CN106106515A - A kind of compositions preventing and treating striped stem borer and preparation method thereof - Google Patents
A kind of compositions preventing and treating striped stem borer and preparation method thereof Download PDFInfo
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- CN106106515A CN106106515A CN201610474281.3A CN201610474281A CN106106515A CN 106106515 A CN106106515 A CN 106106515A CN 201610474281 A CN201610474281 A CN 201610474281A CN 106106515 A CN106106515 A CN 106106515A
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- China
- Prior art keywords
- parts
- calcium chloride
- dialkyl diphenylamine
- acetofenate
- synergist
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/06—Nitrogen directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating striped stem borer and preparation method thereof, including the raw material of following weight portion: acetofenate, 20～30 parts；Petunidin, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Totally 6～8 parts of synergist dialkyl diphenylamine and calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 5～7:1.The compositions that the present invention provides can prevent and treat striped stem borer, the pesticide of preventing and treating striped stem borer can be developed into, prevention effect is relevant with the weight ratio of synergist dialkyl diphenylamine and calcium chloride in raw material, and when the weight ratio of dialkyl diphenylamine and calcium chloride is 5～7:1, prevention effect is best.And, it is little that the present composition sprays dose, is difficult to residual.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating striped stem borer and preparation method thereof.
Background technology
Acetofenate Yuan Xi Bayer A.G product, is that country is permitted producible unique organochlorine class parasite killing at present
Agent.Acetofenate belongs to low toxic pesticide, degradable, to rat acute LD50 of passing through mouth > 10000 mg/kg, acute percutaneous
LD50 > 3500 mg/kg, does not has teratogenesis, mutagenesis and stays toxicity animal.Acetofenate is that a kind of preferably domestic are defended
Raw insecticide.Currently mainly it is applied to mosquito eradication tablet, in the preparation of mosquito eradication smoking paper.Mosquitos and flies is had extremely strong fumigation action of contace poison.
During SARS in 2003, Guangzhou health bureau uses mosquito eradication tablet that each corner or spot as yet untouched by a clean-up campaign is carried out mosquitos and flies in a large number and kills sterilization, obtains
Good effect.Former medicine content % >=95, trichlorine parasite killing fat can also prepare 20%, and 30% cream is to meet agricultural chemical insecticide
Demand.
Striped stem borer is Lepidoptera, Pyralidae.It is distributed in Chinese most of province, often mixes generation with Pyrausta nubilalis (Hubern)..Mainly
Harm Sorghum vulgare Pers. and Semen Maydis, also endanger the crops such as foxtail millet, Caulis Sacchari sinensis, Semen Coicis, fiber crops.The stem stalk boring moth crop with larva is caused harm, by moth stem stalk
Larva number head or ten remainder clusters seen from, killed strain suffers wind to be easily converted into deaf ear and affect yield and quality.Be injured plant seedling
Hour form withered heart Seedling, lobus cardiacus be injured expansion time have irregular translucent speckle or worm channel, near have particulate frass.
Have not yet to see acetofenate and work in coordination with the report preventing and treating striped stem borer with petunidin.
Summary of the invention
It is an object of the invention to provide the compositions of a kind of preventing and treating striped stem borer containing acetofenate and petunidin
And the application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating striped stem borer, including the raw material of following weight portion: acetofenate, 20～30 parts；Short
Lead a cow element, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and calcium chloride totally 6～
8 parts, the weight ratio of dialkyl diphenylamine and calcium chloride is 5～7:1.
Further, the compositions of described preventing and treating striped stem borer includes the raw material of following weight portion: acetofenate, 25
Part；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Totally 7 parts of synergist dialkyl diphenylamine and calcium chloride, dialkyl group two
The weight ratio of aniline and calcium chloride is 6:1.
Further, the compositions of described preventing and treating striped stem borer includes the raw material of following weight portion: acetofenate, 20
Part；Petunidin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Totally 6 parts of synergist dialkyl diphenylamine and calcium chloride, dialkyl group two
The weight ratio of aniline and calcium chloride is 5:1.
Further, the compositions of described preventing and treating striped stem borer includes the raw material of following weight portion: acetofenate, 30
Part；Petunidin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Totally 8 parts of synergist dialkyl diphenylamine and calcium chloride, dialkyl group two
The weight ratio of aniline and calcium chloride is 7:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat striped stem borer, can develop into the pesticide of preventing and treating striped stem borer.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating striped stem borer
Parts by weight of raw materials compares:
Acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine
With totally 7 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 6:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating striped stem borer
Parts by weight of raw materials compares:
Acetofenate, 20 parts；Petunidin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine
With totally 6 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 5:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating striped stem borer
Parts by weight of raw materials compares:
Acetofenate, 30 parts；Petunidin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine
With totally 8 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 7:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating striped stem borer
Parts by weight of raw materials compares:
Acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine
With totally 7 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 5:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating striped stem borer
Parts by weight of raw materials compares:
Acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine
With totally 7 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 7:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, dialkyl diphenylamine and calcium chloride is 4:1
Parts by weight of raw materials compares:
Acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine
With totally 7 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 4:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, dialkyl diphenylamine and calcium chloride is 8:1
Parts by weight of raw materials compares:
Acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine
With totally 7 parts of calcium chloride, the weight ratio of dialkyl diphenylamine and calcium chloride is 8:1.
Preparation method:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage (%) to striped stem borer.
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 50g/hm in terms of acetofenate2.Plot area
For 50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Between test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 97 |
| Embodiment 4 | 92 |
| Embodiment 5 | 93 |
| Embodiment 6 | 63 |
| Embodiment 7 | 64 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat striped stem borer, can develop into preventing and treating Sorghum vulgare Pers. bar
The pesticide of snout moth's larva, prevention effect is relevant with the weight ratio of synergist dialkyl diphenylamine and calcium chloride in raw material, dialkyl group two
When the weight ratio of aniline and calcium chloride is 5～7:1, prevention effect is best.If without petunidin, the present composition
Preventing and treating effective percentage less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating striped stem borer, it is characterised in that include the raw material of following weight portion: acetofenate, 20
～30 parts；Petunidin, 10～20 parts；Glycerol, 130～150 parts；Water, 350～370 parts；Synergist dialkyl diphenylamine and chlorine
Changing calcium totally 6～8 parts, the weight ratio of dialkyl diphenylamine and calcium chloride is 5～7:1.
The compositions of preventing and treating striped stem borer the most according to claim 1, it is characterised in that include the former of following weight portion
Material: acetofenate, 25 parts；Petunidin, 15 parts；Glycerol, 140 parts；Water, 360 parts；Synergist dialkyl diphenylamine and chlorination
Calcium totally 7 parts, the weight ratio of dialkyl diphenylamine and calcium chloride is 6:1.
The compositions of preventing and treating striped stem borer the most according to claim 1, it is characterised in that include the former of following weight portion
Material: acetofenate, 20 parts；Petunidin, 10 parts；Glycerol, 130 parts；Water, 350 parts；Synergist dialkyl diphenylamine and chlorination
Calcium totally 6 parts, the weight ratio of dialkyl diphenylamine and calcium chloride is 5:1.
The compositions of preventing and treating striped stem borer the most according to claim 1, it is characterised in that include the former of following weight portion
Material: acetofenate, 30 parts；Petunidin, 20 parts；Glycerol, 150 parts；Water, 370 parts；Synergist dialkyl diphenylamine and chlorination
Calcium totally 8 parts, the weight ratio of dialkyl diphenylamine and calcium chloride is 7:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, dissolves acetofenate, petunidin and synergist dialkyl diphenylamine G & W；
Step S2, by calcium chloride water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610474281.3A CN106106515A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating striped stem borer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610474281.3A CN106106515A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating striped stem borer and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106106515A true CN106106515A (en) | 2016-11-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610474281.3A Pending CN106106515A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating striped stem borer and preparation method thereof |
Country Status (1)
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| CN (1) | CN106106515A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103004803A (en) * | 2013-01-21 | 2013-04-03 | 山东滨农科技有限公司 | Insecticide composition containing fluorous cyantraniliprole and emamectin benzoate |
| CN104472483A (en) * | 2014-12-31 | 2015-04-01 | 广州甘蔗糖业研究所 | Proceras venosatus sex pheromone microsphere and preparing method thereof |
| CN104824010A (en) * | 2015-05-20 | 2015-08-12 | 北京大北农科技集团股份有限公司 | Application of insecticidal protein |
-
2016
- 2016-06-22 CN CN201610474281.3A patent/CN106106515A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103004803A (en) * | 2013-01-21 | 2013-04-03 | 山东滨农科技有限公司 | Insecticide composition containing fluorous cyantraniliprole and emamectin benzoate |
| CN104472483A (en) * | 2014-12-31 | 2015-04-01 | 广州甘蔗糖业研究所 | Proceras venosatus sex pheromone microsphere and preparing method thereof |
| CN104824010A (en) * | 2015-05-20 | 2015-08-12 | 北京大北农科技集团股份有限公司 | Application of insecticidal protein |
Non-Patent Citations (1)
| Title |
|---|
| 刘善政: "高效低毒杀虫剂—三氯杀虫酯", 《河南科技》 * |
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