CN106070299A - A kind of compositions preventing and treating striped flea-beetle and preparation method thereof - Google Patents
A kind of compositions preventing and treating striped flea-beetle and preparation method thereof Download PDFInfo
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- CN106070299A CN106070299A CN201610394819.XA CN201610394819A CN106070299A CN 106070299 A CN106070299 A CN 106070299A CN 201610394819 A CN201610394819 A CN 201610394819A CN 106070299 A CN106070299 A CN 106070299A
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- sodium benzoate
- beetle
- dialkyl diphenylamine
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
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- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating striped flea-beetle and preparation method thereof, including the raw material of following weight portion: cyclethrin, 20～30 parts；Azaleatin, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and sodium benzoate totally 6～8 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5～7:1.The compositions that the present invention provides can prevent and treat striped flea-beetle, the pesticide of preventing and treating striped flea-beetle can be developed into, prevention effect is relevant with the weight ratio of synergist dialkyl diphenylamine and sodium benzoate in raw material, when the weight ratio of dialkyl diphenylamine and sodium benzoate is 5～7:1, prevention effect is best.And, it is little that the present composition sprays dose, is difficult to residual.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating striped flea-beetle and preparation method thereof.
Background technology
Belong to coleoptera, Chrysomelidae in striped flea-beetle classification, including phyllotreta striolata, yellow vertical bar flea beetle, yellow slat flea beetle and
Yellow wide bar flea beetle 4 kinds.Phyllotreta striolata is most commonly seen.The cabbage of main harm Cruciferae, Caulis et Folium Brassicae capitatae class and Radix Raphani etc., also may be used
Injure solanaceous vegetables, melon and legume vegetable.
Have not yet to see cyclethrin and work in coordination with the report preventing and treating striped flea-beetle with azaleatin.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating striped flea-beetle containing cyclethrin and azaleatin compositions and
Its application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating striped flea-beetle, including the raw material of following weight portion: cyclethrin, 20～30 parts；Cuculus polioephalus
Flavin, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and sodium benzoate totally 6～
8 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5～7:1.
Further, the compositions of described preventing and treating striped flea-beetle includes the raw material of following weight portion: cyclethrin, 25
Part；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and sodium benzoate totally 7 parts, dialkyl group
The weight ratio of diphenylamines and sodium benzoate is 6:1.
Further, the compositions of described preventing and treating striped flea-beetle includes the raw material of following weight portion: cyclethrin, 20
Part；Azaleatin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and sodium benzoate totally 6 parts, dialkyl group
The weight ratio of diphenylamines and sodium benzoate is 5:1.
Further, the compositions of described preventing and treating striped flea-beetle includes the raw material of following weight portion: cyclethrin, 30
Part；Azaleatin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and sodium benzoate totally 8 parts, dialkyl group
The weight ratio of diphenylamines and sodium benzoate is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat striped flea-beetle, can develop into the pesticide of preventing and treating striped flea-beetle.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating striped flea-beetle
Parts by weight of raw materials compares:
Cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 7 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 6:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating striped flea-beetle
Parts by weight of raw materials compares:
Cyclethrin, 20 parts；Azaleatin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 6 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating striped flea-beetle
Parts by weight of raw materials compares:
Cyclethrin, 30 parts；Azaleatin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 8 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 7:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating striped flea-beetle
Parts by weight of raw materials compares:
Cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 7 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating striped flea-beetle
Parts by weight of raw materials compares:
Cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 7 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 7:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, dialkyl diphenylamine and sodium benzoate is 4:1
Parts by weight of raw materials compares:
Cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 7 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 4:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, dialkyl diphenylamine and sodium benzoate is 8:1
Parts by weight of raw materials compares:
Cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and
Sodium benzoate totally 7 parts, the weight ratio of dialkyl diphenylamine and sodium benzoate is 8:1.
Preparation method:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage (%) to striped flea-beetle.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 50g/hm in terms of cyclethrin2.Plot area is
50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 97 |
| Embodiment 4 | 92 |
| Embodiment 5 | 93 |
| Embodiment 6 | 63 |
| Embodiment 7 | 64 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat striped flea-beetle, can develop into anti-bar of harnessing the Yellow River and jump
The pesticide of first, prevention effect is relevant with the weight ratio of synergist dialkyl diphenylamine and sodium benzoate in raw material, dialkyl group
When the weight ratio of diphenylamines and sodium benzoate is 5～7:1, prevention effect is best.If without azaleatin, of the present invention group
The preventing and treating effective percentage of compound is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating striped flea-beetle, it is characterised in that include the raw material of following weight portion: cyclethrin, 20～
30 parts；Azaleatin, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and benzene first
Totally 6～8 parts of sodium of acid, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5～7:1.
The compositions of preventing and treating striped flea-beetle the most according to claim 1, it is characterised in that include the former of following weight portion
Material: cyclethrin, 25 parts；Azaleatin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and benzoic acid
Totally 7 parts of sodium, the weight ratio of dialkyl diphenylamine and sodium benzoate is 6:1.
The compositions of preventing and treating striped flea-beetle the most according to claim 1, it is characterised in that include the former of following weight portion
Material: cyclethrin, 20 parts；Azaleatin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and benzoic acid
Totally 6 parts of sodium, the weight ratio of dialkyl diphenylamine and sodium benzoate is 5:1.
The compositions of preventing and treating striped flea-beetle the most according to claim 1, it is characterised in that include the former of following weight portion
Material: cyclethrin, 30 parts；Azaleatin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and benzoic acid
Totally 8 parts of sodium, the weight ratio of dialkyl diphenylamine and sodium benzoate is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves cyclethrin, azaleatin and synergist dialkyl diphenylamine G & W；
Step S2, by sodium benzoate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394819.XA CN106070299A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating striped flea-beetle and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394819.XA CN106070299A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating striped flea-beetle and preparation method thereof |
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| CN106070299A true CN106070299A (en) | 2016-11-09 |
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| CN201610394819.XA Pending CN106070299A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating striped flea-beetle and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100166818A1 (en) * | 2008-11-17 | 2010-07-01 | Troutman Stevan L | Laundry additive for the treatment and prevention of bed bugs |
| CN101778568A (en) * | 2007-08-08 | 2010-07-14 | 巴斯夫欧洲公司 | aqueous microemulsions containing organic insecticide compounds |
| CN104798798A (en) * | 2014-01-26 | 2015-07-29 | 沈阳化工研究院有限公司 | Binary composition and application thereof |
-
2016
- 2016-05-31 CN CN201610394819.XA patent/CN106070299A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101778568A (en) * | 2007-08-08 | 2010-07-14 | 巴斯夫欧洲公司 | aqueous microemulsions containing organic insecticide compounds |
| US20100166818A1 (en) * | 2008-11-17 | 2010-07-01 | Troutman Stevan L | Laundry additive for the treatment and prevention of bed bugs |
| CN104798798A (en) * | 2014-01-26 | 2015-07-29 | 沈阳化工研究院有限公司 | Binary composition and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| 朱永和 等: "《农药大典》", 31 October 2006 * |
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Application publication date: 20161109 |
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