心实验室 Dichlorovos kadethrine compounded pesticide

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
程若愚 等: "《农用商品归类手册》", 30 September 2012, 中国海关出版社 *

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Application publication date: 20161123