CN106053175A - 一种萃取工具钢中碳化物的简易方法 - Google Patents
一种萃取工具钢中碳化物的简易方法 Download PDFInfo
- Publication number
- CN106053175A CN106053175A CN201610559044.7A CN201610559044A CN106053175A CN 106053175 A CN106053175 A CN 106053175A CN 201610559044 A CN201610559044 A CN 201610559044A CN 106053175 A CN106053175 A CN 106053175A
- Authority
- CN
- China
- Prior art keywords
- carbide
- tool steel
- easy method
- extractor tool
- sample
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 title claims abstract description 39
- 229910001315 Tool steel Inorganic materials 0.000 title claims abstract description 33
- 150000001247 metal acetylides Chemical class 0.000 title abstract 4
- 238000010438 heat treatment Methods 0.000 claims abstract description 17
- 238000001035 drying Methods 0.000 claims abstract description 16
- 238000005260 corrosion Methods 0.000 claims abstract description 14
- 230000007797 corrosion Effects 0.000 claims abstract description 14
- 239000006185 dispersion Substances 0.000 claims abstract description 10
- 238000005520 cutting process Methods 0.000 claims abstract description 6
- 238000005119 centrifugation Methods 0.000 claims abstract description 4
- 238000001914 filtration Methods 0.000 claims abstract description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 44
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 238000005498 polishing Methods 0.000 claims description 9
- 239000000725 suspension Substances 0.000 claims description 8
- 239000002244 precipitate Substances 0.000 claims description 7
- 238000013019 agitation Methods 0.000 claims description 6
- 238000013459 approach Methods 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 5
- 238000012545 processing Methods 0.000 claims description 4
- 238000003828 vacuum filtration Methods 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000003763 carbonization Methods 0.000 claims description 2
- 238000005352 clarification Methods 0.000 claims description 2
- 238000002604 ultrasonography Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 description 18
- 239000000523 sample Substances 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 14
- 239000002253 acid Substances 0.000 description 11
- 238000005868 electrolysis reaction Methods 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 5
- 239000010959 steel Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 239000003792 electrolyte Substances 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 238000012827 research and development Methods 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 229910000963 austenitic stainless steel Inorganic materials 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- 150000001722 carbon compounds Chemical class 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000010813 municipal solid waste Substances 0.000 description 2
- NICDRCVJGXLKSF-UHFFFAOYSA-N nitric acid;trihydrochloride Chemical compound Cl.Cl.Cl.O[N+]([O-])=O NICDRCVJGXLKSF-UHFFFAOYSA-N 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 239000001117 sulphuric acid Substances 0.000 description 2
- 235000011149 sulphuric acid Nutrition 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 229910001566 austenite Inorganic materials 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 229910001651 emery Inorganic materials 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052756 noble gas Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 238000010183 spectrum analysis Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F1/00—Etching metallic material by chemical means
- C23F1/10—Etching compositions
- C23F1/14—Aqueous compositions
- C23F1/16—Acidic compositions
- C23F1/28—Acidic compositions for etching iron group metals
Landscapes
- Chemical & Material Sciences (AREA)
- Immunology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Pathology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Sampling And Sample Adjustment (AREA)
- Investigating And Analyzing Materials By Characteristic Methods (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610559044.7A CN106053175B (zh) | 2016-07-15 | 2016-07-15 | 一种萃取工具钢中碳化物的简易方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610559044.7A CN106053175B (zh) | 2016-07-15 | 2016-07-15 | 一种萃取工具钢中碳化物的简易方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106053175A true CN106053175A (zh) | 2016-10-26 |
CN106053175B CN106053175B (zh) | 2019-04-26 |
Family
ID=57187608
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610559044.7A Active CN106053175B (zh) | 2016-07-15 | 2016-07-15 | 一种萃取工具钢中碳化物的简易方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106053175B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108871924A (zh) * | 2018-07-04 | 2018-11-23 | 湖南大学 | 一种从高铬铸铁中提取碳化物的方法 |
CN110618003A (zh) * | 2019-08-29 | 2019-12-27 | 江苏大学 | 一种萃取热作模具钢中碳化物的方法 |
CN114166603A (zh) * | 2021-12-08 | 2022-03-11 | 安徽工业大学 | 一种提取c-hra-5奥氏体耐热钢中微量第二相的方法 |
CN117589545A (zh) * | 2024-01-19 | 2024-02-23 | 武汉科技大学 | 一种用于透射电镜分析的纳米微粒样品的制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5814036A (ja) * | 1981-07-17 | 1983-01-26 | Kawasaki Steel Corp | ミルスケ−ル、鉄粉等中の炭化けい素分析方法 |
CN101236151A (zh) * | 2007-11-27 | 2008-08-06 | 西安交通大学 | 一种测量钢铁中碳化物相电化学行为的方法 |
CN103048180A (zh) * | 2012-12-12 | 2013-04-17 | 广东电网公司电力科学研究院 | 一种提取Super304H奥氏体不锈钢中微量碳化物的方法 |
-
2016
- 2016-07-15 CN CN201610559044.7A patent/CN106053175B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5814036A (ja) * | 1981-07-17 | 1983-01-26 | Kawasaki Steel Corp | ミルスケ−ル、鉄粉等中の炭化けい素分析方法 |
CN101236151A (zh) * | 2007-11-27 | 2008-08-06 | 西安交通大学 | 一种测量钢铁中碳化物相电化学行为的方法 |
CN103048180A (zh) * | 2012-12-12 | 2013-04-17 | 广东电网公司电力科学研究院 | 一种提取Super304H奥氏体不锈钢中微量碳化物的方法 |
Non-Patent Citations (2)
Title |
---|
曲文玉 等: "快速法测定钢中稳定夹杂物", 《河北冶金》 * |
金荣植: "《模具热处理及其常见缺陷与对策》", 31 August 2014, 机械工业出版社 * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108871924A (zh) * | 2018-07-04 | 2018-11-23 | 湖南大学 | 一种从高铬铸铁中提取碳化物的方法 |
CN110618003A (zh) * | 2019-08-29 | 2019-12-27 | 江苏大学 | 一种萃取热作模具钢中碳化物的方法 |
CN114166603A (zh) * | 2021-12-08 | 2022-03-11 | 安徽工业大学 | 一种提取c-hra-5奥氏体耐热钢中微量第二相的方法 |
CN114166603B (zh) * | 2021-12-08 | 2024-05-03 | 安徽工业大学 | 一种提取c-hra-5奥氏体耐热钢中微量第二相的方法 |
CN117589545A (zh) * | 2024-01-19 | 2024-02-23 | 武汉科技大学 | 一种用于透射电镜分析的纳米微粒样品的制备方法 |
CN117589545B (zh) * | 2024-01-19 | 2024-04-12 | 武汉科技大学 | 一种用于透射电镜分析的纳米微粒样品的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN106053175B (zh) | 2019-04-26 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN106053175A (zh) | 一种萃取工具钢中碳化物的简易方法 | |
Liu et al. | Electrochemical milling of TB6 titanium alloy in NaNO3 solution | |
CN102538703B (zh) | 一种全尺寸提取和观察钢中非金属夹杂物三维形貌的方法 | |
CN106757299A (zh) | 一种镍基合金金相组织的电解抛光腐蚀剂及其使用方法 | |
Jin et al. | Electrolytic recovery of bismuth and copper as a powder from acidic sulfate effluents using an emew® cell | |
CN102435485B (zh) | 用于扫描电镜观测钢中夹杂物的样品预处理方法 | |
CN111238916B (zh) | 一种高温合金中非金属夹杂物的分类提取与定量分析方法 | |
CN102033008B (zh) | 电解法提取s30432钢碳氮化物的方法 | |
CN107607567A (zh) | 一种镍基高温合金粉末中非金属夹杂物的定量表征方法 | |
CN102443840B (zh) | 金相组织电解液、钴的腐蚀方法及其金相组织显示方法 | |
CN106868578A (zh) | 一种用于ebsd测试的铍材电解抛光和腐蚀的一体化方法 | |
CN103884550B (zh) | 一种通过电解提取分析钢中氧化物的方法 | |
CN107328619A (zh) | 一种分离钢夹杂物中非金属夹杂物和碳化物的方法 | |
CN108845078B (zh) | 电站锅炉高温部件蠕变寿命预测方法 | |
CN108871924A (zh) | 一种从高铬铸铁中提取碳化物的方法 | |
CN111238915B (zh) | 一种高温合金中非金属夹杂物的提取方法 | |
Wang et al. | Corrosion resistance of steel materials in LiCl-KCl melts | |
CN106084188B (zh) | 一种咪唑基多孔有机离子聚合物的制备方法 | |
CN113466271B (zh) | 精确测定钢中金属间化合物类型、形貌和元素组成的方法 | |
JP3943488B2 (ja) | 鉄鋼試料中の非金属介在物の組成および/または粒径の分析法 | |
CN116818483A (zh) | 一种高碳钢中高稳定性析出相定量分析溶样方法 | |
CN110441119A (zh) | 饱和草酸溶液的应用、gh4169合金的电解腐蚀方法和微观组织观察方法 | |
Xu et al. | A novel method to prepare metal oxide electrode: Spin-coating with thermal decomposition | |
KR20110021631A (ko) | 재생 텅스텐 카바이드 | |
CN109161934A (zh) | 分离钕铁硼合金废料中稀土元素并直接制备稀土金属的方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200201 Address after: 710000 3 / F, Gaoke building, Kaiyuan Avenue, high tech Industrial Park, Yulin City, Shaanxi Province Patentee after: Shaanxi Hualing New Material Technology Co.,Ltd. Address before: 650093 No. 68, Wenchang Road, 121 Avenue, Kunming, Yunnan Patentee before: Kunming University of Science and Technology |
|
CP03 | Change of name, title or address | ||
CP03 | Change of name, title or address |
Address after: 719099 3rd Floor, High tech Building, Kaiyuan Avenue, High tech Industrial Park, Yulin City, Shaanxi Province Patentee after: Shaanxi Hualing New Materials Technology Co.,Ltd. Country or region after: China Address before: 710000 yuan, 3rd floor, Gaoke Building, Kaiyuan Avenue, High tech Industrial Park, Yulin City, Shaanxi Province Patentee before: Shaanxi Hualing New Material Technology Co.,Ltd. Country or region before: China |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240301 Address after: Room 1211, 12th Floor, Xinyuan Center Office Building, Taoyuan North Road, Lianhu District, Xi'an City, Shaanxi Province, 710077 Patentee after: Hualing (Xi'an) New Materials Co.,Ltd. Country or region after: China Address before: 719099 3rd Floor, High tech Building, Kaiyuan Avenue, High tech Industrial Park, Yulin City, Shaanxi Province Patentee before: Shaanxi Hualing New Materials Technology Co.,Ltd. Country or region before: China |