CN105994278A - Composition for preventing and treating illiberis psychina and preparing method thereof - Google Patents

Composition for preventing and treating illiberis psychina and preparing method thereof Download PDF

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Publication number
CN105994278A
CN105994278A CN201610474207.1A CN201610474207A CN105994278A CN 105994278 A CN105994278 A CN 105994278A CN 201610474207 A CN201610474207 A CN 201610474207A CN 105994278 A CN105994278 A CN 105994278A
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Prior art keywords
parts
preventing
bta
dihydrogen phosphate
sodium dihydrogen
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CN201610474207.1A
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Chinese (zh)
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叶松
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Individual
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Individual
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/40Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N27/00Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/02Acyclic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647Triazoles; Hydrogenated triazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/26Phosphorus; Compounds thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a composition for preventing and treating illiberis psychina and a preparing method thereof. The composition is prepared from, by weight, 45-55 parts of pyriproxyfen, 25-35 parts of ocimene, 120-140 parts of glycerol, 390-410 parts of water and 6-8 parts of synergist comprising benzotriazole and sodium dihydrogen phosphate by the weight ratio of (5-7):1. The provided composition can prevent and treat illiberis psychina and developed into pesticide for preventing and treating illiberis psychina, the preventing and treating effect is related to the weight ratio of the synergist benzotriazole to sodium dihydrogen phosphate, and the preventing and treating effect is best when the weight ratio of benzotriazole to sodium dihydrogen phosphate is (5-7):1. The composition is small in spray dosage and not prone to residual.

Description

A kind of compositions preventing and treating Fructus Pruni caterpillar and preparation method thereof
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Fructus Pruni caterpillar and preparation method thereof.
Background technology
Nylar is the insect growth regulator, IGR that phenylate class upsets insect growth, belongs to the novel pesticide of juvenoid, tool Having interior suction transfer activity, low toxicity, the lasting period is long, to crop safety, to Fish low toxicity, the feature little to eco-environmental impact.
Have not yet to see Nylar and work in coordination with the report preventing and treating Fructus Pruni caterpillar with alloocimene.
Summary of the invention
It is an object of the invention to provide the compositions of the preventing and treating Fructus Pruni caterpillar of a kind of pyriproxyfen-containing and alloocimene and in pesticide Application.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Fructus Pruni caterpillar, including the raw material of following weight portion: Nylar, 45~55 parts;Alloocimene, 25~35 Part;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist BTA and sodium dihydrogen phosphate totally 6~8 parts, benzo three The weight ratio of nitrogen azoles and sodium dihydrogen phosphate is 5~7:1.
Further, the compositions of described preventing and treating Fructus Pruni caterpillar includes the raw material of following weight portion: Nylar, 50 parts;Other Herba Ocimi (Herba Ocimi Pilosi) Alkene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and sodium dihydrogen phosphate totally 7 parts, benzo three nitrogen The weight ratio of azoles and sodium dihydrogen phosphate is 6:1.
Further, the compositions of described preventing and treating Fructus Pruni caterpillar includes the raw material of following weight portion: Nylar, 45 parts;Other Herba Ocimi (Herba Ocimi Pilosi) Alkene, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and sodium dihydrogen phosphate totally 6 parts, benzo three nitrogen The weight ratio of azoles and sodium dihydrogen phosphate is 5:1.
Further, the compositions of described preventing and treating Fructus Pruni caterpillar includes the raw material of following weight portion: Nylar, 55 parts;Other Herba Ocimi (Herba Ocimi Pilosi) Alkene, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and sodium dihydrogen phosphate totally 8 parts, benzo three nitrogen The weight ratio of azoles and sodium dihydrogen phosphate is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Fructus Pruni caterpillar, can develop into the pesticide of preventing and treating Fructus Pruni caterpillar.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Fructus Pruni caterpillar
Parts by weight of raw materials compares:
Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and phosphorus Totally 7 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 6:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Fructus Pruni caterpillar
Parts by weight of raw materials compares:
Nylar, 45 parts;Alloocimene, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and phosphorus Totally 6 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 5:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Fructus Pruni caterpillar
Parts by weight of raw materials compares:
Nylar, 55 parts;Alloocimene, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and phosphorus Totally 8 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 7:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Fructus Pruni caterpillar
Parts by weight of raw materials compares:
Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and phosphorus Totally 7 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 5:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Fructus Pruni caterpillar
Parts by weight of raw materials compares:
Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and phosphorus Totally 7 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 7:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, BTA and sodium dihydrogen phosphate is 4:1
Parts by weight of raw materials compares:
Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and phosphorus Totally 7 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 4:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, BTA and sodium dihydrogen phosphate is 8:1
Parts by weight of raw materials compares:
Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and phosphorus Totally 7 parts of acid dihydride sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 8:1.
Preparation method:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1~7 preventing and treating effective percentage (%) to Fructus Pruni caterpillar.
Test sets chemicals treatment group 1~7 and blank group, and chemicals treatment group 1~7 sprays combination prepared by embodiment 1~7 respectively Thing, blank group sprays clear water.Chemicals treatment group agent fountain height 20g/hm in terms of Nylar2.Plot area is 50m2, with The group arrangement of machine district.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture's field efficacy Test rule, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
Preventing and treating effective percentage (%)
Embodiment 1 99
Embodiment 4 93
Embodiment 5 92
Embodiment 6 65
Embodiment 7 67
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Fructus Pruni caterpillar, can develop into the pesticide of preventing and treating Fructus Pruni caterpillar, Prevention effect is relevant with the weight ratio of synergist BTA and sodium dihydrogen phosphate in raw material, BTA and di(2-ethylhexyl)phosphate When the weight ratio of hydrogen sodium is 5~7:1, prevention effect is best.If without alloocimene, the preventing and treating of the present composition has Efficiency is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this. It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off Essence and protection domain from technical solution of the present invention.

Claims (5)

1. the compositions preventing and treating Fructus Pruni caterpillar, it is characterised in that include the raw material of following weight portion: Nylar, 45~55 parts; Alloocimene, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist BTA and sodium dihydrogen phosphate Totally 6~8 parts, the weight ratio of BTA and sodium dihydrogen phosphate is 5~7:1.
The compositions of preventing and treating Fructus Pruni caterpillar the most according to claim 1, it is characterised in that include the raw material of following weight portion: Nylar, 50 parts;Alloocimene, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist BTA and di(2-ethylhexyl)phosphate Totally 7 parts of hydrogen sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 6:1.
The compositions of preventing and treating Fructus Pruni caterpillar the most according to claim 1, it is characterised in that include the raw material of following weight portion: Nylar, 45 parts;Alloocimene, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist BTA and di(2-ethylhexyl)phosphate Totally 6 parts of hydrogen sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 5:1.
The compositions of preventing and treating Fructus Pruni caterpillar the most according to claim 1, it is characterised in that include the raw material of following weight portion: Nylar, 55 parts;Alloocimene, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist BTA and di(2-ethylhexyl)phosphate Totally 8 parts of hydrogen sodium, the weight ratio of BTA and sodium dihydrogen phosphate is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves Nylar, alloocimene and synergist BTA G & W;
Step S2, by sodium dihydrogen phosphate water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
CN201610474207.1A 2016-06-22 2016-06-22 Composition for preventing and treating illiberis psychina and preparing method thereof Pending CN105994278A (en)

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Application Number Priority Date Filing Date Title
CN201610474207.1A CN105994278A (en) 2016-06-22 2016-06-22 Composition for preventing and treating illiberis psychina and preparing method thereof

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101822252A (en) * 2010-01-27 2010-09-08 深圳诺普信农化股份有限公司 Pyriproxyfen-containing insecticide composition and application thereof
CN105123699A (en) * 2015-10-22 2015-12-09 唐睿 Miticide and insecticide composite containing thymol and pyriproxyfen

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101822252A (en) * 2010-01-27 2010-09-08 深圳诺普信农化股份有限公司 Pyriproxyfen-containing insecticide composition and application thereof
CN105123699A (en) * 2015-10-22 2015-12-09 唐睿 Miticide and insecticide composite containing thymol and pyriproxyfen

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
徐仁权 等: "0.5%吡丙醚颗粒剂对白纹伊蚊控制效果的研究", 《中国媒介生物学及控制杂志》 *
於文俊 等: "吡丙醚及其复配剂对柑桔红蜡蚧的防治试验研究", 《上海农业科技》 *
汪佳晴 等: "18种植物挥发物对柳黑毛蚜行为的调控效应", 《热带作物学报》 *

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