CN106087441A - 皮划艇用帆布及其制备方法 - Google Patents

皮划艇用帆布及其制备方法 Download PDF

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Publication number
CN106087441A
CN106087441A CN201610576044.8A CN201610576044A CN106087441A CN 106087441 A CN106087441 A CN 106087441A CN 201610576044 A CN201610576044 A CN 201610576044A CN 106087441 A CN106087441 A CN 106087441A
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Prior art keywords
cloth
undercoating
fire retardant
raw material
external coating
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CN201610576044.8A
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CN106087441B (zh
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王憬义
王云侠
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Ningbo TianDun waterproof material Co., Ltd.
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FENGHUA TIANDUN WATERPROOF MATERIAL Co Ltd
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    • D—TEXTILES; PAPER
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0002—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
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    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
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    • B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
    • B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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    • C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
    • C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
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    • C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
    • C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
    • C09D127/04—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
    • C09D127/06—Homopolymers or copolymers of vinyl chloride
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    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Plant Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Laminated Bodies (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

皮划艇用帆布，包括坯布、内涂层和外涂层，坯布采用长丝机织平纹布，内涂层包括如下重量百分比原料：聚氯乙烯糊树脂25‑35％，邻苯二甲酸二辛酯10‑30％，己二酸二辛酯10‑20％，聚酯型增塑剂8‑10％，轻质碳酸钙20‑35％，二盐基亚磷酸铅2‑5％，二氧化钛1‑3％，防腐剂0.1‑1.5％，阻燃剂0.5‑3％，还包括颜料1‑2％，内涂层厚度为0.5‑1mm。外涂层采用聚丙烯压延膜，包括如下重量百分比原料：聚丙烯树脂60‑70％，紫外线吸收剂0.3‑0.8％，阻燃剂15‑30％，玻璃纤维10‑15％，还包括0.6‑1％颜料，或者采用市购的聚酰胺薄膜，厚度为0.2‑0.4mm。其制备步骤主要为浸轧上浆→烘箱塑化→表面压平→冷却成卷。

Description

皮划艇用帆布及其制备方法
技术领域
本发明涉及一种帆布，尤其是涉及一种皮划艇用帆布，同时涉及其制备方法。
背景技术
现有的制作充气皮划艇的材质大体可以分为两类，分别是橡胶材质和PVC布料材质。
其中橡胶材质的主要成分是天然橡胶，该原材料通过手工收集获取，产量较少，虽然具备耐磨、耐热、抗撕扯、抗屈抗龟裂、气密好、高强度、重量轻等优点，但是橡胶制备工序繁杂造成皮划艇造价成本高，而且不够美观。而PVC布料材质皮划艇的主要成分为塑料涂层布料，能够实现流水线大批量生产，因此成本较低，但是这种材质的皮划艇耐磨性、耐扎刮性较差，经常需要修补。
发明内容
为解决上述技术问题，本发明提供一种皮划艇用帆布，具有抗拉、抗撕、抗剥离、防水耐污的特性，同时不易发霉生菌，适宜制作皮划艇在户外水上长时间使用。
本发明的技术方案是提供一种皮划艇用帆布，包括坯布、内涂层和外涂层。所述坯布采用涤纶长丝机织平纹布，其纬斜范围为0-1％，所述坯布也可称为基布。
所述内涂层为聚氯乙烯树脂，包括如下重量百分比原料：聚氯乙烯糊树脂25-35％，邻苯二甲酸二辛酯10-30％，己二酸二辛酯10-20％，聚酯型增塑剂8-10％，轻质碳酸钙20-35％，二盐基亚磷酸铅2-5％，二氧化钛1-3％，防腐剂0.1-1.5％，阻燃剂0.5-3％，还包括颜料1-2％。所述阻燃剂为膨胀型阻燃剂。
作为进一步改进，所述内涂层包括如下重量百分比原料：聚氯乙烯糊树脂30-35％，邻苯二甲酸二辛酯15-25％，己二酸二辛酯10-15％，聚酯型增塑剂8-10％，轻质碳酸钙20-25％，二盐基亚磷酸铅2-3％，二氧化钛1-3％，防腐剂0.1-1.5％，阻燃剂0.5-3％，还包括颜料1-2％，所述阻燃剂为膨胀型阻燃剂。
优选地，所述内涂层包括如下重量百分比原料：聚氯乙烯糊树脂30％，邻苯二甲酸二辛酯20％，己二酸二辛酯10％，聚酯型增塑剂8％，轻质碳酸钙25％，二盐基亚磷酸铅2.5％，二氧化钛1％，防腐剂0.5％，阻燃剂2％，颜料1％
所述外涂层采用聚丙烯压延膜，包括如下重量百分比原料：聚丙烯树脂60-70％，紫外线吸收剂0.3-0.8％，阻燃剂15-30％，玻璃纤维10-15％，还包括0.6-1％颜料。所述阻燃剂为膨胀型阻燃剂。
作为进一步改进，所述外涂层采用聚丙烯压延膜，包括如下重量百分比原料：聚丙烯树脂60-65％，紫外线吸收剂0.4-0.6％，阻燃剂20-25％，玻璃纤维10-15％，还包括0.5-1％颜料，所述阻燃剂为膨胀型阻燃剂。
优选地，所述聚丙烯压延膜包括如下重量百分比原料：聚丙烯树脂64％，紫外线吸收剂0.5％，阻燃剂22％，玻璃纤维13％，颜料0.5％。
所述外涂层还可以采用聚酰胺薄膜。
所述内涂层厚度为0.5-1mm，所述外涂层厚度0.2-0.4mm。
优选地，所述内涂层厚度为0.5mm。
优选地，所述外涂层厚度为0.2mm。
本发明还提供一种皮划艇用帆布的制备方法，步骤如下：
1)取如下重量百分比原料配制成内涂层：
2)取如下重量百分比原料制成压延膜作为外涂层：
压延膜厚度为0.2-0.4mm。
优选地，压延膜厚度为0.2mm。
此外，可采用市场上常见的聚酰胺薄膜。
3)上述原料调和之后，投放入搅拌桶内，在常温下用搅拌机搅拌均匀，由于其中还会存留少量的颗粒，再用三辊研磨机对搅拌物进行研磨，研磨8-10min之后即可使用。
4)坯布经过清洗后通过烫平牵引机整平烘干，烘干温度为110℃-130℃。优选地烘干温度为120℃。
5)通过浸轧上浆的方式将步骤1)制得的内涂层涂料均匀地涂布于经步骤4)处理的坯布两面，然后通过烘箱塑化处理，烘道长度为5-7m。
涂布时，涂料粘度控制在150-160Pa·s，塑化烘燥时温度为180-200℃。
优选地，涂层粘度控制在155Pa·s，塑化烘燥温度为200℃，烘道长度为6m。
6)在步骤5)制得的布料内涂层2-1上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。
7)将步骤6)制得的布料送入烘箱塑化烘干，烘干温度为170-190℃，烘道长度为8-9m。优选地，烘干温度为180℃，烘道长度为8m。
步骤4)、5)、7)烘干时未将布料完全干燥，以便使布料保持一定的韧性，防止脆化，同时保证内涂层的附着牢固度。
8)将步骤7)制得的布料经冷却压布机冷却整平后，在内涂层2-2上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。并对涂层厚度进行测定，保证涂层均匀。
内涂层厚度控制在0.5-1mm。
优选地，内涂层厚度为0.5mm。
9)将步骤8)制得的布料送入烘箱塑化烘干，烘干温度为140-160℃，烘道长度为20-25m，至布料干透。优选地烘干温度为160℃，烘道长度为25m。
10)将步骤9)经双面双道涂布工艺制得的布料送入压光机整平，并使聚氯乙烯内涂层与布料更加紧密地结合，提升布料的抗拉抗撕和耐水耐磨性能。
11)热熔贴合
将步骤2)所得的外涂层聚丙烯压延膜或者聚酰胺薄膜与步骤10)所得的布料通过压料辊压紧后，进行热熔贴合，热熔温度为150-190℃，受热均匀快速。
优选地，热熔温度为180℃。
根据产品要求，可对布料单面贴膜(形成3-1或者3-2)或者双面贴膜(形成3-1和3-2)。
12)对步骤11)制得的布料再次进行压光处理，使布料平整，并使贴膜与布料贴合更加紧密。经过贴膜处理，布料的抗撕、抗拉、耐水耐磨的性能得到进一步提高。
13)根据产品要求，可以对布料进行表面压花处理。
14)将步骤12)或者步骤13)制得的布料进行冷却。
采用上述技术方案后，本发明具有以下显著优点和有益效果：
通过采用长丝机织平纹布作为坯布，保证本发明帆布基材的强度。坯布上覆聚氯乙烯树脂内涂层，内涂层上覆聚丙烯压延膜或者聚酰胺薄膜，涂布过程中涂料填补了布料纤维间的微小空隙，内外涂层本身具有抗拉性能，加强了纤维之间的张力，提高了布料的气密性，因此提升了帆布的强度、耐磨和防水耐污的性能。并且内涂层或者外涂层配方中的助剂，包括阻燃剂、抗紫外线剂、抗菌防腐剂，使帆布具有防火阻燃、抗紫外线、抗氧化和防霉抗菌的优点。
附图说明
图1为本发明帆布的结构示意图
图2为本发明帆布制备流程示意图
图1中标记1为坯布，标记2-1、2-2为内涂层，标记3-1、3-2为外涂层。
具体实施方式
下面结合实施示例对本发明作进一步说明。
实施例一
1)取如下重量百分比原料配制成内涂层：
2)取如下重量百分比原料制成压延膜作为外涂层：
压延膜厚度为0.2mm。
3)上述原料调和之后，投放入搅拌桶内，在常温下用搅拌机搅拌均匀，由于其中还会存留少量的颗粒，再用三辊研磨机对搅拌物进行研磨，研磨8-10min之后即可使用。
4)坯布经过清洗后通过烫平牵引机整平烘干，烘干温度为130℃。
5)通过浸轧上浆的方式将步骤1)制得的内涂层均匀地涂布于经步骤4)处理的坯布两面，然后通过烘箱塑化处理。
涂布时，涂料粘度为150Pa·s，塑化烘燥温度为180℃，烘道长度为5m。
6)在步骤5)制得的布料内涂层2-1上再次涂布步骤1)的内涂层涂料，增加布料气密性，提升防水性能。
7)将步骤6)制得的布料送入烘箱塑化烘干，烘干温度为170℃，烘道长度为8m。
8)将步骤7)制得的布料经冷却压布机冷却整平后，在内涂层2-2上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。并对涂层厚度进行测定，保证涂层均匀。
9)将步骤8)制得的布料送入烘箱塑化烘干，烘干温度为150℃，烘道长度为20m，至布料干透。
10)将步骤9)的经双面双道涂布工艺制得的布料送入压光机整平，并使聚氯乙烯内涂层与布料更加紧密地结合，提升布料的抗拉抗撕和耐水耐磨性能。
11)热熔贴合
将步骤2)所得的外涂层聚丙烯压延膜与步骤10)所得的布料通过压料辊压紧后，对布料单面进行热熔贴合，热熔温度为150℃，受热均匀快速。
12)对步骤11)制得的布料再次进行压光处理，使布料平整，并使贴膜与布料贴合更加紧密。经过贴膜处理，布料的抗撕、抗拉、耐水耐磨的性能得到进一步提高。
13)根据产品要求，对布料进行表面压花。
14)将步骤13)制得的布料进行冷却。
实施例二
1)取如下重量百分比原料配制成内涂层：
2)上述原料调和之后，投放入搅拌桶内，在常温下用搅拌机搅拌均匀，由于其中还会存留少量的颗粒，再用三辊研磨机对搅拌物进行研磨，研磨8-10min之后即可使用。
3)坯布经过清洗后通过烫平牵引机整平烘干，烘干温度为110℃。
4)通过浸轧上浆的方式将步骤1)制得的内涂层均匀地涂布于经步骤4)处理的坯布两面，然后通过烘箱塑化处理。
涂布时，涂料粘度为160Pa·s，塑化烘燥温度为200℃，烘道长度为6m。
5)在步骤5)制得的布料内涂层2-1上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。
6)将步骤6)制得的布料送入烘箱塑化烘干，烘干温度为180℃，烘道长度为8m。
7)将步骤7)制得的布料经冷却压布机冷却整平后，在内涂层2-2上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。并对涂层厚度进行测定，保证涂层均匀。
8)将步骤8)制得的布料送入烘箱塑化烘干，烘干温度为160℃，烘道长度为23m，至布料干透。
9)将步骤9)的经双面双道涂布工艺制得的布料送入压光机整平，并使聚氯乙烯内涂层与布料更加紧密地结合，提升布料的抗拉抗撕和耐水耐磨性能。
10)热熔贴合
将市场上购得的聚酰胺薄膜与步骤10)所得的布料通过压料辊压紧后，对布料双面进行热熔贴合，热熔温度为180℃，受热均匀快速。
11)对步骤11)制得的布料再次进行压光处理，使布料平整，并使贴膜与布料贴合更加紧密。经过贴膜处理，布料的抗撕、抗拉、耐水耐磨的性能得到进一步提高。
12)根据产品要求，对布料进行表面压花。
13)将步骤12)制得的布料进行冷却。
实施例三
1)取如下重量百分比原料配制成内涂层：
2)取如下重量百分比原料制成压延膜作为外涂层：
压延膜厚度为0.2mm。
3)上述原料调和之后，投放入搅拌桶内，在常温下用搅拌机搅拌均匀，由于其中还会存留少量的颗粒，再用三辊研磨机对搅拌物进行研磨，研磨8-10min之后即可使用。
4)坯布经过清洗后通过烫平牵引机整平烘干，烘干温度为120℃。
5)通过浸轧上浆的方式将步骤1)制得的内涂层均匀地涂布于经步骤4)处理的坯布两面，然后通过烘箱塑化处理。
涂布时，涂料粘度为155Pa·s，塑化烘燥温度为190℃，烘道长度为7m。
6)在步骤5)制得的布料内涂层2-1上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。
7)将步骤6)制得的布料送入烘箱塑化烘干，烘干温度为190℃，烘道长度为9m。
8)将步骤7)制得的布料经冷却压布机冷却整平后，在内涂层2-2上再次涂布步骤1)制得的内涂层涂料，增加布料气密性，提升防水性能。并对涂层厚度进行测定，保证涂层均匀。
9)将步骤8)制得的布料送入烘箱塑化烘干，烘干温度为140℃，烘道长度为25m，至布料干透。
10)将步骤9)的经双面双道涂布工艺制得的布料送入压光机整平，并使聚氯乙烯内涂层与布料更加紧密地结合，提升布料的抗拉抗撕和耐水耐磨性能。
11)热熔贴合
将步骤2)所得的外涂层聚丙烯压延膜与步骤10)所得的布料通过压料辊压紧后，对布料单面进行热熔贴合，热熔温度为160℃，受热均匀快速。
12)对步骤11)制得的布料再次进行压光处理，使布料平整，并使贴膜与布料贴合更加紧密。经过贴膜处理，布料的抗撕、抗拉、耐水耐磨的性能得到进一步提高。
13)将步骤12)制得的布料进行冷却。
制得的皮划艇用帆布产品指标如下：
上述指标检验值均符合或者高于国家标准。因此，采用本发明技术方案，即以涤纶长丝机织平纹布作为坯布，结合聚氯乙烯树脂内涂层，内涂层结合聚丙烯压延膜或者聚酰胺薄膜外涂层，渗入纤维间的聚氯乙烯树脂起到粘合纤维的作用，能够加强纤维之间的张力，提升帆布的强度，帆布表面的内涂层和外涂层进一步提升了布料的气密性，抗冲击性，耐磨和防水耐污的性能，而且内涂层或者外涂层配方中的助剂使帆布具有防火阻燃、抗紫外线、抗氧化和防霉抗菌的优点。

Claims (10)

1.一种皮划艇用帆布，其特征在于，包括坯布、内涂层和外涂层，所述坯布采用涤纶长丝机织平纹布，其纬斜范围为0-1％，所述内涂层包括如下重量百分比原料：聚氯乙烯糊树脂25-35％，邻苯二甲酸二辛酯10-30％，己二酸二辛酯10-20％，聚酯型增塑剂8-10％，轻质碳酸钙20-35％，二盐基亚磷酸铅2-5％，二氧化钛1-3％，防腐剂0.1-1.5％，阻燃剂0.5-3％，还包括颜料1-2％，所述阻燃剂为膨胀型阻燃剂，所述内涂层厚度为0.5-1mm。
2.根据权利要求1所述的皮划艇用帆布，其特征在于，所述内涂层包括如下重量百分比原料：聚氯乙烯糊树脂30-35％，邻苯二甲酸二辛酯15-25％，己二酸二辛酯10-15％，聚酯型增塑剂8-10％，轻质碳酸钙20-25％，二盐基亚磷酸铅2-3％，二氧化钛1-3％，防腐剂0.1-1.5％，阻燃剂0.5-3％，还包括颜料1-2％，所述阻燃剂为膨胀型阻燃剂。
3.根据权利要求1所述的皮划艇用帆布，其特征在于，所述内涂层包括如下重量百分比原料：聚氯乙烯糊树脂30％，邻苯二甲酸二辛酯20％，己二酸二辛酯10％，聚酯型增塑剂8％，轻质碳酸钙25％，二盐基亚磷酸铅2.5％，二氧化钛1％，防腐剂0.5％，阻燃剂2％，颜料1％。
4.根据权利要求1所述的皮划艇用帆布，其特征在于，所述外涂层采用聚丙烯压延膜，包括如下重量百分比原料：聚丙烯树脂60-70％，紫外线吸收剂0.3-0.8％，阻燃剂15-30％，玻璃纤维10-15％，还包括0.5-1％颜料，所述阻燃剂为膨胀型阻燃剂。
5.根据权利要求4所述的皮划艇用帆布，其特征在于，所述外涂层采用聚丙烯压延膜，包括如下重量百分比原料：聚丙烯树脂60-65％，紫外线吸收剂0.4-0.6％，阻燃剂20-25％，玻璃纤维10-15％，还包括0.5-1％颜料，所述阻燃剂为膨胀型阻燃剂。
6.根据权利要求5所述的皮划艇用帆布，其特征在于，所述外涂层包括如下重量百分比原料：聚丙烯树脂64％，紫外线吸收剂0.5％，阻燃剂22％，玻璃纤维13％，颜料0.5％。
7.根据权利要求6所述的皮划艇用帆布，其特征在于，所述外涂层厚度为0.2-0.4mm。
8.根据权利要求1所述的皮划艇用帆布的制备方法，其特征在于，步骤包括如下：
1)根据配方的重量百分比取内涂层和外涂层原料，原料调和之后，投放入搅拌桶内，常温下搅拌均匀，再进行研磨，研磨8-10min；
2)坯布经过清洗后通过烫平牵引机整平烘干，烘干温度为110℃-130℃；
3)通过浸轧上浆的方式将步骤1)制得的内涂层涂层均匀地涂布于经步骤2)处理的坯布两面，然后通过烘箱塑化处理；
4)将塑化烘干的布料送入压光机整平；
5)将步骤2)所得的外涂层聚丙烯压延膜与步骤4)所得的布料通过压料辊压紧后，进行热熔贴合，热熔温度为150-190℃；
6)对步骤5)制得的布料进行压光处理；
7)将步骤6)制得的布料进行冷却。
9.根据权利要求8所述的皮划艇用帆布的制备方法，其特征在于，步骤3)选择的参数为：涂布时，涂料粘度为150-160Pa·s，塑化烘燥温度为160-200℃，烘道长度为5-25m。
10.根据权利要求8所述的皮划艇用帆布的制备方法，其特征在于，在步骤5)中对布料单面或者双面进行热熔贴合处理。
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