CN107372497A - A kind of three-spotted plusia attractant and its application process - Google Patents
A kind of three-spotted plusia attractant and its application process Download PDFInfo
- Publication number
- CN107372497A CN107372497A CN201710703804.1A CN201710703804A CN107372497A CN 107372497 A CN107372497 A CN 107372497A CN 201710703804 A CN201710703804 A CN 201710703804A CN 107372497 A CN107372497 A CN 107372497A
- Authority
- CN
- China
- Prior art keywords
- attractant
- spotted plusia
- acetic acid
- lure
- acid esters
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241001367013 Ctenoplusia agnata Species 0.000 title claims abstract description 30
- 239000005667 attractant Substances 0.000 title claims abstract description 30
- 230000031902 chemoattractant activity Effects 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 9
- 239000003960 organic solvent Substances 0.000 claims abstract description 8
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000004128 high performance liquid chromatography Methods 0.000 claims abstract description 3
- 238000002360 preparation method Methods 0.000 claims abstract description 3
- 150000002168 ethanoic acid esters Chemical class 0.000 claims description 12
- 229940099367 lanolin alcohols Drugs 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 9
- 239000000741 silica gel Substances 0.000 claims description 9
- 229910002027 silica gel Inorganic materials 0.000 claims description 9
- 239000004166 Lanolin Substances 0.000 abstract 2
- -1 alcohol acetic acid esters Chemical class 0.000 abstract 2
- 229940039717 lanolin Drugs 0.000 abstract 2
- 235000019388 lanolin Nutrition 0.000 abstract 2
- 230000000694 effects Effects 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000000178 monomer Substances 0.000 description 3
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 240000006497 Dianthus caryophyllus Species 0.000 description 1
- 235000009355 Dianthus caryophyllus Nutrition 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241000256259 Noctuidae Species 0.000 description 1
- 240000002834 Paulownia tomentosa Species 0.000 description 1
- 235000004347 Perilla Nutrition 0.000 description 1
- 244000124853 Perilla frutescens Species 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 244000061458 Solanum melongena Species 0.000 description 1
- 235000002597 Solanum melongena Nutrition 0.000 description 1
- 244000046101 Sophora japonica Species 0.000 description 1
- 235000010586 Sophora japonica Nutrition 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000001418 larval effect Effects 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
- A01M1/00—Stationary means for catching or killing insects
- A01M1/02—Stationary means for catching or killing insects with devices or substances, e.g. food, pheronones attracting the insects
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01M—CATCHING, TRAPPING OR SCARING OF ANIMALS; APPARATUS FOR THE DESTRUCTION OF NOXIOUS ANIMALS OR NOXIOUS PLANTS
- A01M1/00—Stationary means for catching or killing insects
- A01M1/10—Catching insects by using Traps
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Insects & Arthropods (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of three-spotted plusia attractant and its application process, the principle active component of the attractant is to reach more than 98% along 7 lanolin alcohol acetic acid esters, its purity；400 800 μ g are dissolved in 10 μ l organic solvent along 7 lanolin alcohol acetic acid esters during preparation, the organic solvent used for purity more than 98% high performance liquid chromatography n-hexane.Lure is put into trapper by the present invention in application, can be monitored the generation dynamic of field three-spotted plusia, be predicted its occurrence degree, instruct prophylactico-therapeutic measures to carry out in good time, and traps and kills three-spotted plusia simultaneously, has significant ecological benefits and social benefit.
Description
Technical field
The present invention relates to a kind of attractant of trapping pests, be specifically it is a kind of be used to traping rare tree, flowers forest with
And the attractant and its application process of the three-spotted plusia of the polyphagous pest-insect of vegetable crop etc..
Background technology
Three-spotted plusia Argyrogramma agnata Staudinger also known as stain three-spotted plusia, beans looper, belong to squama wing
Mesh, Noctuidae, the whole world are distributed, and are the rare trees such as paulownia, Chinese scholartree, bamboo, carnation, purple perilla, beans, eggplant, flowers
Forest and the important pests of vegetable crop.The worm is endangered with larva, and larval feeding causes blade to be incised or hole, serious hair
Life can eat up whole blades, and 4-7 generations occur for year, and Adult worms producting eggs amount is for up to 700.
The larva of three-spotted plusia have it is binge, at present the prevention and controls of generally use be mostly using black light lamps into
Worm, protection and using natural enemy, Agro-chemicals control etc., but the above method is not only time-consuming, takes a lot of work, effect is not necessarily notable, together
When environment can also be polluted, cause medicament to remain, cause insect resistance, kill the problems such as natural enemy, contaminated food products.
Relevant three-spotted plusia attractant and its application also have research at present, but composition used is more, and material synthesis is difficult
Degree is big, and cost is high.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of attractant and its application process for three-spotted plusia, should
Attractant application is convenient, composition is simple, cost is cheap, selectivity is strong, pollution-free and do not injure natural enemy.
The present invention solves above-mentioned technical problem with following technical scheme：
The principle active component that the attractant that the present invention is used for three-spotted plusia uses is cis- 7- lanolin alcohols acetic acid esters (Z7-
12:AC), its purity reaches more than 98%；The cis- 7- lanolin alcohols acetic acid esters of 400-800 μ g is dissolved in the organic of 10 μ l during preparation
In solvent, the organic solvent that uses for purity more than 98% high performance liquid chromatography n-hexane.
The present invention is used for the application process of the attractant of three-spotted plusia, including following operating procedure：
1) lure is made：Cis- 7- lanolin alcohols acetic acid esters is dissolved in after organic solvent and is put into organic silica gel lure, it is single
The amount of cis- 7- lanolin alcohols acetic acid esters contained by lure is 400-800 μ g；
2) organic silica gel lure is put into trapper, to monitor the generation of field three-spotted plusia dynamic, predicts its generation
Degree, instruct prophylactico-therapeutic measures to carry out in good time, and trap and kill three-spotted plusia simultaneously.
Three-spotted plusia attractant of the present invention has the advantages that：
1. main component of the present invention using cis- 7- lanolin alcohols acetic acid esters as attractant, it can not only monitor adult hair
The raw phase, a large amount of adults can be also killed, reduce population density, mitigate its harm.
2. can directly prevent and treat three-spotted plusia using attractant of the present invention, the use of chemical pesticide can be reduced, improves food peace
Quan Xing, environmental protection and natural enemy, improve the efficiency and effect of preventing and treating three-spotted plusia, and society and ecological benefits are notable.
3. attractant of the present invention application is convenient, composition is simple, cost is cheap, selectivity is strong, pollution-free and do not injure natural enemy.
Brief description of the drawings
Fig. 1 is that the organic silica gel lure that the present invention uses in example 3 is individual with cis- 7- lanolin alcohols acetic acid esters 0-800 μ g/
The Contrast on effect schematic diagram lured of addition.
Embodiment
Three-spotted plusia attractant of the present invention is made below in conjunction with specific embodiment and being further described.
Embodiment 1, tested with common four kinds of moth class attractants：
Moth class monomer attractant known to three kinds is selected in this experiment, and concentration is more than 98%.By attractant according to 400 μ
The dosage of g/ is added in organic silica gel lure, then by these three compositions with 1:1:3 ratio is mixed into attractant D, four kinds
Moth class attractant and its proportioning are shown in Table 1.
1 four kinds of moth class attractants of table and its proportioning
This embodiment includes the monomer dosage of three kinds of moth class attractants and a kind of dosage of mixture.
Embodiment 2, four kinds of moth class timber quarantine three-spotted plusias in example 1 are tested：
The phase occurs in three-spotted plusia, the lure containing 400 μ g attractants is suspended on field, lure with triangle trapper
1 cm distance is kept with trapper bottom surface, counts the adult quantity traped, its effect is shown in Table 2.
Lure three-spotted plusia effect in 2 four kinds of moth class attractant fields of table
This embodiment illustrates that A, C monomer do not have attracting action to three-spotted plusia, and B, D material have to three-spotted plusia and lured
Effect.
Embodiment 3, prepares attractant in the process of the present invention：
1) lure is made：Cis- 7- lanolin alcohols acetic acid esters is dissolved in after organic solvent and is put into organic silica gel lure, will be had
Machine silica gel lure containing cis- 7- lanolin alcohols acetic acid esters as 0 μ g, 400 μ g, tri- groups of 800 μ g to be tested；
2) organic silica gel lure is put into trapper, places into field, statistics trapping adult total quantity, and calculate each
Trapper averagely lures worm amount, and effect is as shown in Figure 1.
Described above, the present invention has been invented a kind of for luring drawing for three-spotted plusia by Field information moth class attractant
Lure, composition is simple, composition is low, operation is easy, available for monitoring and prevent and treat three-spotted plusia.
Claims (2)
1. a kind of three-spotted plusia attractant, it is characterised in that the principle active component of the attractant is cis- 7- lanolin alcohols acetic acid
Ester, its purity reach more than 98%；400-800 μ g cis- 7- lanolin alcohols acetic acid esters is dissolved in 10 μ l organic solvent during preparation
In, the organic solvent that uses for purity more than 98% high performance liquid chromatography n-hexane.
2. the application process of three-spotted plusia attractant according to claim 1, it is characterised in that it includes following operation and walked
Suddenly：
1) lure is made：Cis- 7- lanolin alcohols acetic acid esters is dissolved in after organic solvent and is put into organic silica gel lure, single lure
The amount of contained cis- 7- lanolin alcohols acetic acid esters is 400-800 μ g；
2) organic silica gel lure is put into trapper, to monitor the generation of field three-spotted plusia dynamic, predicts its occurrence degree,
Instruct prophylactico-therapeutic measures to carry out in good time, and trap and kill three-spotted plusia simultaneously.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710703804.1A CN107372497B (en) | 2017-08-16 | 2017-08-16 | Trichoplusia agnata attractant and application method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710703804.1A CN107372497B (en) | 2017-08-16 | 2017-08-16 | Trichoplusia agnata attractant and application method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107372497A true CN107372497A (en) | 2017-11-24 |
| CN107372497B CN107372497B (en) | 2020-05-26 |
Family
ID=60352992
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710703804.1A Active CN107372497B (en) | 2017-08-16 | 2017-08-16 | Trichoplusia agnata attractant and application method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107372497B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221119A (en) * | 2018-11-09 | 2019-01-18 | 中国农业科学院植物保护研究所 | It is a kind of for preventing and treating the sex pheromone composition and application of three-spotted plusia |
| CN109258639A (en) * | 2018-11-09 | 2019-01-25 | 中国农业科学院植物保护研究所 | A kind of three-spotted plusia sex attractant composition and its application |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102669093A (en) * | 2012-04-27 | 2012-09-19 | 董志平 | Highly-efficient sex attractant for Athetis lepigone |
| CN102696596A (en) * | 2012-04-27 | 2012-10-03 | 董志平 | Insect sex attractant comprising butyl hydroxy anisole as synergist |
| CN104488863A (en) * | 2014-12-17 | 2015-04-08 | 广西壮族自治区林业科学研究院 | Sex attractant for melia azedarach cryptophlebia ombrodelta lower |
| CN106070293A (en) * | 2016-06-13 | 2016-11-09 | 漳州市英格尔农业科技有限公司 | Black cutworm sex pheromone and preparation method thereof and lure |
| CN106172395A (en) * | 2016-07-19 | 2016-12-07 | 南京江宁台湾农民创业园发展有限公司 | A kind of three-spotted plusia attractant and application thereof |
-
2017
- 2017-08-16 CN CN201710703804.1A patent/CN107372497B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102669093A (en) * | 2012-04-27 | 2012-09-19 | 董志平 | Highly-efficient sex attractant for Athetis lepigone |
| CN102696596A (en) * | 2012-04-27 | 2012-10-03 | 董志平 | Insect sex attractant comprising butyl hydroxy anisole as synergist |
| CN104488863A (en) * | 2014-12-17 | 2015-04-08 | 广西壮族自治区林业科学研究院 | Sex attractant for melia azedarach cryptophlebia ombrodelta lower |
| CN106070293A (en) * | 2016-06-13 | 2016-11-09 | 漳州市英格尔农业科技有限公司 | Black cutworm sex pheromone and preparation method thereof and lure |
| CN106172395A (en) * | 2016-07-19 | 2016-12-07 | 南京江宁台湾农民创业园发展有限公司 | A kind of three-spotted plusia attractant and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| 湖北省林业学校: "《森林害虫生物防治》", 31 May 1984, 中国林业出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109221119A (en) * | 2018-11-09 | 2019-01-18 | 中国农业科学院植物保护研究所 | It is a kind of for preventing and treating the sex pheromone composition and application of three-spotted plusia |
| CN109258639A (en) * | 2018-11-09 | 2019-01-25 | 中国农业科学院植物保护研究所 | A kind of three-spotted plusia sex attractant composition and its application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107372497B (en) | 2020-05-26 |
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| EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20171124 Assignee: GUANGXI YUKOU INNOVATION AGRICULTURE CO.,LTD. Assignor: GUANGXI ZHUANG AUTONOMOUS REGION FORESTRY Research Institute Contract record no.: X2023980045104 Denomination of invention: A lure for silver striped armyworm and its application method Granted publication date: 20200526 License type: Common License Record date: 20231102 |
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