CN106070220A - A kind of compositions preventing and treating two-spotted spider mite and preparation method thereof - Google Patents
A kind of compositions preventing and treating two-spotted spider mite and preparation method thereof Download PDFInfo
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- CN106070220A CN106070220A CN201610394804.3A CN201610394804A CN106070220A CN 106070220 A CN106070220 A CN 106070220A CN 201610394804 A CN201610394804 A CN 201610394804A CN 106070220 A CN106070220 A CN 106070220A
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- octyldiphenylamine
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- mercaptopropionic acid
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/26—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
- A01N43/28—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/04—Oxygen or sulfur attached to an aliphatic side-chain of a carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/06—Nitrogen directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
Abstract
The invention discloses a kind of compositions preventing and treating two-spotted spider mite and preparation method thereof, including the raw material of following weight portion: difenolan, 45～55 parts；Agarospirol, 25～35 parts；Glycerol, 120～140 parts；Water, 390～410 parts；Synergist di-iso-octyldiphenylamine and mercaptopropionic acid totally 6～8 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5～7:1.The compositions that the present invention provides can prevent and treat two-spotted spider mite, the pesticide of preventing and treating two-spotted spider mite can be developed into, prevention effect is relevant with the weight ratio of synergist di-iso-octyldiphenylamine and mercaptopropionic acid in raw material, when the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5～7:1, prevention effect is best.And, it is little that the present composition sprays dose, is difficult to residual.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating two-spotted spider mite and preparation method thereof.
Background technology
Two-spotted spider mite is the general designation of tetranychid of Cotton Gossypii of causing harm, including Tetranychus cinnabarinus, Mite, Tetranychus urticae etc..Cinnabaris
Tetranychus Acarina Tetranychidae.If demodicid mite, one-tenth demodicid mite clustering draw juice in blade back, making blade is canescence or the thin speckle of withered yellow, sternly
During weight, blade is withered comes off, and weaves silk on leaf and knot, and serious affects growth and development of plants.In raw 10-20 generation in year, is (by north orientation south
By increasing), overwintering stage and place are different with area, survive the winter with female one-tenth demodicid mite in North China in weeds, dry branches and fallen leaves and soil seam；?
Survive the winter in weeds and bark are stitched with various worm states in Central China；Surviving the winter on weeds with female one-tenth demodicid mite in Sichuan, heavy rain has inhibitory action.
Have not yet to see difenolan and work in coordination with the report preventing and treating two-spotted spider mite with agarospirol.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating two-spotted spider mite containing difenolan and agarospirol compositions and
Application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating two-spotted spider mite, including the raw material of following weight portion: difenolan, 45～55 parts；Lignum Aquilariae Resinatum spiral shell
Alcohol, 25～35 parts；Glycerol, 120～140 parts；Water, 390～410 parts；Synergist di-iso-octyldiphenylamine and mercaptopropionic acid totally 6～
8 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5～7:1.
Further, the compositions of described preventing and treating two-spotted spider mite includes the raw material of following weight portion: difenolan, 50 parts；
Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and mercaptopropionic acid totally 7 parts, two is different pungent
The weight ratio of base diphenylamines and mercaptopropionic acid is 6:1.
Further, the compositions of described preventing and treating two-spotted spider mite includes the raw material of following weight portion: difenolan, 45 parts；
Agarospirol, 25 parts；Glycerol, 120 parts；Water, 390 parts；Synergist di-iso-octyldiphenylamine and mercaptopropionic acid totally 6 parts, two is different pungent
The weight ratio of base diphenylamines and mercaptopropionic acid is 5:1.
Further, the compositions of described preventing and treating two-spotted spider mite includes the raw material of following weight portion: difenolan, 55 parts；
Agarospirol, 35 parts；Glycerol, 140 parts；Water, 410 parts；Synergist di-iso-octyldiphenylamine and mercaptopropionic acid totally 8 parts, two is different pungent
The weight ratio of base diphenylamines and mercaptopropionic acid is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat two-spotted spider mite, can develop into the pesticide of preventing and treating two-spotted spider mite.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating two-spotted spider mite
Parts by weight of raw materials compares:
Difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 6:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating two-spotted spider mite
Parts by weight of raw materials compares:
Difenolan, 45 parts；Agarospirol, 25 parts；Glycerol, 120 parts；Water, 390 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 6 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating two-spotted spider mite
Parts by weight of raw materials compares:
Difenolan, 55 parts；Agarospirol, 35 parts；Glycerol, 140 parts；Water, 410 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 8 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 7:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating two-spotted spider mite
Parts by weight of raw materials compares:
Difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating two-spotted spider mite
Parts by weight of raw materials compares:
Difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 7:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, di-iso-octyldiphenylamine and mercaptopropionic acid is 4:1
Parts by weight of raw materials compares:
Difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 4:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, di-iso-octyldiphenylamine and mercaptopropionic acid is 8:1
Parts by weight of raw materials compares:
Difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and
Mercaptopropionic acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 8:1.
Preparation method:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage (%) to two-spotted spider mite.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 20g/hm in terms of difenolan2.Plot area is
50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 96 |
| Embodiment 4 | 93 |
| Embodiment 5 | 92 |
| Embodiment 6 | 65 |
| Embodiment 7 | 67 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat two-spotted spider mite, can develop into the cotton red spider of preventing and treating
The pesticide of spider, prevention effect is relevant with the weight ratio of synergist di-iso-octyldiphenylamine and mercaptopropionic acid in raw material, and two is different
When the weight ratio of octyl diphenylamine and mercaptopropionic acid is 5～7:1, prevention effect is best.If without agarospirol, this
The preventing and treating effective percentage of bright compositions is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating two-spotted spider mite, it is characterised in that include the raw material of following weight portion: difenolan, 45～55
Part；Agarospirol, 25～35 parts；Glycerol, 120～140 parts；Water, 390～410 parts；Synergist di-iso-octyldiphenylamine and sulfydryl
Propanoic acid totally 6～8 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5～7:1.
The compositions of preventing and treating two-spotted spider mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: difenolan, 50 parts；Agarospirol, 30 parts；Glycerol, 130 parts；Water, 400 parts；Synergist di-iso-octyldiphenylamine and sulfydryl third
Acid totally 7 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 6:1.
The compositions of preventing and treating two-spotted spider mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: difenolan, 45 parts；Agarospirol, 25 parts；Glycerol, 120 parts；Water, 390 parts；Synergist di-iso-octyldiphenylamine and sulfydryl third
Acid totally 6 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 5:1.
The compositions of preventing and treating two-spotted spider mite the most according to claim 1, it is characterised in that include the former of following weight portion
Material: difenolan, 55 parts；Agarospirol, 35 parts；Glycerol, 140 parts；Water, 410 parts；Synergist di-iso-octyldiphenylamine and sulfydryl third
Acid totally 8 parts, the weight ratio of di-iso-octyldiphenylamine and mercaptopropionic acid is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves difenolan, agarospirol and synergist di-iso-octyldiphenylamine G & W；
Step S2, by mercaptopropionic acid water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394804.3A CN106070220A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating two-spotted spider mite and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394804.3A CN106070220A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating two-spotted spider mite and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106070220A true CN106070220A (en) | 2016-11-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610394804.3A Pending CN106070220A (en) | 2016-05-31 | 2016-05-31 | A kind of compositions preventing and treating two-spotted spider mite and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114698639A (en) * | 2021-11-09 | 2022-07-05 | 上海生农生化制品股份有限公司 | Mite-killing suspending agent with reduced quantity and enhanced effect and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1185716A (en) * | 1996-03-29 | 1998-06-24 | 梅瑞尔公司 | Insecticidal composition effective against fleas on mammals particularly cats and dogs |
| JP2001506616A (en) * | 1996-12-12 | 2001-05-22 | イサグロ ソシエタ ペル アチオニ | Compositions for systematic control of parasites of constant temperature animals |
| CN1452457A (en) * | 2000-09-05 | 2003-10-29 | 拜尔农作物科学股份公司 | Active ingredient combinations with insecticidal and acaricidal properties |
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2016
- 2016-05-31 CN CN201610394804.3A patent/CN106070220A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1185716A (en) * | 1996-03-29 | 1998-06-24 | 梅瑞尔公司 | Insecticidal composition effective against fleas on mammals particularly cats and dogs |
| JP2001506616A (en) * | 1996-12-12 | 2001-05-22 | イサグロ ソシエタ ペル アチオニ | Compositions for systematic control of parasites of constant temperature animals |
| CN1452457A (en) * | 2000-09-05 | 2003-10-29 | 拜尔农作物科学股份公司 | Active ingredient combinations with insecticidal and acaricidal properties |
Non-Patent Citations (1)
| Title |
|---|
| 刘长令: "杀虫剂及杀螨剂的研究进展", 《农药科学与管理》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114698639A (en) * | 2021-11-09 | 2022-07-05 | 上海生农生化制品股份有限公司 | Mite-killing suspending agent with reduced quantity and enhanced effect and preparation method thereof |
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