CN105994350A - Composition for preventing and treating cotton leaf hoppers and preparation method thereof - Google Patents
Composition for preventing and treating cotton leaf hoppers and preparation method thereof Download PDFInfo
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- CN105994350A CN105994350A CN201610397613.2A CN201610397613A CN105994350A CN 105994350 A CN105994350 A CN 105994350A CN 201610397613 A CN201610397613 A CN 201610397613A CN 105994350 A CN105994350 A CN 105994350A
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- parts
- dialkyl diphenylamine
- preventing
- synergist
- demissine
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/06—Nitrogen directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a composition for preventing and treating cotton leaf hoppers and a preparation method thereof. The composition comprises the following raw materials by weight: 20 to 30 parts of chlorfenvinphos, 10 to 20 parts of demissine, 130 to 150 parts of glycerin, 350 to 370 parts of water and 6 to 8 parts of a synergist consisting of dialkyl diphenylamine and iron citrate, wherein a weight ratio of dialkyl diphenylamine to iron citrate is 5-7: 1. The composition provided by the invention can prevent and treat cotton leaf hoppers and can be developed into a pesticide for preventing and treating cotton leaf hoppers; and the prevention and treatment effect of the composition is related to the weight ratio of dialkyl diphenylamine to iron citrate in the synergist, and optimal prevention and treatment effect is obtained when the weight ratio of dialkyl diphenylamine to iron citrate is 5-7: 1. Moreover, the composition is small in a spraying dosage and hardly leaves residues.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating chlorita biguttula and preparation method thereof.
Background technology
Chlorita biguttula has another name called Amrasca biguttula (Ishida), cotton leafhopper, cotton two leafhoppers etc., inhales juice with one-tenth, nymph in cotton leaf back thorn.State
It is distributed in outward India, Japan.Domestic all have distribution in addition to Xinjiang, and its distribution north is limited to Liaoning, Shanxi, but the most accidental；Gansu
On the south north and south, western Sichuan and Huaihe River, density gradually steps up；The Yangtze river basin and areas to the south thereof, particularly Hubei, Hunan,
The provinces and regions such as Jiangxi, Guangxi, Guizhou occur density higher, and cotton growth later stage almost every leaf has.
Have not yet to see chlorfenviphos and work in coordination with the report preventing and treating chlorita biguttula with demissine.
Summary of the invention
It is an object of the invention to provide a kind of compositions of preventing and treating chlorita biguttula containing chlorfenviphos and demissine and answering in pesticide thereof
With.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating chlorita biguttula, including the raw material of following weight portion: chlorfenviphos, 20～30 parts；Demissine, 10～20
Part；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and ferric citrate totally 6～8 parts, dialkyl group
The weight ratio of diphenylamines and ferric citrate is 5～7:1.
Further, the compositions of described preventing and treating chlorita biguttula includes the raw material of following weight portion: chlorfenviphos, 25 parts；Demissine,
15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and ferric citrate totally 7 parts, dialkyl diphenylamine
It is 6:1 with the weight ratio of ferric citrate.
Further, the compositions of described preventing and treating chlorita biguttula includes the raw material of following weight portion: chlorfenviphos, 20 parts；Demissine,
10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and ferric citrate totally 6 parts, dialkyl diphenylamine
It is 5:1 with the weight ratio of ferric citrate.
Further, the compositions of described preventing and treating chlorita biguttula includes the raw material of following weight portion: chlorfenviphos, 30 parts；Demissine,
20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and ferric citrate totally 8 parts, dialkyl diphenylamine
It is 7:1 with the weight ratio of ferric citrate.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat chlorita biguttula, can develop into the pesticide of preventing and treating chlorita biguttula.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent
The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention
Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating chlorita biguttula
Parts by weight of raw materials compares:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 6:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating chlorita biguttula
Parts by weight of raw materials compares:
Chlorfenviphos, 20 parts；Demissine, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 6 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 5:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating chlorita biguttula
Parts by weight of raw materials compares:
Chlorfenviphos, 30 parts；Demissine, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 8 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 7:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating chlorita biguttula
Parts by weight of raw materials compares:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 5:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating chlorita biguttula
Parts by weight of raw materials compares:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 7:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, dialkyl diphenylamine and ferric citrate is 4:1
Parts by weight of raw materials compares:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 4:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, dialkyl diphenylamine and ferric citrate is 8:1
Parts by weight of raw materials compares:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and lemon
Lemon acid ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 8:1.
Preparation method:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage (%) to chlorita biguttula.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 sprays combination prepared by embodiment 1～7 respectively
Thing, blank group sprays clear water.Chemicals treatment group agent fountain height 50g/hm in terms of chlorfenviphos2.Plot area is 50m2, with
The group arrangement of machine district.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture's field efficacy
Test rule, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 97 |
| Embodiment 4 | 92 |
| Embodiment 5 | 93 |
| Embodiment 6 | 63 |
| Embodiment 7 | 64 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat chlorita biguttula, can develop into the pesticide of preventing and treating chlorita biguttula,
Prevention effect is relevant with the weight ratio of synergist dialkyl diphenylamine and ferric citrate in raw material, dialkyl diphenylamine and Fructus Citri Limoniae
When the weight ratio of acid ferrum is 5～7:1, prevention effect is best.If without demissine, the preventing and treating of the present composition is effective
Rate is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this.
It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off
Essence and protection domain from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating chlorita biguttula, it is characterised in that include the raw material of following weight portion: chlorfenviphos, 20～30 parts；
Demissine, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and ferric citrate are altogether
6～8 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 5～7:1.
The compositions of preventing and treating chlorita biguttula the most according to claim 1, it is characterised in that include the raw material of following weight portion:
Chlorfenviphos, 25 parts；Demissine, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and citric acid
Ferrum totally 7 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 6:1.
The compositions of preventing and treating chlorita biguttula the most according to claim 1, it is characterised in that include the raw material of following weight portion:
Chlorfenviphos, 20 parts；Demissine, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and citric acid
Ferrum totally 6 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 5:1.
The compositions of preventing and treating chlorita biguttula the most according to claim 1, it is characterised in that include the raw material of following weight portion:
Chlorfenviphos, 30 parts；Demissine, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and citric acid
Ferrum totally 8 parts, the weight ratio of dialkyl diphenylamine and ferric citrate is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves chlorfenviphos, demissine and synergist dialkyl diphenylamine G & W；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610397613.2A CN105994350A (en) | 2016-06-01 | 2016-06-01 | Composition for preventing and treating cotton leaf hoppers and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610397613.2A CN105994350A (en) | 2016-06-01 | 2016-06-01 | Composition for preventing and treating cotton leaf hoppers and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105994350A true CN105994350A (en) | 2016-10-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610397613.2A Pending CN105994350A (en) | 2016-06-01 | 2016-06-01 | Composition for preventing and treating cotton leaf hoppers and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104273162A (en) * | 2014-09-16 | 2015-01-14 | 青岛永通电梯工程有限公司 | Efficient insecticide containing chlorfenvinphos, cyphenothrin and amitraz |
| CN104273161A (en) * | 2014-09-16 | 2015-01-14 | 青岛永通电梯工程有限公司 | Efficient insecticide containing fenvalerate, fipronil and chlorfenvinphos |
| CN104273168A (en) * | 2014-09-29 | 2015-01-14 | 青岛康和食品有限公司 | Efficient insecticide containing spirotetramat, acephate and chlorfenvinphos |
-
2016
- 2016-06-01 CN CN201610397613.2A patent/CN105994350A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104273162A (en) * | 2014-09-16 | 2015-01-14 | 青岛永通电梯工程有限公司 | Efficient insecticide containing chlorfenvinphos, cyphenothrin and amitraz |
| CN104273161A (en) * | 2014-09-16 | 2015-01-14 | 青岛永通电梯工程有限公司 | Efficient insecticide containing fenvalerate, fipronil and chlorfenvinphos |
| CN104273168A (en) * | 2014-09-29 | 2015-01-14 | 青岛康和食品有限公司 | Efficient insecticide containing spirotetramat, acephate and chlorfenvinphos |
Non-Patent Citations (1)
| Title |
|---|
| 巩江等: "龙葵素的药理·毒理及药用研究", 《安徽农业科学》 * |
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Application publication date: 20161012 |