CN106035362A - Composition for controlling adoxophyes orana and preparation method of composition - Google Patents
Composition for controlling adoxophyes orana and preparation method of composition Download PDFInfo
- Publication number
- CN106035362A CN106035362A CN201610393081.5A CN201610393081A CN106035362A CN 106035362 A CN106035362 A CN 106035362A CN 201610393081 A CN201610393081 A CN 201610393081A CN 106035362 A CN106035362 A CN 106035362A
- Authority
- CN
- China
- Prior art keywords
- parts
- dialkyl diphenylamine
- edta
- nerol
- brofenxalerate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N49/00—Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/06—Nitrogen directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/34—Nitriles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
Abstract
The invention discloses composition for controlling adoxophyes orana and a preparation method of the composition. The composition comprises raw materials in parts by weight as follows: 20-30 parts of brofenvalerate, 10-20 parts of nerol, 130-150 parts of glycerin, 350-370 parts of water and 6-8 parts of synergists dialkyl diphenylamine and ferric EDTA (ethylenediaminetetreacetic acid), wherein a weight part ratio of dialkyl diphenylamine to ferric EDTA is 5-7:1. The composition can control the adoxophyes orana and can be developed into a pesticide for controlling the adoxophyes orana, the control effect is related with the weight part ratio of dialkyl diphenylamine to ferric EDTA serving as the synergists in the raw materials, and the best control effect is realized when the weight part ratio of dialkyl diphenylamine to ferric EDTA is 5-7:1. Besides, the spraying amount of the composition is small, and the composition is not prone to remaining.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Fructus Mali pumilae rouleau leaf worm and preparation method thereof.
Background technology
Brofenxalerate belongs to pyrethroid insecticides.Have the advantages that micro-poison, power of knocking down are strong, quick-acting.Brofenxalerate pair
Insect knocks down power by force, mainly makes pest movements nervous disorder, spasm, paralysis die.
Have not yet to see brofenxalerate and work in coordination with the report preventing and treating Fructus Mali pumilae rouleau leaf worm with nerol.
Summary of the invention
It is an object of the invention to provide the compositions of a kind of preventing and treating Fructus Mali pumilae rouleau leaf worm containing brofenxalerate and nerol
And the application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Fructus Mali pumilae rouleau leaf worm, including the raw material of following weight portion: brofenxalerate, 20～30 parts；
Nerol, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and ethylenediamine tetrem
Acid ferrum totally 6～8 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5～7:1.
Further, the compositions of described preventing and treating Fructus Mali pumilae rouleau leaf worm includes the raw material of following weight portion: brofenxalerate,
25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and EDTA-Fe totally 7 parts,
The weight ratio of dialkyl diphenylamine and EDTA-Fe is 6:1.
Further, the compositions of described preventing and treating Fructus Mali pumilae rouleau leaf worm includes the raw material of following weight portion: brofenxalerate,
20 parts；Nerol, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and EDTA-Fe totally 6 parts,
The weight ratio of dialkyl diphenylamine and EDTA-Fe is 5:1.
Further, the compositions of described preventing and treating Fructus Mali pumilae rouleau leaf worm includes the raw material of following weight portion: brofenxalerate,
30 parts；Nerol, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and EDTA-Fe totally 8 parts,
The weight ratio of dialkyl diphenylamine and EDTA-Fe is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Fructus Mali pumilae rouleau leaf worm, can develop into the agriculture of preventing and treating Fructus Mali pumilae rouleau leaf worm
Medicine.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm
Parts by weight of raw materials compares:
Brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 6:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm
Parts by weight of raw materials compares:
Brofenxalerate, 20 parts；Nerol, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 6 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm
Parts by weight of raw materials compares:
Brofenxalerate, 30 parts；Nerol, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 8 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 7:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm
Parts by weight of raw materials compares:
Brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm
Parts by weight of raw materials compares:
Brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 7:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, dialkyl diphenylamine and EDTA-Fe is 4:1
Parts by weight of raw materials compares:
Brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 4:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, dialkyl diphenylamine and EDTA-Fe is 8:1
Parts by weight of raw materials compares:
Brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 8:1.
Preparation method:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage to Fructus Mali pumilae rouleau leaf worm
(%).
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 50g/hm in terms of brofenxalerate2.Plot area is
50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 97 |
| Embodiment 4 | 92 |
| Embodiment 5 | 93 |
| Embodiment 6 | 63 |
| Embodiment 7 | 64 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Fructus Mali pumilae rouleau leaf worm, can develop into preventing and treating Herba Marsileae Quadrifoliae
The really pesticide of rouleau leaf worm, in prevention effect and raw material the weight portion of synergist dialkyl diphenylamine and EDTA-Fe it
Ratio is relevant, and when the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5～7:1, prevention effect is best.If not adding
Adding nerol, the preventing and treating effective percentage of the present composition is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual
Stay.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating Fructus Mali pumilae rouleau leaf worm, it is characterised in that include the raw material of following weight portion: brofenxalerate,
20～30 parts；Nerol, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and second
Ethylenediamine tetraacetic acid (EDTA) ferrum totally 6～8 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5～7:1.
The compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm the most according to claim 1, it is characterised in that include following weight portion
Raw material: brofenxalerate, 25 parts；Nerol, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and ethylenediamine
Tetraacethyl ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 6:1.
The compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm the most according to claim 1, it is characterised in that include following weight portion
Raw material: brofenxalerate, 20 parts；Nerol, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and ethylenediamine
Tetraacethyl ferrum totally 6 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 5:1.
The compositions of preventing and treating Fructus Mali pumilae rouleau leaf worm the most according to claim 1, it is characterised in that include following weight portion
Raw material: brofenxalerate, 30 parts；Nerol, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and ethylenediamine
Tetraacethyl ferrum totally 8 parts, the weight ratio of dialkyl diphenylamine and EDTA-Fe is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves brofenxalerate, nerol and synergist dialkyl diphenylamine G & W；
Step S2, by EDTA-Fe water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610393081.5A CN106035362A (en) | 2016-05-31 | 2016-05-31 | Composition for controlling adoxophyes orana and preparation method of composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610393081.5A CN106035362A (en) | 2016-05-31 | 2016-05-31 | Composition for controlling adoxophyes orana and preparation method of composition |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106035362A true CN106035362A (en) | 2016-10-26 |
Family
ID=57170292
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610393081.5A Pending CN106035362A (en) | 2016-05-31 | 2016-05-31 | Composition for controlling adoxophyes orana and preparation method of composition |
Country Status (1)
| Country | Link |
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| CN (1) | CN106035362A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1279016A (en) * | 1999-06-29 | 2001-01-10 | 张业升 | Insecticiding-miticiding composition containing brofenxalerate |
| CN102083311A (en) * | 2008-04-11 | 2011-06-01 | 巴斯夫公司 | Pesticidal compositions |
| CN102499236A (en) * | 2011-10-17 | 2012-06-20 | 浙江大学 | Solid microemulsion comprising pyrethroid pesticide and preparation method of solid microemulsion |
-
2016
- 2016-05-31 CN CN201610393081.5A patent/CN106035362A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1279016A (en) * | 1999-06-29 | 2001-01-10 | 张业升 | Insecticiding-miticiding composition containing brofenxalerate |
| CN102083311A (en) * | 2008-04-11 | 2011-06-01 | 巴斯夫公司 | Pesticidal compositions |
| CN102499236A (en) * | 2011-10-17 | 2012-06-20 | 浙江大学 | Solid microemulsion comprising pyrethroid pesticide and preparation method of solid microemulsion |
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Application publication date: 20161026 |