CN105985153A - Grape fertilizer mainly from wine dregs - Google Patents

Grape fertilizer mainly from wine dregs Download PDF

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Publication number
CN105985153A
CN105985153A CN201511016586.1A CN201511016586A CN105985153A CN 105985153 A CN105985153 A CN 105985153A CN 201511016586 A CN201511016586 A CN 201511016586A CN 105985153 A CN105985153 A CN 105985153A
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China
Prior art keywords
parts
gained
bone
fermentation
slaughterhouse
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CN201511016586.1A
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Chinese (zh)
Inventor
高恒东
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Wuhu Chuangyuan New Materials Co Ltd
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Wuhu Chuangyuan New Materials Co Ltd
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Priority to CN201511016586.1A priority Critical patent/CN105985153A/en
Publication of CN105985153A publication Critical patent/CN105985153A/en
Withdrawn legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D1/00Fertilisers containing potassium
    • C05D1/02Manufacture from potassium chloride or sulfate or double or mixed salts thereof
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a grape fertilizer mainly from wine dregs, made from the following materials according to parts by weight: 55-65 parts of wine dregs, 5-6 parts of hemp seed, 1.3-1.6 parts of solid polyethylene glycol, 4-5 parts of forsterite powder, 6-7 parts of salt slurry, 4-5 parts of potassium sulfate, 3.5-3.8 parts of calcium formate, 17-18 parts of nano carbon black, 35-36 parts of organic household waste, 14-15 parts of slaughterhouse pig bone waste, 20-22 parts of slaughterhouse bovine bone waste, 2.8-3.2 parts of citric acid, and suitable water; the grape fertilizer is mainly made from the main material, wine dregs, in cooperation with rich nutrients such as salt slurry and potassium sulfate, wine making wastes are recycled, waste discharge in wine making is reduced, organics content of planting soil is increased, and the concept of green and cyclic sustainable development in agricultural production is met.

Description

A kind of wine brewer's grains is the grape fertilizer of primary raw material
Technical field
The present invention relates to technical field of fertilizers, particularly relate to the grape that a kind of wine brewer's grains is primary raw material fertile Material.
Background technology
Vitis bejuco, can eat raw or raisins processed, and can make wine, and root and rattan can make medicinal, All there is cultivation all over China, be a kind of important industrial crops, the huge market demand.
Its yield and quality are played a key effect by the use of fertilizer during wine-growing, but presently commercially available Portugal But there is more defect in grape fertilizer: one is not make the concrete nutritional need and soil nutrient feature of grape For simply a large amount of nutrients such as simple offer nitrogen phosphorus;Two be many with based on chemical fertilizer, fertilizer be auxiliary, easily Produce chemical drug remain and pollute environment;Three is cannot to play improved effect to soil, will cause soil on long terms Barren, be not suitable for plantation;Four is that utilization rate of fertilizer is low, also carries in the case of cannot playing resource reutilization Carry out the excess waste of available resources.
Bone black is that animal skeleton removes the product after part or all of organic matter through charing, and wherein pig bone black is through aerobic It is mainly composed of tricalcium phosphate after burning, preferably can not only carry out the supply of phosphorus to soil, simultaneously can be with soil In the adsorption site of heavy metal competition soil surface, thus replace heavy metal-polluted soil, reduce its poison to crop Evil.Ox bone charcoal under anoxycausis not only surface contain the abundant functional group such as carboxyl and hydroxyl, and have many Permeability and very big specific surface area, have good absorption property, therefore can be fine as fertiliser granulates skeleton Offer water conservation fertilizer conservation effect.Being used in combination the two applies in the production of fertiliser granulates, is simply easily achieved, Production for grape special fertilizer material opens new way.
Content of the invention
The object of the invention is contemplated to make up the defect of prior art, provides a kind of wine brewer's grains to be primary raw material Grape fertilizer.
The present invention is achieved by the following technical solutions:
A kind of wine brewer's grains is the grape fertilizer of primary raw material, is prepared by the raw materials in: grape wine Slag 55-65, little fiber crops seed 5-6, solid fraction polyethylene glycol 1.3-1.6, forsterite powder 4-5, salt slurry 6-7, sulphur Acid potassium 4-5, calcium formate 3.5-3.8, nano carbon black 17-18, domestic organic garbage 35-36, slaughterhouse are discarded It is appropriate that ox bone 20-22, citric acid 2.8-3.2, water are discarded in pig bone 14-15, slaughterhouse.
Described wine brewer's grains is specifically comprising the following steps that of the grape method for preparing fertilizer of primary raw material
(1) nano carbon black is joined in the salpeter solution of 65% of 8-10 times of quality, and be heated to 105-115 DEG C, oxidation reaction stops heating after 2 hours, and rinses until PH is 5.8-6.2 with water, then will Gained carbon black is dried at 100-110 DEG C, obtains modified Nano carbon black standby;
(2) by step 1 gained modified Nano carbon black and domestic organic garbage, wine brewer's grains, little fiber crops seed, salt Mud mixes and carries out compost fermentation, ferments first 2 weeks and takes anaerobic fermentation, and keeps the fermentation heap water content to be 40-50%, abundant afterwards turning is simultaneously passed through oxygen, keeps fermentation heap water content to be the 70% of maximum water-holding capacity, send out Ferment 3-4 week, by gained fermentation material through squeeze ferment slag and ferment liquid standby;
(3) slaughterhouse is discarded pig bone clean be placed in high temperature furnace, be constantly passed through at 1150-1250 DEG C Air calcination 120-150 minute, obtains pig bone black, then slaughterhouse is discarded ox bone cleans and be placed in high temperature furnace, Calcine 3-4 hour under 780-820 DEG C and airtight condition, obtain ox bone charcoal, for later use;
(4) step 2 gained ferment liquid and citric acid, potassium sulfate, calcium formate are mixed and heated to 65-68 DEG C, Insulation 30-40 minute, is down to room temperature afterwards and must ferment chelating liquid, then by step 2 gained ferment slag, step 3 The mixing of gained ox bone charcoal is placed in mixer, uniformly sprays fermentation chelating liquid into mixer in whipping process In, the wet stock that must mix is standby;
(5) by step 4 gained wet stock after centrifugal dehydration with step 3 gained pig bone black, the poly-second of solid fraction two Alcohol, forsterite powder and remaining leftover materials mixing granulation, obtain fertilizer of the present invention.
The invention have the advantage that
Organic waste is passivated repairing by fertilizer utilization modified Nano carbon black of the present invention, in retaining organic waste Reduce heavy metals from waste compost non-residual form total amount in the case of the elements such as N, P, K, improve compost security, Further through the applicability adding raising fertilizer of pig, ox mixing bone black, with wine brewer's grains as primary raw material, coordinate The abundant nutrition composition such as salt slurry, potassium sulfate, it is achieved that the recycling of grape wine brewing discarded object, decreases and made wine Waste discharge in journey, improves the organic content of planting soil, meets continuing of agricultural production Green circulation Idea of development.
Detailed description of the invention
A kind of wine brewer's grains is the grape fertilizer of primary raw material, is made up of the raw material of following weight portion (kg): Wine brewer's grains the 55th, little fiber crops seed the 5th, solid fraction polyethylene glycol the 1.3rd, forsterite powder the 4th, salt slurry the 6th, potassium sulfate is the 4th, Calcium formate the 3.5th, nano carbon black the 17th, domestic organic garbage the 35th, slaughterhouse is discarded pig bone the 14th, slaughterhouse and is discarded Ox bone the 20th, citric acid the 2.8th, water is appropriate.
Described wine brewer's grains is specifically comprising the following steps that of the grape method for preparing fertilizer of primary raw material
(1) nano carbon black is joined in the salpeter solution of 65% of 8 times of quality, and be heated to 105 DEG C, oxygen Stop heating after changing reaction 2 hours, and rinse until PH is 5.8 with water, then by gained carbon black at 100 DEG C Dry, obtain modified Nano carbon black standby;
(2) by step 1 gained modified Nano carbon black and domestic organic garbage, wine brewer's grains, little fiber crops seed, salt Mud mixes and carries out compost fermentation, ferments first 2 weeks and takes anaerobic fermentation, and keeps fermentation heap water content to be 40%, Abundant afterwards turning is simultaneously passed through oxygen, keeps fermentation heap water content to be the 70% of maximum water-holding capacity, ferments 3 weeks, By gained fermentation material through squeeze ferment slag and ferment liquid standby;
(3) slaughterhouse is discarded pig bone clean be placed in high temperature furnace, at 1150 DEG C, be constantly passed through air forge Burn 120 minutes, obtain pig bone black, then slaughterhouse is discarded ox bone clean and be placed in high temperature furnace, at 780 DEG C and Calcine 3 hours under airtight condition, obtain ox bone charcoal, for later use;
(4) step 2 gained ferment liquid and citric acid, potassium sulfate, calcium formate are mixed and heated to 65 DEG C, protect Temperature 30 minutes, is down to room temperature afterwards and must ferment chelating liquid, then by step 2 gained ferment slag, step 3 gained ox Bone black mixing is placed in mixer, uniformly sprays fermentation chelating liquid in mixer, obtain mixed in whipping process Close uniform wet stock standby;
(5) by step 4 gained wet stock after centrifugal dehydration with step 3 gained pig bone black, the poly-second of solid fraction two Alcohol, forsterite powder and remaining leftover materials mixing granulation, obtain fertilizer of the present invention.
In order to further illustrate the using value of the present invention, inventor is chosen experimental plot and is tested by the plantation of grape Demonstrate,proving the concrete effect of fertilizer of the present invention, wherein 5 mu of ground use fertilizer of the present invention as experimental group, and another 5 mu of ground make With common commercially available fertilizer as a control group, during plantation, field control measures are identical, and experimental data is as follows:
As can be seen from the above data, after employing this fertilizer, yield and quality is all improved, and has high reality Use value, is suitable for promoting the use of of large-scale planting.

Claims (2)

1. a wine brewer's grains is the grape fertilizer of primary raw material, it is characterized in that, be prepared by the raw materials in: wine brewer's grains 55-65, little fiber crops seed 5-6, solid fraction polyethylene glycol 1.3-1.6, forsterite powder 4-5, salt slurry 6-7, potassium sulfate 4-5, calcium formate 3.5-3.8, nano carbon black 17-18, domestic organic garbage 35-36, pig bone 14-15 is discarded in slaughterhouse, ox bone 20-22 is discarded in slaughterhouse, citric acid 2.8-3.2, water are appropriate.
2. wine brewer's grains according to claim 1 is the grape fertilizer of primary raw material, it is characterised in that specifically comprising the following steps that of preparation method
(1) nano carbon black is joined in the salpeter solution of 65% of 8-10 times of quality, and it is heated to 105-115 DEG C, oxidation reaction stops heating after 2 hours, and rinses until PH is 5.8-6.2 with water, again gained carbon black is dried at 100-110 DEG C, obtain modified Nano carbon black standby;
(2) step 1 gained modified Nano carbon black is mixed with domestic organic garbage, wine brewer's grains, little fiber crops seed, salt slurry and carries out compost fermentation, ferment first 2 weeks and take anaerobic fermentation, and keep fermentation heap water content to be 40-50%, abundant afterwards turning is simultaneously passed through oxygen, fermentation heap water content is kept to be the 70% of maximum water-holding capacity, fermentation 3-4 week, by gained fermentation material through squeeze ferment slag and ferment liquid standby;
(3) slaughterhouse is discarded pig bone clean be placed in high temperature furnace, it is constantly passed through air calcination 120-150 minute at 1150-1250 DEG C, obtain pig bone black, again slaughterhouse is discarded ox bone clean be placed in high temperature furnace, 3-4 hour is calcined under 780-820 DEG C and airtight condition, obtain ox bone charcoal, for later use;
(4) step 2 gained ferment liquid and citric acid, potassium sulfate, calcium formate are mixed and heated to 65-68 DEG C, insulation 30-40 minute, it is down to room temperature afterwards must ferment chelating liquid, it is placed in step 2 gained ferment slag, the mixing of step 3 gained ox bone charcoal in mixer again, uniformly spraying fermentation chelating liquid in mixer in whipping process, the wet stock that must mix is standby;
(5) by step 4 gained wet stock after centrifugal dehydration with step 3 gained pig bone black, solid fraction polyethylene glycol, forsterite powder and remaining leftover materials mixing granulation, obtain fertilizer of the present invention.
CN201511016586.1A 2015-12-29 2015-12-29 Grape fertilizer mainly from wine dregs Withdrawn CN105985153A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201511016586.1A CN105985153A (en) 2015-12-29 2015-12-29 Grape fertilizer mainly from wine dregs

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106673897A (en) * 2016-12-12 2017-05-17 新昌县奥而特农业科技有限公司 Fertilizer for grapes as well as preparation method and application thereof
CN107266162A (en) * 2017-05-31 2017-10-20 新昌县瑞天食品科技有限公司 The preparation method of grape fertilizer
CN107337505A (en) * 2017-06-14 2017-11-10 芜湖县花桥镇恒乐水果种植专业合作社 A kind of plum plantation high nitrogen fertilizer material
CN109020718A (en) * 2018-09-30 2018-12-18 芜湖县花桥镇恒乐水果种植专业合作社 A kind of grape compound fertilizer preparation method adjusting soil texture
CN109824401A (en) * 2019-01-02 2019-05-31 赤水市幸福源生物科技股份有限公司 A kind of fruit fertilizer special for organic and preparation method thereof
CN110526750A (en) * 2019-09-27 2019-12-03 泸州品创科技有限公司 Utilize the method for fresh wine brewing useless grain production organic fertilizer

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103172439A (en) * 2013-03-02 2013-06-26 安徽程翔肥料有限公司 Special organic-inorganic compound biological medicine fertilizer for sweet potatoes, and preparation method thereof
CN103819288A (en) * 2013-12-09 2014-05-28 芜湖美农农业科技有限公司 Novel grape formula fertilizer and preparation method thereof
CN103819275A (en) * 2014-03-11 2014-05-28 天津师范大学 Method for controlling different forms of heavy metal in urban life compost by modified nano carbon
CN104311204A (en) * 2014-09-25 2015-01-28 安徽圣堡利诺葡萄酒庄园有限公司 Composite fertilizer prepared from waste residue generated during wine production
CN104609946A (en) * 2014-12-30 2015-05-13 杭州师范大学 Composite controlled retarder for soil heavy metal pollution of vegetable field and application thereof
CN105016883A (en) * 2015-07-23 2015-11-04 合肥众月健康科技有限公司 Liquid fertilizer for adjusting soil pH value and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103172439A (en) * 2013-03-02 2013-06-26 安徽程翔肥料有限公司 Special organic-inorganic compound biological medicine fertilizer for sweet potatoes, and preparation method thereof
CN103819288A (en) * 2013-12-09 2014-05-28 芜湖美农农业科技有限公司 Novel grape formula fertilizer and preparation method thereof
CN103819275A (en) * 2014-03-11 2014-05-28 天津师范大学 Method for controlling different forms of heavy metal in urban life compost by modified nano carbon
CN104311204A (en) * 2014-09-25 2015-01-28 安徽圣堡利诺葡萄酒庄园有限公司 Composite fertilizer prepared from waste residue generated during wine production
CN104609946A (en) * 2014-12-30 2015-05-13 杭州师范大学 Composite controlled retarder for soil heavy metal pollution of vegetable field and application thereof
CN105016883A (en) * 2015-07-23 2015-11-04 合肥众月健康科技有限公司 Liquid fertilizer for adjusting soil pH value and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106673897A (en) * 2016-12-12 2017-05-17 新昌县奥而特农业科技有限公司 Fertilizer for grapes as well as preparation method and application thereof
CN107266162A (en) * 2017-05-31 2017-10-20 新昌县瑞天食品科技有限公司 The preparation method of grape fertilizer
CN107337505A (en) * 2017-06-14 2017-11-10 芜湖县花桥镇恒乐水果种植专业合作社 A kind of plum plantation high nitrogen fertilizer material
CN109020718A (en) * 2018-09-30 2018-12-18 芜湖县花桥镇恒乐水果种植专业合作社 A kind of grape compound fertilizer preparation method adjusting soil texture
CN109824401A (en) * 2019-01-02 2019-05-31 赤水市幸福源生物科技股份有限公司 A kind of fruit fertilizer special for organic and preparation method thereof
CN110526750A (en) * 2019-09-27 2019-12-03 泸州品创科技有限公司 Utilize the method for fresh wine brewing useless grain production organic fertilizer

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Application publication date: 20161005