CN106070303A - A kind of compositions preventing and treating celery septoria disease and preparation method thereof - Google Patents
A kind of compositions preventing and treating celery septoria disease and preparation method thereof Download PDFInfo
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- CN106070303A CN106070303A CN201610397621.7A CN201610397621A CN106070303A CN 106070303 A CN106070303 A CN 106070303A CN 201610397621 A CN201610397621 A CN 201610397621A CN 106070303 A CN106070303 A CN 106070303A
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- Prior art keywords
- parts
- tricresyl phosphate
- ferric citrate
- alanycarb
- compositions
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/10—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
- A01N47/24—Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating celery septoria disease and preparation method thereof, including the raw material of following weight portion: alanycarb, 25～35 parts；Ailantholide, 15～25 parts；Propylene glycol, 135～155 parts；Water, 425～445 parts；Synergist tricresyl phosphate and ferric citrate totally 7～9 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6～8:1.The compositions that the present invention provides can prevent and treat celery septoria disease, the pesticide of preventing and treating celery septoria disease can be developed into, prevention effect is relevant with the weight ratio of synergist tricresyl phosphate and ferric citrate in raw material, when the weight ratio of tricresyl phosphate and ferric citrate is 6～8:1, prevention effect is best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating celery septoria disease and preparation method thereof.
Background technology
Alanycarb is applicable on vegetable, Fructus Vitis viniferae, Cotton Gossypii prevent and treat coleoptera, Semiptera and lepidoptera pest.
Celery septoria disease has another name called Herba Apii graveolentis late blight, leaf blight.It is the important disease of Winter-Spring protecting field and seed collecting Herba Apii graveolentis, occurs
Universal and serious, yield and quality are affected bigger.This disease can also continue harm in the storing phase.
Have not yet to see alanycarb and work in coordination with the report preventing and treating celery septoria disease with ailantholide.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating celery septoria disease containing alanycarb and ailantholide compositions and
Its application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating celery septoria disease, including the raw material of following weight portion: alanycarb, 25～35 parts；Ailanthus altissima (mill.) swingle
Lactone, 15～25 parts；Propylene glycol, 135～155 parts；Water, 425～445 parts；Synergist tricresyl phosphate and ferric citrate totally 7
～9 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6～8:1.
Further, the compositions of described preventing and treating celery septoria disease includes the raw material of following weight portion: alanycarb, 30
Part；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and ferric citrate totally 8 parts, phosphoric acid
The weight ratio of front three phenolic ester and ferric citrate is 7:1.
Further, the compositions of described preventing and treating celery septoria disease includes the raw material of following weight portion: alanycarb, 25
Part；Ailantholide, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Synergist tricresyl phosphate and ferric citrate totally 7 parts, phosphoric acid
The weight ratio of front three phenolic ester and ferric citrate is 6:1.
Further, the compositions of described preventing and treating celery septoria disease includes the raw material of following weight portion: alanycarb, 35
Part；Ailantholide, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Synergist tricresyl phosphate and ferric citrate totally 9 parts, phosphoric acid
The weight ratio of front three phenolic ester and ferric citrate is 8:1.
The preparation method of above-mentioned composition, it is characterised in that comprise the steps:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat celery septoria disease, can develop into the pesticide of preventing and treating celery septoria disease.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating celery septoria disease
Parts by weight of raw materials compares:
Alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and
Ferric citrate totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 7:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating celery septoria disease
Parts by weight of raw materials compares:
Alanycarb, 25 parts；Ailantholide, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Synergist tricresyl phosphate and
Ferric citrate totally 7 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating celery septoria disease
Parts by weight of raw materials compares:
Alanycarb, 35 parts；Ailantholide, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Synergist tricresyl phosphate and
Ferric citrate totally 9 parts, the weight ratio of tricresyl phosphate and ferric citrate is 8:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating celery septoria disease
Parts by weight of raw materials compares:
Alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and
Ferric citrate totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating celery septoria disease
Parts by weight of raw materials compares:
Alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and
Ferric citrate totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 8:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, tricresyl phosphate and ferric citrate is 5:1
Parts by weight of raw materials compares:
Alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and
Ferric citrate totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 5:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, tricresyl phosphate and ferric citrate is 9:1
Parts by weight of raw materials compares:
Alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and
Ferric citrate totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 9:1.
Preparation method:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
Use the field test compositions that respectively prepared by the testing example 1～7 preventing and treating effective percentage to celery septoria disease
(%).
Test sets chemicals treatment group 1～7 and blank group, and chemicals treatment group 1～7 is sprayed embodiment 1～7 respectively and prepared
Compositions, blank group spray clear water.Chemicals treatment group agent fountain height 40g/hm in terms of alanycarb2.Plot area is
50m2, random district group arranges.It is repeated 4 times.Use workers and peasants-16 aerosol apparatus spray medicine, spouting liquid 750kg/hm2.With reference to Ministry of Agriculture field
Test of pesticide effectiveness criterion, 15d after medicine, calculate preventing and treating effective percentage (%).
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 95 |
| Embodiment 4 | 91 |
| Embodiment 5 | 92 |
| Embodiment 6 | 66 |
| Embodiment 7 | 68 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat celery septoria disease, can develop into preventing and treating Herba Apii graveolentis
The pesticide of spot blight, prevention effect is relevant with the weight ratio of synergist tricresyl phosphate and ferric citrate in raw material, phosphorus
When the weight ratio of acid front three phenolic ester and ferric citrate is 6～8:1, prevention effect is best.If without ailantholide, this
The preventing and treating effective percentage of bright compositions is less than 50%.And, it is little that the present composition sprays dose, is difficult to residual.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating celery septoria disease, it is characterised in that include the raw material of following weight portion: alanycarb, 25～
35 parts；Ailantholide, 15～25 parts；Propylene glycol, 135～155 parts；Water, 425～445 parts；Synergist tricresyl phosphate and lemon
Lemon acid ferrum totally 7～9 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6～8:1.
The compositions of preventing and treating celery septoria disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: alanycarb, 30 parts；Ailantholide, 20 parts；Propylene glycol, 145 parts；Water, 435 parts；Synergist tricresyl phosphate and citric acid
Ferrum totally 8 parts, the weight ratio of tricresyl phosphate and ferric citrate is 7:1.
The compositions of preventing and treating celery septoria disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: alanycarb, 25 parts；Ailantholide, 15 parts；Propylene glycol, 135 parts；Water, 425 parts；Synergist tricresyl phosphate and citric acid
Ferrum totally 7 parts, the weight ratio of tricresyl phosphate and ferric citrate is 6:1.
The compositions of preventing and treating celery septoria disease the most according to claim 1, it is characterised in that include the former of following weight portion
Material: alanycarb, 35 parts；Ailantholide, 25 parts；Propylene glycol, 155 parts；Water, 445 parts；Synergist tricresyl phosphate and citric acid
Ferrum totally 9 parts, the weight ratio of tricresyl phosphate and ferric citrate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by alanycarb, ailantholide and synergist tricresyl phosphate propylene glycol and water dissolution；
Step S2, by ferric citrate water dissolution；
Step S3, slowly adds the solution of step S2 in the solution of step S1, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610397621.7A CN106070303A (en) | 2016-06-01 | 2016-06-01 | A kind of compositions preventing and treating celery septoria disease and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610397621.7A CN106070303A (en) | 2016-06-01 | 2016-06-01 | A kind of compositions preventing and treating celery septoria disease and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106070303A true CN106070303A (en) | 2016-11-09 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610397621.7A Pending CN106070303A (en) | 2016-06-01 | 2016-06-01 | A kind of compositions preventing and treating celery septoria disease and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106070303A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1613784A (en) * | 2004-10-28 | 2005-05-11 | 上海交通大学 | Method for light catalytic degrading carbamate pesticide in water |
| JP2011148760A (en) * | 2009-12-25 | 2011-08-04 | Sumitomo Chemical Co Ltd | Offensive insect pest-controlling composition |
| CN104663687A (en) * | 2013-11-26 | 2015-06-03 | 中国中化股份有限公司 | Insecticidal and acaricidal composition containing carbamate insecticide |
-
2016
- 2016-06-01 CN CN201610397621.7A patent/CN106070303A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1613784A (en) * | 2004-10-28 | 2005-05-11 | 上海交通大学 | Method for light catalytic degrading carbamate pesticide in water |
| JP2011148760A (en) * | 2009-12-25 | 2011-08-04 | Sumitomo Chemical Co Ltd | Offensive insect pest-controlling composition |
| CN104663687A (en) * | 2013-11-26 | 2015-06-03 | 中国中化股份有限公司 | Insecticidal and acaricidal composition containing carbamate insecticide |
Non-Patent Citations (2)
| Title |
|---|
| 谭庆伟等: ""臭椿化学成分及生物活性研究进展"", 《天然产物研究与开发》 * |
| 黄硕等: ""新型氨基甲酸酯类杀虫剂棉铃威的合成及其杀虫效果"", 《精细化工中间体》 * |
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Application publication date: 20161109 |