CN105961418A - Composition for controlling prodenia litura, and preparation method thereof - Google Patents

Composition for controlling prodenia litura, and preparation method thereof Download PDF

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Publication number
CN105961418A
CN105961418A CN201610474284.7A CN201610474284A CN105961418A CN 105961418 A CN105961418 A CN 105961418A CN 201610474284 A CN201610474284 A CN 201610474284A CN 105961418 A CN105961418 A CN 105961418A
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CN
China
Prior art keywords
parts
triethanolamine
decanedioic acid
cartap
prodenia litura
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CN201610474284.7A
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Chinese (zh)
Inventor
赵思璐
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Individual
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Individual
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Priority to CN201610474284.7A priority Critical patent/CN105961418A/en
Publication of CN105961418A publication Critical patent/CN105961418A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/12Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing a —O—CO—N< group, or a thio analogue thereof, neither directly attached to a ring nor the nitrogen atom being a member of a heterocyclic ring
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/30Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests characterised by the surfactants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02Amines; Quaternary ammonium compounds
    • A01N33/08Amines; Quaternary ammonium compounds containing oxygen or sulfur
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A01N37/04Saturated carboxylic acids or thio analogues thereof; Derivatives thereof polybasic
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system

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  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a composition for controlling prodenia litura, and a preparation method thereof. The composition comprises raw materials in parts by weight as follows: 45-55 parts of cartap, 25-35 parts of byak-angelicin, 120-140 parts of glycerol, 390-410 parts of water, and 6-8 parts of synergists triethanolamine and disodium sebacate in a weight part ratio of (5-7):1. The composition provided by the invention can control prodenia litura, and can be developed into pesticides for controlling prodenia litura; the control effect relates to the weight part ratio of synergists triethanolamine and disodium sebacate, and the control effect is the best when the synergists triethanolamine and disodium sebacate are in the weight part ratio of (5-7):1. Moreover, the composition is small in spray amount, and low in probability of remaining.

Description

A kind of compositions preventing and treating Prodenia litura and preparation method thereof
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Prodenia litura and preparation method thereof.
Background technology
Cartap belongs to moderate toxicity insecticide.Under normal operation to eyes and skin without anaphylaxis.Have no carcinogenic, teratogenesis, Mutagenic action.Poisonous to fish, poisonous to Apis and silkworm, to birds low toxicity, nontoxic to natural enemies such as Araneas.
One species of spodoptera Lepidoptera Noctuidae spodoptera.Crop pests.Worldwide distribution.China is except green grass or young crops Outside extra large, Xinjiang is the brightest, each province is found.
Have not yet to see cartap and work in coordination with the report preventing and treating Prodenia litura with byak-angelicin.
Summary of the invention
It is an object of the invention to provide the compositions of a kind of preventing and treating Prodenia litura containing cartap and byak-angelicin and in pesticide Application.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Prodenia litura, including the raw material of following weight portion: cartap, 45~55 parts;Byak-angelicin, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist triethanolamine and decanedioic acid disodium totally 6~8 parts, three The weight ratio of ethanolamine and decanedioic acid disodium is 5~7:1.
Further, the compositions of described preventing and treating Prodenia litura includes the raw material of following weight portion: cartap, 50 parts;Work as in vain Gui Su, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and decanedioic acid disodium totally 7 parts, triethanolamine It is 6:1 with the weight ratio of decanedioic acid disodium.
Further, the compositions of described preventing and treating Prodenia litura includes the raw material of following weight portion: cartap, 45 parts;Work as in vain Gui Su, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist triethanolamine and decanedioic acid disodium totally 6 parts, triethanolamine It is 5:1 with the weight ratio of decanedioic acid disodium.
Further, the compositions of described preventing and treating Prodenia litura includes the raw material of following weight portion: cartap, 55 parts;Work as in vain Gui Su, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist triethanolamine and decanedioic acid disodium totally 8 parts, triethanolamine It is 7:1 with the weight ratio of decanedioic acid disodium.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Prodenia litura, can develop into the pesticide of preventing and treating Prodenia litura.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Prodenia litura
Parts by weight of raw materials compares:
Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 7 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 6:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Prodenia litura
Parts by weight of raw materials compares:
Cartap, 45 parts;Byak-angelicin, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 6 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 5:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Prodenia litura
Parts by weight of raw materials compares:
Cartap, 55 parts;Byak-angelicin, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 8 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 7:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Prodenia litura
Parts by weight of raw materials compares:
Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 7 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 5:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Prodenia litura
Parts by weight of raw materials compares:
Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 7 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 7:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 6: comparative example, the weight ratio of triethanolamine and decanedioic acid disodium is 4:1
Parts by weight of raw materials compares:
Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 7 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 4:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 7: comparative example, the weight ratio of triethanolamine and decanedioic acid disodium is 8:1
Parts by weight of raw materials compares:
Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and the last of the ten Heavenly stems two Acid disodium totally 7 parts, the weight ratio of triethanolamine and decanedioic acid disodium is 8:1.
Preparation method:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1~7 preventing and treating effective percentage (%) to Prodenia litura.
Test sets chemicals treatment group 1~7 and blank group, and chemicals treatment group 1~7 sprays combination prepared by embodiment 1~7 respectively Thing, blank group sprays clear water.Chemicals treatment group agent fountain height 20g/hm in terms of cartap2.Plot area is 50m2, with The group arrangement of machine district.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture's field efficacy Test rule, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
Preventing and treating effective percentage (%)
Embodiment 1 96
Embodiment 4 93
Embodiment 5 92
Embodiment 6 65
Embodiment 7 67
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Prodenia litura, can develop into the agriculture of preventing and treating Prodenia litura Medicine, prevention effect is relevant with the weight ratio of synergist triethanolamine and decanedioic acid disodium in raw material, triethanolamine and decanedioic acid When the weight ratio of disodium is 5~7:1, prevention effect is best.If without byak-angelicin, the preventing and treating of the present composition has Efficiency is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this. It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off Essence and protection domain from technical solution of the present invention.

Claims (5)

1. the compositions preventing and treating Prodenia litura, it is characterised in that include the raw material of following weight portion: cartap, 45~55 Part;Byak-angelicin, 25~35 parts;Glycerol, 120~140 parts;Water, 390~410 parts;Synergist triethanolamine and decanedioic acid two Totally 6~8 parts of sodium, the weight ratio of triethanolamine and decanedioic acid disodium is 5~7:1.
The compositions of preventing and treating Prodenia litura the most according to claim 1, it is characterised in that include the raw material of following weight portion: Cartap, 50 parts;Byak-angelicin, 30 parts;Glycerol, 130 parts;Water, 400 parts;Synergist triethanolamine and decanedioic acid two Totally 7 parts of sodium, the weight ratio of triethanolamine and decanedioic acid disodium is 6:1.
The compositions of preventing and treating Prodenia litura the most according to claim 1, it is characterised in that include the raw material of following weight portion: Cartap, 45 parts;Byak-angelicin, 25 parts;Glycerol, 120 parts;Water, 390 parts;Synergist triethanolamine and decanedioic acid two Totally 6 parts of sodium, the weight ratio of triethanolamine and decanedioic acid disodium is 5:1.
The compositions of preventing and treating Prodenia litura the most according to claim 1, it is characterised in that include the raw material of following weight portion: Cartap, 55 parts;Byak-angelicin, 35 parts;Glycerol, 140 parts;Water, 410 parts;Synergist triethanolamine and decanedioic acid two Totally 8 parts of sodium, the weight ratio of triethanolamine and decanedioic acid disodium is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves cartap, byak-angelicin and synergist triethanolamine G & W;
Step S2, by decanedioic acid disodium water dissolution;
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
CN201610474284.7A 2016-06-22 2016-06-22 Composition for controlling prodenia litura, and preparation method thereof Pending CN105961418A (en)

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CN201610474284.7A CN105961418A (en) 2016-06-22 2016-06-22 Composition for controlling prodenia litura, and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610474284.7A CN105961418A (en) 2016-06-22 2016-06-22 Composition for controlling prodenia litura, and preparation method thereof

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CN105961418A true CN105961418A (en) 2016-09-28

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101755776A (en) * 2009-11-17 2010-06-30 陕西汤普森生物科技有限公司 Pesticidal composition containing cartap and flubendiamide
CN102224825A (en) * 2011-04-25 2011-10-26 青岛海利尔药业有限公司 Pesticide composition containing sulfoxaflor and nereistoxin compound
CN103053581A (en) * 2012-12-29 2013-04-24 广东中迅农科股份有限公司 Insecticidal composition of indoxacarb and cartap
CN103109822A (en) * 2013-01-28 2013-05-22 江苏省中国科学院植物研究所 Application of byakangelicin used as agricultural insect antifeedant and pesticide

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101755776A (en) * 2009-11-17 2010-06-30 陕西汤普森生物科技有限公司 Pesticidal composition containing cartap and flubendiamide
CN102224825A (en) * 2011-04-25 2011-10-26 青岛海利尔药业有限公司 Pesticide composition containing sulfoxaflor and nereistoxin compound
CN103053581A (en) * 2012-12-29 2013-04-24 广东中迅农科股份有限公司 Insecticidal composition of indoxacarb and cartap
CN103109822A (en) * 2013-01-28 2013-05-22 江苏省中国科学院植物研究所 Application of byakangelicin used as agricultural insect antifeedant and pesticide

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Application publication date: 20160928