CN106106475A - A kind of compositions preventing and treating pears food bud moth and preparation method thereof - Google Patents
A kind of compositions preventing and treating pears food bud moth and preparation method thereof Download PDFInfo
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- CN106106475A CN106106475A CN201610466658.0A CN201610466658A CN106106475A CN 106106475 A CN106106475 A CN 106106475A CN 201610466658 A CN201610466658 A CN 201610466658A CN 106106475 A CN106106475 A CN 106106475A
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- acryloyloxy
- ethanol
- sodium glutamate
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating pears food bud moth and preparation method thereof, including the raw material of following weight portion: levamisole, 20～30 parts；Epiquinine is fixed, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate totally 6～8 parts, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5～7:1.The compositions that the present invention provides can prevent and treat pears food bud moth, the pesticide of preventing and treating pears food bud moth can be developed into, prevention effect is relevant with the weight ratio of synergist 2-(Acryloyloxy)ethanol and sodium glutamate in raw material, when the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5～7:1, prevention effect is best.And, it is little that the present composition sprays dose, is difficult to residual.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating pears food bud moth and preparation method thereof.
Background technology
Pears food bud moth is commonly called as magic flower worm, belongs to Lepidoptera, Olethreutidae.Main harm pear tree etc..Be distributed widely in Liaoning,
Hebei, Henan etc. save.
Have not yet to see the report of levamisole and epiquinine surely collaborative preventing and treating pears food bud moth.
Summary of the invention
It is an object of the invention to provide a kind of containing levamisole and epiquinine fixed preventing and treating pears food bud moth compositions and
Application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating pears food bud moth, including the raw material of following weight portion: levamisole, 20～30 parts；Epiquinine
Fixed, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate totally 6～8
Part, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5～7:1.
Further, the compositions of described preventing and treating pears food bud moth includes the raw material of following weight portion: levamisole, 25 parts；
Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate totally 7 parts, acrylic acid hydroxyl
The weight ratio of ethyl ester and sodium glutamate is 6:1.
Further, the compositions of described preventing and treating pears food bud moth includes the raw material of following weight portion: levamisole, 20 parts；
Epiquinine is fixed, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate totally 6 parts, acrylic acid hydroxyl
The weight ratio of ethyl ester and sodium glutamate is 5:1.
Further, the compositions of described preventing and treating pears food bud moth includes the raw material of following weight portion: levamisole, 30 parts；
Epiquinine is fixed, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate totally 8 parts, acrylic acid hydroxyl
The weight ratio of ethyl ester and sodium glutamate is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat pears food bud moth, can develop into the pesticide of preventing and treating pears food bud moth.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating pears food bud moth
Parts by weight of raw materials compares:
Levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 7 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 6:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating pears food bud moth
Parts by weight of raw materials compares:
Levamisole, 20 parts；Epiquinine is fixed, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 6 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating pears food bud moth
Parts by weight of raw materials compares:
Levamisole, 30 parts；Epiquinine is fixed, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 8 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 7:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating pears food bud moth
Parts by weight of raw materials compares:
Levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 7 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating pears food bud moth
Parts by weight of raw materials compares:
Levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 7 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 7:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, 2-(Acryloyloxy)ethanol and sodium glutamate is 4:1
Parts by weight of raw materials compares:
Levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 7 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 4:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, 2-(Acryloyloxy)ethanol and sodium glutamate is 8:1
Parts by weight of raw materials compares:
Levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and paddy
Totally 7 parts of propylhomoserin sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 8:1.
Preparation method:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The preventing and treating effective percentage (%) of bud moth eaten by pears by the compositions using field test testing example 1～7 preparation respectively.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 50g/hm in terms of levamisole2.Plot area is
50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 97 |
| Embodiment 4 | 92 |
| Embodiment 5 | 93 |
| Embodiment 6 | 63 |
| Embodiment 7 | 64 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat pears food bud moth, can develop into preventing and treating pears food bud
The pesticide of moth, prevention effect is relevant with the weight ratio of synergist 2-(Acryloyloxy)ethanol and sodium glutamate in raw material, acrylic acid
When the weight ratio of hydroxyl ethyl ester and sodium glutamate is 5～7:1, prevention effect is best.If fixed without epiquinine, of the present invention group
The preventing and treating effective percentage of compound is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating pears food bud moth, it is characterised in that include the raw material of following weight portion: levamisole, 20～30
Part；Epiquinine is fixed, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist 2-(Acryloyloxy)ethanol and glutamic acid
Totally 6～8 parts of sodium, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5～7:1.
The compositions of preventing and treating pears the most according to claim 1 food bud moth, it is characterised in that include the former of following weight portion
Material: levamisole, 25 parts；Epiquinine is fixed, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate
Totally 7 parts, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 6:1.
The compositions of preventing and treating pears the most according to claim 1 food bud moth, it is characterised in that include the former of following weight portion
Material: levamisole, 20 parts；Epiquinine is fixed, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate
Totally 6 parts, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 5:1.
The compositions of preventing and treating pears the most according to claim 1 food bud moth, it is characterised in that include the former of following weight portion
Material: levamisole, 30 parts；Epiquinine is fixed, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist 2-(Acryloyloxy)ethanol and sodium glutamate
Totally 8 parts, the weight ratio of 2-(Acryloyloxy)ethanol and sodium glutamate is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by levamisole, epiquinine is fixed and synergist 2-(Acryloyloxy)ethanol G & W dissolves；
Step S2, by sodium glutamate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610466658.0A CN106106475A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating pears food bud moth and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610466658.0A CN106106475A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating pears food bud moth and preparation method thereof |
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| CN106106475A true CN106106475A (en) | 2016-11-16 |
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| CN201610466658.0A Pending CN106106475A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating pears food bud moth and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110759905A (en) * | 2019-10-21 | 2020-02-07 | 河南科技大学 | 9S-acyloxy cinchonine derivative, preparation method and application thereof, and botanical pesticide |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110759905B (en) * | 2019-10-21 | 2021-05-11 | 河南科技大学 | 9S-acyloxy cinchonine derivative, preparation method and application thereof, and botanical pesticide |
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Application publication date: 20161116 |