CN106070293A - Black cutworm sex pheromone and preparation method thereof and lure - Google Patents

Black cutworm sex pheromone and preparation method thereof and lure Download PDF

Info

Publication number
CN106070293A
CN106070293A CN201610410540.6A CN201610410540A CN106070293A CN 106070293 A CN106070293 A CN 106070293A CN 201610410540 A CN201610410540 A CN 201610410540A CN 106070293 A CN106070293 A CN 106070293A
Authority
CN
China
Prior art keywords
black cutworm
sex pheromone
cutworm sex
lure
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610410540.6A
Other languages
Chinese (zh)
Other versions
CN106070293B (en
Inventor
陈丽萍
高剑龙
张炯森
林志平
谢和凤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhangzhou Enjoy Sci & Tech Development Co Ltd
Original Assignee
Zhangzhou Enjoy Sci & Tech Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhangzhou Enjoy Sci & Tech Development Co Ltd filed Critical Zhangzhou Enjoy Sci & Tech Development Co Ltd
Priority to CN201610410540.6A priority Critical patent/CN106070293B/en
Publication of CN106070293A publication Critical patent/CN106070293A/en
Application granted granted Critical
Publication of CN106070293B publication Critical patent/CN106070293B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N49/00Biocides, pest repellants or attractants, or plant growth regulators, containing compounds containing the group, wherein m+n>=1, both X together may also mean —Y— or a direct carbon-to-carbon bond, and the carbon atoms marked with an asterisk are not part of any ring system other than that which may be formed by the atoms X, the carbon atoms in square brackets being part of any acyclic or cyclic structure, or the group, wherein A means a carbon atom or Y, n>=0, and not more than one of these carbon atoms being a member of the same ring system, e.g. juvenile insect hormones or mimics thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01MCATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M1/00Stationary means for catching or killing insects
    • A01M1/02Stationary means for catching or killing insects with devices or substances, e.g. food, pheronones attracting the insects
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/08Oxygen or sulfur directly attached to an aromatic ring system
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N35/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
    • A01N35/04Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01MCATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
    • A01M2200/00Kind of animal
    • A01M2200/01Insects
    • A01M2200/011Crawling insects

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Wood Science & Technology (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Insects & Arthropods (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catching Or Destruction (AREA)

Abstract

Open a kind of black cutworm sex pheromone of the present invention and preparation method thereof and lure, black cutworm sex pheromone includes following component by mass fraction: 20%~37% along 7 dodecylene acetass, 4%~17% along 9 tetradecene acetass, 23%~the carvacrol of 35% and 2 hydroxyl 4 oxy-octyl benzophenones of 15%~35%;Black cutworm sex pheromone use acetone solution is made black cutworm sex pheromone solution;Black cutworm sex pheromone solution loading release is made lure, is slowly discharged black cutworm sex pheromone by lure.Black cutworm is lured by the present invention has potentiation, can trap and kill male worm, Insect pest suppression in a large number, reach the effect of comprehensive control black cutworm, for the preventing and treating of black cutworm with forecast significant.

Description

Black cutworm sex pheromone and preparation method thereof and lure
Technical field
The present invention relates to insect sex pheromone manufacturing technology field, especially black cutworm sex pheromone and preparation method thereof And lure.
Background technology
Black cutworm another name Stachys geobombycis C. Y. Wu, grub, cutworm etc., belong to Lepidoptera, Noctuidae, be in agricultural production important relatively The subterranean pest-insect of difficult preventing and treating, the young root of main feeding plant, children lotus, tender leaf.Its harm floristics many, can to Cruciferae, Section's various plants such as grass family, Compositae, Semen Maydis, Cotton Gossypii work the mischief.It is widely distributed, the most all has distribution, mainly Generating region at along the lake, extra large, river and level of ground water is higher, humidity is bigger low-lying place, some cotton grains folder kind region, dry farming grains All there is harm in various degree district, Vegetable area etc..
Black cutworm becomes warm, wet environment and fragrant and sweet odoring substance.Therefore, in the big area of soil moisture content, nectar source The field insect density that plant is more, farming is extensive with weedy is big.And the soil that water-retaining property is strong, the soil is porous is also beneficial to The generation of black cutworm.At present the main or method of employing chemical prevention prevent and treat for black cutworm, be usually used in preventing and treating little The medicament of cutworm such as Pyrethrum is cruel, chlorfenapyr, efficient chlorine cyanogen chrysanthemum vinegar, chlopyrifos etc., but rapid due to pest resistance to insecticide Development, conventional chemical pesticide has been difficult to preventing and treating black cutworm.It addition, use the method for chemical prevention to soil and environmental disruption relatively For seriously.
For more environmentally friendly preventing and treating black cutworm and soil protection, people begin with sex pheromone and lure black cutworm Kill.Sex pheromone is by the animal of two sexual lifes, the material discharged for identifying mutually, by this kind of material can make female, Male close, and cause mating.Black cutworm sex pheromone is natural pollution-free due to it, easily operation and the longer feature of lasting effect, Become the control of black cutworm, prediction etc. and have important effect.But current black cutworm sex pheromone is mainly Along 7-dodecylene acetas, along 9-tetradecene acetas both compositions, it is not the strongest to the attracting ability of black cutworm, Trapping efficiency has much room for improvement.
Summary of the invention
It is an object of the invention to provide a kind of black cutworm sex pheromone, black cutworm is lured by it has potentiation work With, male worm, Insect pest suppression can be trapped and killed in a large number, reach the effect of comprehensive control black cutworm.
For achieving the above object, the black cutworm sex pheromone of the present invention, by this sex pheromone bag of mass fraction
Further, black cutworm sex pheromone, include following component by this sex pheromone of mass fraction:
Further preferably, black cutworm sex pheromone, include following component by this sex pheromone of mass fraction:
In said components, live along 7-dodecylene acetas with along 9-tetradecene acetas as the biological of pheromone Property composition for luring the adult of male black cutworm, carvacrol protect active component, prevents activity from becoming as antioxidant Divide oxidized decomposition;Octabenzone, as UV absorbent, matches with antioxidant carvacrol Close, improve the stability of black cutworm sex pheromone;Meanwhile, carvacrol and Octabenzone are also Substantially increase the sucking action of black cutworm sex pheromone;In order to improve the pheromone suction to male black cutworm further Draw, also add isoamyl acetate, owing to isoamyl acetate has a pure and fresh fruital, then coordinate along 7-dodecylene acetas, Along 9-tetradecene acetas, carvacrol and Octabenzone, five kinds of component synergism, to male The stimulation of black cutworm and attraction are more strong, lure worm effect more preferable.Reach the effect of comprehensive control black cutworm, for little The preventing and treating of tiger and forecast significant.
The present invention also provides for the preparation method of above-mentioned black cutworm sex pheromone, and it is to use the above-mentioned little ground of acetone solution old Tiger sex pheromone prepares black cutworm sex pheromone solution.
Preferable amount is: the quality of described black cutworm sex pheromone is 500 to 3000 μ g, and the consumption of described acetone is 100 μ L to 300 μ L.
The present invention also provides for the lure of a kind of black cutworm sex pheromone, including release, by black cutworm sex pheromone Solution is placed in release, prepares black cutworm sex pheromone lure core.
Described release be by natural rubber or synthetic rubber or polyethylene or polrvinyl chloride or paper material or resin or Person's viscose material is made.
Use acetone above-mentioned each component to be dissolved and obtain black cutworm sex pheromone solution, by molten for black cutworm sex pheromone Liquid obtains black cutworm sex pheromone lure core in being placed in release, active component is simple, reasonable mixture ratio, and acetone is by above-mentioned Organic substance Uniform dissolution, loads black cutworm sex pheromone solution in release, slowly discharges, and rate of release is rationally 10 μ g/ hour, The most each release can use 50 hours to 300 hours, and good stability, the persistent period is long.
The present invention is by improveing black cutworm sex pheromone, along 7-dodecylene acetas, along 9-tetradecene Acetas adds carvacrol and the Octabenzone of certain component, improves black cutworm property letter The stability of breath element, and improve the attraction power to black cutworm male worm of black cutworm sex pheromone, can trapping male in a large number Worm, Insect pest suppression, improvement and prediction for black cutworm have significant effect.
Detailed description of the invention
The present invention is further illustrated below by embodiment and comparative example.Lure equipped with black cutworm sex pheromone coordinates Unified trapper trapping black cutworm, relatively the black cutworm sex pheromone of different constituents and consumption is within the set time The black cutworm male worm quantity lured, the attracting ability of the black cutworm quantity the most proofs black cutworm sex pheromone lured is more By force.
Release is as black cutworm sex pheromone carrier, and release uses cuff type rubber below in an example Plug.First cuff type rubber stopper is placed in beaker, adds soaked in absolute ethyl alcohol cuff type rubber stopper 4h;Replacing is used for soaking cuff The ethanol of formula rubber stopper, the beaker that will be equipped with dehydrated alcohol and cuff type rubber stopper is placed in ultrasonic washing unit ultrasonic five minutes; Cuff type rubber stopper after cleaning takes out from beaker, naturally dries, after dehydrated alcohol volatilizees completely, by cuff type rubber Plug seals and preserves, stand-by.
Embodiment 1
Under normal temperature and pressure, it is old that the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 500 μ g makes little ground Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 1, then will be obtained Black cutworm sex pheromone solution be placed in cuff type rubber stopper carrier by liquid-transfering gun, prepare black cutworm sex pheromone lure Core.
Embodiment 2
Under normal temperature and pressure, the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 1000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 2, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 3
Under normal temperature and pressure, the black cutworm sex pheromone using 200 μ L acetone solution gross masses to be 2000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 3, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 4
Under normal temperature and pressure, the black cutworm sex pheromone using 300 μ L acetone solution gross masses to be 3000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 4, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 5
Under normal temperature and pressure, it is old that the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 500 μ g makes little ground Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 5, then will be obtained Black cutworm sex pheromone solution be placed in cuff type rubber stopper carrier by liquid-transfering gun, prepare black cutworm sex pheromone lure Core.
Embodiment 6
Under normal temperature and pressure, the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 1000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 6, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 7
Under normal temperature and pressure, the black cutworm sex pheromone using 200 μ L acetone solution gross masses to be 2000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 7, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 8
Under normal temperature and pressure, the black cutworm sex pheromone using 300 μ L acetone solution gross masses to be 3000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 8, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 9
Under normal temperature and pressure, it is old that the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 500 μ g makes little ground Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 9, then will be obtained Black cutworm sex pheromone solution be placed in cuff type rubber stopper carrier by liquid-transfering gun, prepare black cutworm sex pheromone lure Core.
Embodiment 10
Under normal temperature and pressure, the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 1000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 10, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 11
Under normal temperature and pressure, the black cutworm sex pheromone using 200 μ L acetone solution gross masses to be 2000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 11, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 12
Under normal temperature and pressure, the black cutworm sex pheromone using 300 μ L acetone solution gross masses to be 3000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 12, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 13
Under normal temperature and pressure, it is old that the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 500 μ g makes little ground Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 13, then will be obtained Black cutworm sex pheromone solution be placed in cuff type rubber stopper carrier by liquid-transfering gun, prepare black cutworm sex pheromone lure Core.
Embodiment 14
Under normal temperature and pressure, the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 1000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 14, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Embodiment 15
Under normal temperature and pressure, the black cutworm sex pheromone using 200 μ L acetone solution gross masses to be 2000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 embodiment 15, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares black cutworm sex pheromone Lure.
Comparative example 1
Under normal temperature and pressure, it is old that the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 500 μ g makes little ground Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 comparative example 1, then will be obtained Black cutworm sex pheromone solution be placed in cuff type rubber stopper carrier by liquid-transfering gun, prepare comparative example 1 black cutworm property Pheromone lure.
Comparative example 2
Under normal temperature and pressure, the black cutworm sex pheromone using 100 μ L acetone solution gross masses to be 1000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 comparative example 2, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares comparative example 2 black cutworm Sex pheromone lure core.
Comparative example 3
Under normal temperature and pressure, the black cutworm sex pheromone using 200 μ L acetone solution gross masses to be 2000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 comparative example 3, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares comparative example 3 black cutworm Sex pheromone lure core.
Comparative example 4
Under normal temperature and pressure, the black cutworm sex pheromone using 300 μ L acetone solution gross masses to be 3000 μ g is made littlely Tiger sex pheromone solution, the component of black cutworm sex pheromone and mass fraction, as shown in table 1 comparative example 4, then will be obtained The black cutworm sex pheromone solution obtained is placed in cuff type rubber stopper carrier by liquid-transfering gun, prepares comparative example 4 black cutworm Sex pheromone lure core.
Table 1 embodiment 1-15 and comparative example 1-4 formula table
/ expression does not contains this kind of material.
Field test was carried out on Shi Shi farm, Changtai County of Zhangzhou City of Fujian Province in March, 2015, and this field test area is 100 mu, essentialspecies plant Caulis et Folium Lactucae sativae and Rhizoma Solani tuber osi, field management is consistent, and that a situation arises is close for insect population.Equipped with different embodiments The triangle trapper of black cutworm sex pheromone is randomly arranged in field with checkerboard.
The lure of the black cutworm sex pheromone that will be equipped with embodiment 1 to 15 and comparative example 1 to 4 is arranged on triangle trapping The lure of device is placed in bucket, utilizes the replaceable adhesive boards on triangle trapper to catch black cutworm.Triangle trapper is used Bamboo pole inserts in test field, and triangle trapper distance ground level is 40 cm, higher than Caulis et Folium Lactucae sativae and horse bottom trapper The top of bell potato, to ensure the circulation of trapper surrounding air, it is ensured that affects the natural conditions of black cutworm sex pheromone volatilization Unanimously.The spacing 50m rice of each two trapper, changes the viscose plate of triangle trapper every day, record trapping arrive littlely The data of tiger.After the black cutworm sex pheromone lure core of embodiment 1 to 15 and comparative example 1 to 4 correspondence puts into field test The quantity of corresponding insect-catching quantity, trapping time and average daily insect-catching is as shown in table 2.
Table 2 embodiment 1-15 and comparative example 1-4 insect-catching quantity and trapping timetable
From Table 2, it can be seen that the black cutworm sex pheromone in embodiment 1 to embodiment 4 is included by mass fraction The carvacrol of the Z9-14AC of Z7-12AC, 4%~17%, 23%~33% of 20%~37% and the 2-hydroxyl of 15%~35% Base-4-oxy-octyl benzophenone, average daily insect-catching quantity 17.4, the evaporation rate of black cutworm sex pheromone is 10 μ g/h.
The black cutworm sex pheromone of embodiment 5 to embodiment 15 by mass fraction include the Z7-12AC of 28%~33%, The Octabenzone of the carvacrol of Z9-14AC, 27%~31%, 24%~31% of 11%~15% With the isoamyl acetate of 3%~5%, average daily insect-catching quantity 20.2, the evaporation rate of black cutworm sex pheromone is 10 μ g/h.
The black cutworm sex pheromone of comparative example 1 to comparative example 4 is included the Z7-12AC's and 34% of 66% by mass fraction Z9-14AC, average daily insect-catching quantity 7.2, the evaporation rate of black cutworm sex pheromone is 10 μ g/h.
Knowable to above-mentioned data, include by mass fraction Z7-12AC, 4%~17% of 20%~37% Z9-14AC, The carvacrol of 23%~33% and 15%~35% Octabenzone black cutworm sex pheromone relatively The black cutworm sex pheromone trapping containing the Z7-12AC of 66% and the Z9-14AC of 34% by mass fraction of the prior art The quantity of tigerkin dramatically increases.Black cutworm is not only increased added with carvacrol and Octabenzone The stability of sex pheromone, also significantly increases the sucking action of black cutworm male worm with Z7-12AC and Z9-14AC Synergistic By force.
The little ground adding isoamyl acetate in embodiment 5 to embodiment 15 on the basis of embodiment 1 to embodiment 4 is old The fruital abnormal smells from the patient that tiger sex pheromone is strong owing to isoamyl acetate has, further enhancing pheromone for black cutworm male worm Attraction thus improve average daily insect-catching quantity.
Therefore black cutworm sex pheromone in the present invention and preparation method thereof and lure significantly improve triangle and lure Catch the device trapping capability to black cutworm, it is possible to effectively black cutworm prevented and treated and predict.

Claims (7)

1. black cutworm sex pheromone, it is characterised in that: include following component by this sex pheromone of mass fraction:
Black cutworm sex pheromone the most according to claim 1, it is characterised in that: include by this sex pheromone of mass fraction Following component:
Black cutworm sex pheromone the most according to claim 1, it is characterised in that: include by this sex pheromone of mass fraction Following component:
4. the preparation method of black cutworm sex pheromone, it is characterised in that: use in acetone solution any one of claim 1-3 Black cutworm sex pheromone prepares black cutworm sex pheromone solution.
The preparation method of black cutworm sex pheromone the most according to claim 4, it is characterised in that: described black cutworm property The quality of pheromone is 500 to 3000 μ g, and the consumption of described acetone is 100 μ L to 300 μ L.
6. the lure of black cutworm sex pheromone, it is characterised in that: include release, by black cutworm property described in claim 4 Pheromone solution is placed in release.
The lure of black cutworm sex pheromone the most according to claim 6, it is characterised in that: described release is by natural Rubber or synthetic rubber or polyethylene or polrvinyl chloride or paper material or resin or viscose material are made.
CN201610410540.6A 2016-06-13 2016-06-13 Black cutworm sex pheromone and preparation method thereof and lure Active CN106070293B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610410540.6A CN106070293B (en) 2016-06-13 2016-06-13 Black cutworm sex pheromone and preparation method thereof and lure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610410540.6A CN106070293B (en) 2016-06-13 2016-06-13 Black cutworm sex pheromone and preparation method thereof and lure

Publications (2)

Publication Number Publication Date
CN106070293A true CN106070293A (en) 2016-11-09
CN106070293B CN106070293B (en) 2019-01-22

Family

ID=57845136

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610410540.6A Active CN106070293B (en) 2016-06-13 2016-06-13 Black cutworm sex pheromone and preparation method thereof and lure

Country Status (1)

Country Link
CN (1) CN106070293B (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107286021A (en) * 2017-05-29 2017-10-24 中国农业科学院植物保护研究所 A kind of halo parapheromone analog for being used to prevent and treat Xestia c nigrum
CN107318832A (en) * 2017-08-08 2017-11-07 中国农业科学院植物保护研究所 A kind of sex attractant halogenated analogues for being used to prevent and treat black cutworm
CN107372497A (en) * 2017-08-16 2017-11-24 广西壮族自治区林业科学研究院 A kind of three-spotted plusia attractant and its application process
CN107467020A (en) * 2017-08-20 2017-12-15 中国农业科学院植物保护研究所 A kind of lure composition for being used to prevent and treat black cutworm
CN107836450A (en) * 2017-11-06 2018-03-27 中国农业科学院植物保护研究所 A kind of preparation method and application of big cutworm gyplure
CN108990982A (en) * 2018-08-29 2018-12-14 广西驰胜农业科技有限公司 A kind of lure and preparation method thereof for preventing and treating black cutworm
CN113678827A (en) * 2021-09-06 2021-11-23 广东省科学院动物研究所 Attractant composition for black cutworm larvae and application thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1359618A (en) * 2000-12-21 2002-07-24 中国科学院动物研究所 Sex attractant for small carpenter-worm moth
CN102422831A (en) * 2011-09-30 2012-04-25 北京中捷四方生物科技有限公司 Lure core for controlling proxenus lepigone
CN104186469A (en) * 2014-09-12 2014-12-10 陕西理工学院 Sex attractant and attraction core for attracting chilo suppressalis
CN105409950A (en) * 2015-12-08 2016-03-23 中国农业科学院植物保护研究所 Method for preparing insect attractant based on molecular structure fragment changes

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1359618A (en) * 2000-12-21 2002-07-24 中国科学院动物研究所 Sex attractant for small carpenter-worm moth
CN102422831A (en) * 2011-09-30 2012-04-25 北京中捷四方生物科技有限公司 Lure core for controlling proxenus lepigone
CN104186469A (en) * 2014-09-12 2014-12-10 陕西理工学院 Sex attractant and attraction core for attracting chilo suppressalis
CN105409950A (en) * 2015-12-08 2016-03-23 中国农业科学院植物保护研究所 Method for preparing insect attractant based on molecular structure fragment changes

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107286021A (en) * 2017-05-29 2017-10-24 中国农业科学院植物保护研究所 A kind of halo parapheromone analog for being used to prevent and treat Xestia c nigrum
CN107286021B (en) * 2017-05-29 2020-02-04 中国农业科学院植物保护研究所 Halogenated pheromone analogue for preventing and treating black cutworm
CN107318832A (en) * 2017-08-08 2017-11-07 中国农业科学院植物保护研究所 A kind of sex attractant halogenated analogues for being used to prevent and treat black cutworm
CN107372497A (en) * 2017-08-16 2017-11-24 广西壮族自治区林业科学研究院 A kind of three-spotted plusia attractant and its application process
CN107372497B (en) * 2017-08-16 2020-05-26 广西壮族自治区林业科学研究院 Trichoplusia agnata attractant and application method thereof
CN107467020A (en) * 2017-08-20 2017-12-15 中国农业科学院植物保护研究所 A kind of lure composition for being used to prevent and treat black cutworm
CN107467020B (en) * 2017-08-20 2020-04-24 中国农业科学院植物保护研究所 Attractant composition for preventing and treating black cutworm
CN107836450A (en) * 2017-11-06 2018-03-27 中国农业科学院植物保护研究所 A kind of preparation method and application of big cutworm gyplure
CN108990982A (en) * 2018-08-29 2018-12-14 广西驰胜农业科技有限公司 A kind of lure and preparation method thereof for preventing and treating black cutworm
CN113678827A (en) * 2021-09-06 2021-11-23 广东省科学院动物研究所 Attractant composition for black cutworm larvae and application thereof

Also Published As

Publication number Publication date
CN106070293B (en) 2019-01-22

Similar Documents

Publication Publication Date Title
CN106070293A (en) Black cutworm sex pheromone and preparation method thereof and lure
Ayoola Histopathology of Nile Tilapia (Oreochromis niloticus) juveniles exposed to aqueous and ethanolic extracts of Ipomoea aquatica leaf
CN100490644C (en) Pyralid attractant
Amusan et al. Comparative toxicity effect of bush tea leaves (Hyptis suaveolens) and orange peel (Citrus sinensis) oil extract on larvae of the yellow fever mosquito Aedes aegypti
Marianelli et al. Long‐lasting insecticide‐treated nets: A new integrated pest management approach for Popillia japonica (Coleoptera: Scarabaeidae)
CN100490645C (en) Broad spectrum attractant for tumblebug perfect insects
CN104026117A (en) Method for preventing and controlling pomacea canaliculata
CN102125037A (en) Mosquito trapping liquid
KR101192980B1 (en) Manufacturing method of wildlife animal repellent composition
CN106490025A (en) A kind of booth vegetable insecticidal smoke and preparation method thereof
CN105597126A (en) Botanical disinfection deodorant
CN107439545A (en) A kind of lure composition and its application for being used to prevent and treat black cutworm
CN106508996A (en) Greenhouse pesticide and preparation method thereof
Oluwatoyin Histopathology of Nile Tilapia (Oreochromis niloticus) juveniles exposed to aqueous and ethanolic extracts of Ipomoea aquatica leaf
CN109042645A (en) A kind of flat sawfly attractant of the Chuxiong cheek
CN107047554A (en) With natural plant essential oils attractant that function is trapped for Bemisia tabaci and preparation method thereof
CN101810201A (en) Biological preparation for preventing and treating nest insects
CN106472612A (en) Novel environmentally-friendly biological pesticide
CN106508978A (en) Smoke agent for control of greenhouse botrytis cinerea and preparation method thereof
CN110100846A (en) A kind of production method that can trap and kill acarid
CN105994265B (en) The preparation method of Caloptiliatheivora sex pheromone and its sustained release water-dispersed and the two
CN101796956A (en) Application of allyl isothiocyanate in preparation of phyllotreta striolata attractant, composition thereof and releaser with composition
KR101361703B1 (en) Sex pheromone composition for attraction Synanthedon bicingulata and manufacturing thereof
Alhamda et al. Effectiveness of soursop seed extract (Annona muricata L) as a natural repellent on Aedes aegypti
Pariyasi et al. The Use of Natural Insecticides in the Control of The Aedes Aegypti Mosquito

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant