CN1060684C - 通过缩聚制备液体有机硅氧烷聚合物的方法 - Google Patents
通过缩聚制备液体有机硅氧烷聚合物的方法 Download PDFInfo
- Publication number
- CN1060684C CN1060684C CN94112919A CN94112919A CN1060684C CN 1060684 C CN1060684 C CN 1060684C CN 94112919 A CN94112919 A CN 94112919A CN 94112919 A CN94112919 A CN 94112919A CN 1060684 C CN1060684 C CN 1060684C
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- further characterized
- catalyst
- reative cell
- reagent
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- DXIJHCSGLOHNES-UHFFFAOYSA-N 3,3-dimethylbut-1-enylbenzene Chemical compound CC(C)(C)C=CC1=CC=CC=C1 DXIJHCSGLOHNES-UHFFFAOYSA-N 0.000 description 1
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
- C08G77/08—Preparatory processes characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
- B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/122—Pulverisation by spraying
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Silicon Polymers (AREA)
- Glass Compositions (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
- Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9325342.5 | 1993-12-10 | ||
| GB939325342A GB9325342D0 (en) | 1993-12-10 | 1993-12-10 | Process for polymerisation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1106832A CN1106832A (zh) | 1995-08-16 |
| CN1060684C true CN1060684C (zh) | 2001-01-17 |
Family
ID=10746433
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN94112919A Expired - Lifetime CN1060684C (zh) | 1993-12-10 | 1994-12-08 | 通过缩聚制备液体有机硅氧烷聚合物的方法 |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US5492992A (enExample) |
| EP (1) | EP0657209B1 (enExample) |
| JP (1) | JP3668996B2 (enExample) |
| KR (1) | KR100342326B1 (enExample) |
| CN (1) | CN1060684C (enExample) |
| AT (1) | ATE166798T1 (enExample) |
| AU (1) | AU679583B2 (enExample) |
| BR (1) | BR9404922A (enExample) |
| CA (1) | CA2137645C (enExample) |
| DE (1) | DE69410755T2 (enExample) |
| ES (1) | ES2119092T3 (enExample) |
| GB (1) | GB9325342D0 (enExample) |
| IN (1) | IN183322B (enExample) |
| PL (1) | PL177736B1 (enExample) |
| RU (1) | RU2135528C1 (enExample) |
| TW (1) | TW323291B (enExample) |
| ZA (1) | ZA948933B (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0837842A4 (en) * | 1995-06-07 | 1999-03-31 | Twenty First Century Res Corp | METHODS AND DEVICES FOR OBTAINING INTERMEDIATE OXIDATION PRODUCTS BY CONTROLLING CONVERSIONS AND TEMPERATURES IN AN ATOMIZED LIQUID |
| JPH0995534A (ja) * | 1995-09-28 | 1997-04-08 | Toshiba Silicone Co Ltd | ポリオルガノシロキサン粒子の連続製造方法 |
| US6365670B1 (en) * | 2000-03-10 | 2002-04-02 | Wacker Silicones Corporation | Organopolysiloxane gels for use in cosmetics |
| GB0018162D0 (en) | 2000-07-26 | 2000-09-13 | Dow Corning Sa | Polymerisation reactor and process |
| SE527528C2 (sv) | 2004-06-22 | 2006-04-04 | Bone Support Ab | Anordning för framställning av härdbar massa samt användning av anordningen |
| SG11201703903PA (en) | 2014-11-12 | 2017-06-29 | Univ Houston System | Weather-resistant, fungal-resistant, and stain-resistant coatings and methods of applying on wood, masonry, or other porous materials |
| CA2967599C (en) * | 2014-11-12 | 2023-09-12 | University Of Houston System | Soil-resistant, stain-resistant fluorine-free coatings and methods of applying on materials |
| WO2016077532A1 (en) | 2014-11-12 | 2016-05-19 | University Of Houston System | Soil-resistant, stain-resistant coatings and methods of applying on textile or other flexible materials |
| WO2017079107A1 (en) * | 2015-11-04 | 2017-05-11 | Dow Corning Corporation | Method of preparing organopolysiloxane |
| CN108854930A (zh) * | 2018-08-22 | 2018-11-23 | 江苏先导干燥科技有限公司 | 一种新型智能喷雾反应装置及其反应方法 |
| EP3841154B1 (en) | 2018-08-24 | 2022-09-21 | Dow Silicones Corporation | Method for condensation polymerization of hydroxyl-terminated polydiorganosiloxanes |
| CN112469769B (zh) | 2018-08-24 | 2022-07-08 | 美国陶氏有机硅公司 | 用于羟基封端的聚二有机硅氧烷的缩合聚合的方法 |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1192894A (fr) * | 1957-03-13 | 1959-10-29 | Tno | Procédé et appareil pour la préparation d'un produit pulvérulent |
| FR1367524A (fr) * | 1963-05-11 | 1964-07-24 | Appareil de réaction pour synthèses organiques | |
| EP0080147A2 (en) * | 1981-11-19 | 1983-06-01 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | A process for producing a coagulated latex and apparatus therefor |
| EP0522776A1 (en) * | 1991-07-12 | 1993-01-13 | Dow Corning S.A. | Polymerisation reactor and polymerisation process |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5662803A (en) * | 1979-10-29 | 1981-05-29 | Mitsubishi Electric Corp | Fine particles of crosslinked polymer and their production |
| JPS5662804A (en) * | 1979-10-29 | 1981-05-29 | Mitsubishi Electric Corp | Particles of polymer containing a flame retarder and their production |
| DE3106711C2 (de) * | 1981-02-24 | 1986-07-03 | Dr. Melchior Entwicklungsgesellschaft mbH & Co KG, 5630 Remscheid | Verfahren zur kontinuierlichen Herstellung von kleinen Kunststoffteilchen |
-
1993
- 1993-12-10 GB GB939325342A patent/GB9325342D0/en active Pending
-
1994
- 1994-11-10 ZA ZA948933A patent/ZA948933B/xx unknown
- 1994-11-16 IN IN957CA1994 patent/IN183322B/en unknown
- 1994-11-25 TW TW083110985A patent/TW323291B/zh not_active IP Right Cessation
- 1994-12-05 ES ES94309041T patent/ES2119092T3/es not_active Expired - Lifetime
- 1994-12-05 AT AT94309041T patent/ATE166798T1/de active
- 1994-12-05 US US08/349,658 patent/US5492992A/en not_active Expired - Lifetime
- 1994-12-05 EP EP94309041A patent/EP0657209B1/en not_active Expired - Lifetime
- 1994-12-05 DE DE69410755T patent/DE69410755T2/de not_active Expired - Lifetime
- 1994-12-08 AU AU80328/94A patent/AU679583B2/en not_active Ceased
- 1994-12-08 CN CN94112919A patent/CN1060684C/zh not_active Expired - Lifetime
- 1994-12-08 CA CA002137645A patent/CA2137645C/en not_active Expired - Fee Related
- 1994-12-09 KR KR1019940033401A patent/KR100342326B1/ko not_active Expired - Lifetime
- 1994-12-09 BR BR9404922A patent/BR9404922A/pt not_active IP Right Cessation
- 1994-12-09 RU RU94043802A patent/RU2135528C1/ru not_active IP Right Cessation
- 1994-12-09 PL PL94306201A patent/PL177736B1/pl not_active IP Right Cessation
- 1994-12-12 JP JP30787694A patent/JP3668996B2/ja not_active Expired - Lifetime
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1192894A (fr) * | 1957-03-13 | 1959-10-29 | Tno | Procédé et appareil pour la préparation d'un produit pulvérulent |
| FR1367524A (fr) * | 1963-05-11 | 1964-07-24 | Appareil de réaction pour synthèses organiques | |
| EP0080147A2 (en) * | 1981-11-19 | 1983-06-01 | Kanegafuchi Kagaku Kogyo Kabushiki Kaisha | A process for producing a coagulated latex and apparatus therefor |
| EP0522776A1 (en) * | 1991-07-12 | 1993-01-13 | Dow Corning S.A. | Polymerisation reactor and polymerisation process |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2135528C1 (ru) | 1999-08-27 |
| CN1106832A (zh) | 1995-08-16 |
| ATE166798T1 (de) | 1998-06-15 |
| KR100342326B1 (ko) | 2002-12-06 |
| ES2119092T3 (es) | 1998-10-01 |
| DE69410755D1 (de) | 1998-07-09 |
| KR950018173A (ko) | 1995-07-22 |
| RU94043802A (ru) | 1996-11-20 |
| JPH07207035A (ja) | 1995-08-08 |
| CA2137645C (en) | 2006-04-25 |
| EP0657209A1 (en) | 1995-06-14 |
| CA2137645A1 (en) | 1995-06-11 |
| DE69410755T2 (de) | 1998-11-05 |
| PL177736B1 (pl) | 2000-01-31 |
| ZA948933B (en) | 1995-07-18 |
| TW323291B (enExample) | 1997-12-21 |
| IN183322B (enExample) | 1999-11-20 |
| PL306201A1 (en) | 1995-06-12 |
| EP0657209B1 (en) | 1998-06-03 |
| AU8032894A (en) | 1995-06-15 |
| JP3668996B2 (ja) | 2005-07-06 |
| AU679583B2 (en) | 1997-07-03 |
| US5492992A (en) | 1996-02-20 |
| GB9325342D0 (en) | 1994-02-16 |
| BR9404922A (pt) | 1995-08-08 |
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