CN106087393A - 一种纺织服装面料阻燃抗菌涂层 - Google Patents

一种纺织服装面料阻燃抗菌涂层 Download PDF

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CN106087393A
CN106087393A CN201610617591.6A CN201610617591A CN106087393A CN 106087393 A CN106087393 A CN 106087393A CN 201610617591 A CN201610617591 A CN 201610617591A CN 106087393 A CN106087393 A CN 106087393A
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parts
powder
garment fabric
proof antibiotic
textile garment
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李云海
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Abstract

本发明涉及一种纺织服装面料阻燃抗菌涂层，由以下组分组成：聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉、对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸、多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟。本发明产品具有较为优越的阻燃、耐酸碱、防霉变抗菌性能，改善了产品性能。

Description

一种纺织服装面料阻燃抗菌涂层
技术领域
本发明涉及一种纺织服装面料阻燃抗菌涂层，属于纺织面料技术领域。
背景技术
纺织助剂是纺织品生产加工过程中必须的化学品。纺织助剂对提高纺织品的产品质量和附加价值具有不可或缺的重要作用，它不仅能赋予纺织品各种特殊功能和风格，如柔软、防皱、防缩、防水、抗菌、抗静电、阻燃等，还可以改进染整工艺，起到节约能源和降低加工成本的作用。纺织助剂对提升纺织工业的整体水平以及在纺织产业链中的作用是至关重要的。
发明内容
本发明的目的在于提供一种纺织服装面料阻燃抗菌涂层，以便更好地实现纺织服装面料阻燃抗菌涂层的使用功能，使产品具有阻燃、耐酸碱、防霉变抗菌性能，改善产品使用性能。
为了实现上述目的，本发明的技术方案如下。
一种纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂24～28份、聚对苯二甲酰对苯二胺22～26份、聚甲基丙烯酸酯22～26份、熟桐油20～24份、碳酸二乙酯22～26份、烯丙基硫醚22～26份、亚麻籽油20～24份、硬脂酸甘油酯22～26份、甲硝唑22～26份、壳聚糖20～24份、硫酸铜20～24份、纳米改性竹炭20～24份、二氧化钛粉末22～26份、风化煤20～24份、高铝细粉18～22份、铬酸锂粉末22～26份、铬酸锌20～24份、硅铝酸钠粉末18～22份、硅酸铝粉末20～24份、硅藻粉18～22份、对甲苯酚18～22份、聚磷酸铵20～24份、磷酸三甲酚酯20～24份、六溴环十二烷20～24份、对硝基苯甲酸20～24份、多异氰酸酯20～24份、二苯基硅二醇20～24份、二丙二醇二苯甲酸酯20～24份、二丁基锡二月桂酸酯20～24份、二甲基酮肟18～22份。
进一步地，上述纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂24份、聚对苯二甲酰对苯二胺22份、聚甲基丙烯酸酯22份、熟桐油20份、碳酸二乙酯22份、烯丙基硫醚22份、亚麻籽油20份、硬脂酸甘油酯22份、甲硝唑22份、壳聚糖20份、硫酸铜20份、纳米改性竹炭20份、二氧化钛粉末22份、风化煤20份、高铝细粉18份、铬酸锂粉末22份、铬酸锌20份、硅铝酸钠粉末18份、硅酸铝粉末20份、硅藻粉18份、对甲苯酚18份、聚磷酸铵20份、磷酸三甲酚酯20份、六溴环十二烷20份、对硝基苯甲酸20份、多异氰酸酯20份、二苯基硅二醇20份、二丙二醇二苯甲酸酯20份、二丁基锡二月桂酸酯20份、二甲基酮肟18份。
进一步地，上述纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂26份、聚对苯二甲酰对苯二胺24份、聚甲基丙烯酸酯24份、熟桐油22份、碳酸二乙酯24份、烯丙基硫醚24份、亚麻籽油22份、硬脂酸甘油酯24份、甲硝唑24份、壳聚糖22份、硫酸铜22份、纳米改性竹炭22份、二氧化钛粉末24份、风化煤22份、高铝细粉20份、铬酸锂粉末24份、铬酸锌22份、硅铝酸钠粉末20份、硅酸铝粉末22份、硅藻粉20份、对甲苯酚20份、聚磷酸铵22份、磷酸三甲酚酯22份、六溴环十二烷22份、对硝基苯甲酸22份、多异氰酸酯22份、二苯基硅二醇22份、二丙二醇二苯甲酸酯22份、二丁基锡二月桂酸酯22份、二甲基酮肟20份。
进一步地，上述纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂28份、聚对苯二甲酰对苯二胺26份、聚甲基丙烯酸酯26份、熟桐油24份、碳酸二乙酯26份、烯丙基硫醚26份、亚麻籽油24份、硬脂酸甘油酯26份、甲硝唑26份、壳聚糖24份、硫酸铜24份、纳米改性竹炭24份、二氧化钛粉末26份、风化煤24份、高铝细粉22份、铬酸锂粉末26份、铬酸锌24份、硅铝酸钠粉末22份、硅酸铝粉末24份、硅藻粉22份、对甲苯酚22份、聚磷酸铵24份、磷酸三甲酚酯24份、六溴环十二烷24份、对硝基苯甲酸24份、多异氰酸酯24份、二苯基硅二醇24份、二丙二醇二苯甲酸酯24份、二丁基锡二月桂酸酯24份、二甲基酮肟22份。
进一步地，上述纺织服装面料阻燃抗菌涂层制备方法步骤如下：
(1)将所述质量份数的聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉予以混合，超声高速分散，超声波频率为20～40KHz，分散速度5000～5400r/min左右，分散时间为30～60min；
(2)加入所述质量份数的对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸，超声高速分散，超声波频率为20～35KHz，分散速度4800～5200r/min左右，分散时间为30～50min；
(3)加入所述质量份数的多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟，超声高速分散，超声波频率为20～30KHz，分散速度4600～4800r/min左右，分散时间为20～40min；混合均匀后制得本品。
该发明的有益效果在于：本发明中的纺织服装面料阻燃抗菌涂层，由以下组分组成：聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉、对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸、多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟。本发明产品具有较为优越的阻燃、耐酸碱、防霉变抗菌性能，改善了产品性能。
具体实施方式
下面结合实施例对本发明的具体实施方式进行描述，以便更好的理解本发明。
实施例1
本实施例中的纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂24份、聚对苯二甲酰对苯二胺22份、聚甲基丙烯酸酯22份、熟桐油20份、碳酸二乙酯22份、烯丙基硫醚22份、亚麻籽油20份、硬脂酸甘油酯22份、甲硝唑22份、壳聚糖20份、硫酸铜20份、纳米改性竹炭20份、二氧化钛粉末22份、风化煤20份、高铝细粉18份、铬酸锂粉末22份、铬酸锌20份、硅铝酸钠粉末18份、硅酸铝粉末20份、硅藻粉18份、对甲苯酚18份、聚磷酸铵20份、磷酸三甲酚酯20份、六溴环十二烷20份、对硝基苯甲酸20份、多异氰酸酯20份、二苯基硅二醇20份、二丙二醇二苯甲酸酯20份、二丁基锡二月桂酸酯20份、二甲基酮肟18份。
上述纺织服装面料阻燃抗菌涂层制备方法步骤如下：
(1)将所述质量份数的聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉予以混合，超声高速分散，超声波频率为20kHz，分散速度5400r/min左右，分散时间为60min；
(2)加入所述质量份数的对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸，超声高速分散，超声波频率为20kHz，分散速度5200r/min左右，分散时间为50min；
(3)加入所述质量份数的多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟，超声高速分散，超声波频率为20kHz，分散速度4800r/min左右，分散时间为40min；混合均匀后制得本品。
实施例2
本实施例中的纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂26份、聚对苯二甲酰对苯二胺24份、聚甲基丙烯酸酯24份、熟桐油22份、碳酸二乙酯24份、烯丙基硫醚24份、亚麻籽油22份、硬脂酸甘油酯24份、甲硝唑24份、壳聚糖22份、硫酸铜22份、纳米改性竹炭22份、二氧化钛粉末24份、风化煤22份、高铝细粉20份、铬酸锂粉末24份、铬酸锌22份、硅铝酸钠粉末20份、硅酸铝粉末22份、硅藻粉20份、对甲苯酚20份、聚磷酸铵22份、磷酸三甲酚酯22份、六溴环十二烷22份、对硝基苯甲酸22份、多异氰酸酯22份、二苯基硅二醇22份、二丙二醇二苯甲酸酯22份、二丁基锡二月桂酸酯22份、二甲基酮肟20份。
上述纺织服装面料阻燃抗菌涂层制备方法步骤如下：
(1)将所述质量份数的聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉予以混合，超声高速分散，超声波频率为30kHz，分散速度5200r/min左右，分散时间为45min；
(2)加入所述质量份数的对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸，超声高速分散，超声波频率为27kHz，分散速度5000r/min左右，分散时间为40min；
(3)加入所述质量份数的多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟，超声高速分散，超声波频率为25kHz，分散速度4700r/min左右，分散时间为30min；混合均匀后制得本品。
实施例3
本实施例中的纺织服装面料阻燃抗菌涂层，由以下质量份数的组分组成：聚丁二烯环氧树脂28份、聚对苯二甲酰对苯二胺26份、聚甲基丙烯酸酯26份、熟桐油24份、碳酸二乙酯26份、烯丙基硫醚26份、亚麻籽油24份、硬脂酸甘油酯26份、甲硝唑26份、壳聚糖24份、硫酸铜24份、纳米改性竹炭24份、二氧化钛粉末26份、风化煤24份、高铝细粉22份、铬酸锂粉末26份、铬酸锌24份、硅铝酸钠粉末22份、硅酸铝粉末24份、硅藻粉22份、对甲苯酚22份、聚磷酸铵24份、磷酸三甲酚酯24份、六溴环十二烷24份、对硝基苯甲酸24份、多异氰酸酯24份、二苯基硅二醇24份、二丙二醇二苯甲酸酯24份、二丁基锡二月桂酸酯24份、二甲基酮肟22份。
上述纺织服装面料阻燃抗菌涂层制备方法步骤如下：
(1)将所述质量份数的聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉予以混合，超声高速分散，超声波频率为40kHz，分散速度5000r/min，分散时间为30min；
(2)加入所述质量份数的对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸，超声高速分散，超声波频率为35kHz，分散速度4800r/min，分散时间为30min；
(3)加入所述质量份数的多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟，超声高速分散，超声波频率为30kHz，分散速度4600r/min左右，分散时间为20min；混合均匀后制得本品。
针对实施例1、实施例2和实施例3中的产品和某市售产品进行性能测量，所测得的数据如表1所示。防火阻燃等级测试采用UL94标准。
表1性能测试结果
可见，本发明产品具有较好的耐腐蚀、防火阻燃、防霉变、抗菌性能。
以上所述是本发明的优选实施方式，应当指出，对于本技术领域的普通技术人员来说，在不脱离本发明原理的前提下，还可以做出若干改进和润饰，这些改进和润饰也视为本发明的保护范围。

Claims (5)

1.一种纺织服装面料阻燃抗菌涂层，其特征在于：由以下质量份数的组分组成：聚丁二烯环氧树脂24～28份、聚对苯二甲酰对苯二胺22～26份、聚甲基丙烯酸酯22～26份、熟桐油20～24份、碳酸二乙酯22～26份、烯丙基硫醚22～26份、亚麻籽油20～24份、硬脂酸甘油酯22～26份、甲硝唑22～26份、壳聚糖20～24份、硫酸铜20～24份、纳米改性竹炭20～24份、二氧化钛粉末22～26份、风化煤20～24份、高铝细粉18～22份、铬酸锂粉末22～26份、铬酸锌20～24份、硅铝酸钠粉末18～22份、硅酸铝粉末20～24份、硅藻粉18～22份、对甲苯酚18～22份、聚磷酸铵20～24份、磷酸三甲酚酯20～24份、六溴环十二烷20～24份、对硝基苯甲酸20～24份、多异氰酸酯20～24份、二苯基硅二醇20～24份、二丙二醇二苯甲酸酯20～24份、二丁基锡二月桂酸酯20～24份、二甲基酮肟18～22份。
2.根据权利要求1所述的纺织服装面料阻燃抗菌涂层，其特征在于：所述纺织服装面料阻燃抗菌涂层由以下质量份数的组分组成：聚丁二烯环氧树脂24份、聚对苯二甲酰对苯二胺22份、聚甲基丙烯酸酯22份、熟桐油20份、碳酸二乙酯22份、烯丙基硫醚22份、亚麻籽油20份、硬脂酸甘油酯22份、甲硝唑22份、壳聚糖20份、硫酸铜20份、纳米改性竹炭20份、二氧化钛粉末22份、风化煤20份、高铝细粉18份、铬酸锂粉末22份、铬酸锌20份、硅铝酸钠粉末18份、硅酸铝粉末20份、硅藻粉18份、对甲苯酚18份、聚磷酸铵20份、磷酸三甲酚酯20份、六溴环十二烷20份、对硝基苯甲酸20份、多异氰酸酯20份、二苯基硅二醇20份、二丙二醇二苯甲酸酯20份、二丁基锡二月桂酸酯20份、二甲基酮肟18份。
3.根据权利要求1至2所述的纺织服装面料阻燃抗菌涂层，其特征在于：所述纺织服装面料阻燃抗菌涂层由以下质量份数的组分组成：聚丁二烯环氧树脂26份、聚对苯二甲酰对苯二胺24份、聚甲基丙烯酸酯24份、熟桐油22份、碳酸二乙酯24份、烯丙基硫醚24份、亚麻籽油22份、硬脂酸甘油酯24份、甲硝唑24份、壳聚糖22份、硫酸铜22份、纳米改性竹炭22份、二氧化钛粉末24份、风化煤22份、高铝细粉20份、铬酸锂粉末24份、铬酸锌22份、硅铝酸钠粉末20份、硅酸铝粉末22份、硅藻粉20份、对甲苯酚20份、聚磷酸铵22份、磷酸三甲酚酯22份、六溴环十二烷22份、对硝基苯甲酸22份、多异氰酸酯22份、二苯基硅二醇22份、二丙二醇二苯甲酸酯22份、二丁基锡二月桂酸酯22份、二甲基酮肟20份。
4.根据权利要求1至3所述的纺织服装面料阻燃抗菌涂层，其特征在于：所述纺织服装面料阻燃抗菌涂层由以下质量份数的组分组成：聚丁二烯环氧树脂28份、聚对苯二甲酰对苯二胺26份、聚甲基丙烯酸酯26份、熟桐油24份、碳酸二乙酯26份、烯丙基硫醚26份、亚麻籽油24份、硬脂酸甘油酯26份、甲硝唑26份、壳聚糖24份、硫酸铜24份、纳米改性竹炭24份、二氧化钛粉末26份、风化煤24份、高铝细粉22份、铬酸锂粉末26份、铬酸锌24份、硅铝酸钠粉末22份、硅酸铝粉末24份、硅藻粉22份、对甲苯酚22份、聚磷酸铵24份、磷酸三甲酚酯24份、六溴环十二烷24份、对硝基苯甲酸24份、多异氰酸酯24份、二苯基硅二醇24份、二丙二醇二苯甲酸酯24份、二丁基锡二月桂酸酯24份、二甲基酮肟22份。
5.根据权利要求1所述的纺织服装面料阻燃抗菌涂层，其特征在于：所述纺织服装面料阻燃抗菌涂层制备方法步骤如下：
（1）将所述质量份数的聚丁二烯环氧树脂、聚对苯二甲酰对苯二胺、聚甲基丙烯酸酯、熟桐油、碳酸二乙酯、烯丙基硫醚、亚麻籽油、硬脂酸甘油酯、甲硝唑、壳聚糖、硫酸铜、纳米改性竹炭、二氧化钛粉末、风化煤、高铝细粉、铬酸锂粉末、铬酸锌、硅铝酸钠粉末、硅酸铝粉末、硅藻粉予以混合，超声高速分散，超声波频率为20～40KHz，分散速度约5000～5400r/min，分散时间为30～60min左右；
（2）加入所述质量份数的对甲苯酚、聚磷酸铵、磷酸三甲酚酯、六溴环十二烷、对硝基苯甲酸，超声高速分散，超声波频率为20～35KHz，分散速度为约4800～5200r/min，分散时间为30～50min左右；
（3）加入所述质量份数的多异氰酸酯、二苯基硅二醇、二丙二醇二苯甲酸酯、二丁基锡二月桂酸酯、二甲基酮肟，超声高速分散，超声波频率为20～30KHz，分散速度为约4600～4800r/min，分散时间为20～40min左右；混合均匀后制得本品。
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CN106398514A (zh) * 2016-12-03 2017-02-15 肇庆市天地人科技有限公司 一种安全防护服阻燃抗菌涂层
CN106497370A (zh) * 2016-11-17 2017-03-15 佛山市天顺科技有限公司 一种安全防护服阻燃抗菌涂层
CN106702749A (zh) * 2016-12-13 2017-05-24 中山市得高行知识产权中心（有限合伙） 一种纺织面料表面改性处理剂及其制备方法
CN107190356A (zh) * 2017-05-17 2017-09-22 安徽新生纺织有限公司 一种医疗面料用抗菌防辐射纺丝及其制备方法
JP2019157291A (ja) * 2018-03-12 2019-09-19 株式会社アテックス 繊維製品及びその製造方法
CN111424361A (zh) * 2020-03-31 2020-07-17 江西服装学院 一种阻燃型面料及其制备方法

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106497370A (zh) * 2016-11-17 2017-03-15 佛山市天顺科技有限公司 一种安全防护服阻燃抗菌涂层
CN106398514A (zh) * 2016-12-03 2017-02-15 肇庆市天地人科技有限公司 一种安全防护服阻燃抗菌涂层
CN106702749A (zh) * 2016-12-13 2017-05-24 中山市得高行知识产权中心（有限合伙） 一种纺织面料表面改性处理剂及其制备方法
CN107190356A (zh) * 2017-05-17 2017-09-22 安徽新生纺织有限公司 一种医疗面料用抗菌防辐射纺丝及其制备方法
JP2019157291A (ja) * 2018-03-12 2019-09-19 株式会社アテックス 繊維製品及びその製造方法
CN111424361A (zh) * 2020-03-31 2020-07-17 江西服装学院 一种阻燃型面料及其制备方法

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