CN105994362A - Composition for preventing and treating tomato brown rot and preparation method thereof - Google Patents
Composition for preventing and treating tomato brown rot and preparation method thereof Download PDFInfo
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- CN105994362A CN105994362A CN201610394840.XA CN201610394840A CN105994362A CN 105994362 A CN105994362 A CN 105994362A CN 201610394840 A CN201610394840 A CN 201610394840A CN 105994362 A CN105994362 A CN 105994362A
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- propylene glycol
- magnesium sulfate
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/14—Ethers
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/08—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a composition for preventing and treating tomato brown rot and a preparation method thereof, wherein the method comprises the following raw materials in parts by weight: 25-35 parts of butethrin, 15-25 parts of yunnancoronarin, 135-155 parts of propylene glycol, 425-445 parts of water, and synergists of propylene glycol phenyl ether and magnesium sulfate with the total amount of 7-9 parts, wherein the weight part ratio of propylene glycol phenyl ether to magnesium sulfate is (6-8) to 1. The composition provided by the invention can prevent and treat the tomato brown rot, can be developed into a pesticide for preventing and treating the tomato brown rot, and has the preventing and treating effect related to the weight part ratio of the synergist propylene glycol phenyl ether to the synergist magnesium sulfate in the raw materials; when the weight part ratio of propylene glycol phenyl ether to magnesium sulfate is (6-8) to 1, the preventing and treating effect is the best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Fructus Lycopersici esculenti cotton disease and preparation method thereof.
Background technology
Fructus Lycopersici esculenti cotton disease is to have generation in the important disease of Fructus Lycopersici esculenti, open country and canopy room.Occur for fragmentary, indivedual plot sickness rate
High.Meet cloudy weather for several days running weather, plant disease epidemic when temperature is higher, often result in destructive disaster.
Have not yet to see the report of butethrin and Yunnan Hedychium coronarium Koenig penta element collaborative preventing and treating Fructus Lycopersici esculenti cotton disease.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating Fructus Lycopersici esculenti cotton disease containing butethrin and Yunnan Hedychium coronarium Koenig penta element compositions and
Application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Fructus Lycopersici esculenti cotton disease, including the raw material of following weight portion: butethrin, 25～35 parts；Yunnan Hedychium coronarium Koenig
Penta element, 15～25 parts；Propylene glycol, 135～155 parts；Water, 425～445 parts；Synergist propylene glycol phenylate and magnesium sulfate totally 7～9
Part, the weight ratio of propylene glycol phenylate and magnesium sulfate is 6～8:1.
Further, the compositions of described preventing and treating Fructus Lycopersici esculenti cotton disease includes the raw material of following weight portion: butethrin, 30 parts；
Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Totally 8 parts of synergist propylene glycol phenylate and magnesium sulfate, third
The weight ratio of glycol phenylate and magnesium sulfate is 7:1.
Further, the compositions of described preventing and treating Fructus Lycopersici esculenti cotton disease includes the raw material of following weight portion: butethrin, 25 parts；
Yunnan Hedychium coronarium Koenig penta element, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Totally 7 parts of synergist propylene glycol phenylate and magnesium sulfate, third
The weight ratio of glycol phenylate and magnesium sulfate is 6:1.
Further, the compositions of described preventing and treating Fructus Lycopersici esculenti cotton disease includes the raw material of following weight portion: butethrin, 35 parts；
Yunnan Hedychium coronarium Koenig penta element, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Totally 9 parts of synergist propylene glycol phenylate and magnesium sulfate, third
The weight ratio of glycol phenylate and magnesium sulfate is 8:1.
The preparation method of above-mentioned composition, it is characterised in that comprise the steps:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Fructus Lycopersici esculenti cotton disease, can develop into the pesticide of preventing and treating Fructus Lycopersici esculenti cotton disease.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent
The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention
Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Fructus Lycopersici esculenti cotton disease
Parts by weight of raw materials compares:
Butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 7:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Fructus Lycopersici esculenti cotton disease
Parts by weight of raw materials compares:
Butethrin, 25 parts；Yunnan Hedychium coronarium Koenig penta element, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Synergist propylene glycol phenyl
Totally 7 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 6:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Fructus Lycopersici esculenti cotton disease
Parts by weight of raw materials compares:
Butethrin, 35 parts；Yunnan Hedychium coronarium Koenig penta element, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Synergist propylene glycol phenyl
Totally 9 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 8:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Fructus Lycopersici esculenti cotton disease
Parts by weight of raw materials compares:
Butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 6:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Fructus Lycopersici esculenti cotton disease
Parts by weight of raw materials compares:
Butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 8:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 6: comparative example, the weight ratio of propylene glycol phenylate and magnesium sulfate is 5:1
Parts by weight of raw materials compares:
Butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 5:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 7: comparative example, the weight ratio of propylene glycol phenylate and magnesium sulfate is 9:1
Parts by weight of raw materials compares:
Butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 9:1.
Preparation method:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage (%) to Fructus Lycopersici esculenti cotton disease.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 sprays combination prepared by embodiment 1～7 respectively
Thing, blank group sprays clear water.Chemicals treatment group agent fountain height 40g/hm in terms of butethrin2.Plot area is 50m2,
The group arrangement of random district.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture's field medicine
Effect test rule, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 95 |
| Embodiment 4 | 91 |
| Embodiment 5 | 92 |
| Embodiment 6 | 66 |
| Embodiment 7 | 68 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Fructus Lycopersici esculenti cotton disease, can develop into preventing and treating Fructus Lycopersici esculenti cotton disease
Pesticide, prevention effect is relevant with the weight ratio of synergist propylene glycol phenylate and magnesium sulfate in raw material, propylene glycol phenylate and sulfur
When the weight ratio of acid magnesium is 6～8:1, prevention effect is best.If without Yunnan Hedychium coronarium Koenig penta element, the preventing and treating of the present composition
Effective percentage is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this.
It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off
Essence and protection domain from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating Fructus Lycopersici esculenti cotton disease, it is characterised in that include the raw material of following weight portion: butethrin, 25～35
Part；Yunnan Hedychium coronarium Koenig penta element, 15～25 parts；Propylene glycol, 135～155 parts；Water, 425～445 parts；Synergist propylene glycol phenylate and sulfur
Totally 7～9 parts of magnesium of acid, the weight ratio of propylene glycol phenylate and magnesium sulfate is 6～8:1.
The compositions of preventing and treating Fructus Lycopersici esculenti cotton disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: butethrin, 30 parts；Yunnan Hedychium coronarium Koenig penta element, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist propylene glycol phenyl
Totally 8 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 7:1.
The compositions of preventing and treating Fructus Lycopersici esculenti cotton disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: butethrin, 25 parts；Yunnan Hedychium coronarium Koenig penta element, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Synergist propylene glycol phenyl
Totally 7 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 6:1.
The compositions of preventing and treating Fructus Lycopersici esculenti cotton disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: butethrin, 35 parts；Yunnan Hedychium coronarium Koenig penta element, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Synergist propylene glycol phenyl
Totally 9 parts of ether and magnesium sulfate, the weight ratio of propylene glycol phenylate and magnesium sulfate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by butethrin, Yunnan Hedychium coronarium Koenig penta element and synergist propylene glycol phenylate propylene glycol and water dissolution；
Step S2, by magnesium sulfate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394840.XA CN105994362A (en) | 2016-05-31 | 2016-05-31 | Composition for preventing and treating tomato brown rot and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610394840.XA CN105994362A (en) | 2016-05-31 | 2016-05-31 | Composition for preventing and treating tomato brown rot and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105994362A true CN105994362A (en) | 2016-10-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610394840.XA Pending CN105994362A (en) | 2016-05-31 | 2016-05-31 | Composition for preventing and treating tomato brown rot and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105994362A (en) |
-
2016
- 2016-05-31 CN CN201610394840.XA patent/CN105994362A/en active Pending
Non-Patent Citations (4)
| Title |
|---|
| 农业部种植业管理司 等编著，: "《中国农药进出口商品编码实用手册》", 31 December 2006, 中国农业出版社 * |
| 刘丽娟 等，: ""姜花属植物中化学成分的研究进展"", 《中山大学研究生学刊(自然科学、医学版)》 * |
| 赵庆 等，: ""滇姜花新二萜成分的研究"", 《高等学校化学学报》 * |
| 陈雪梅 等，: ""具有杀菌活性的新型二萜化合物合成"", 《有机化学》 * |
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Application publication date: 20161012 |
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