CN105982369B - A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil - Google Patents
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil Download PDFInfo
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- CN105982369B CN105982369B CN201610415612.6A CN201610415612A CN105982369B CN 105982369 B CN105982369 B CN 105982369B CN 201610415612 A CN201610415612 A CN 201610415612A CN 105982369 B CN105982369 B CN 105982369B
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- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B11/00—Hosiery; Panti-hose
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B17/00—Selection of special materials for underwear
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
- C11B1/106—Production of fats or fatty oils from raw materials by extracting using ultra-sounds
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04B—KNITTING
- D04B1/00—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B1/22—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration
- D04B1/24—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration wearing apparel
- D04B1/26—Weft knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes specially adapted for knitting goods of particular configuration wearing apparel stockings
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/20—Air permeability; Ventilation
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41B—SHIRTS; UNDERWEAR; BABY LINEN; HANDKERCHIEFS
- A41B2400/00—Functions or special features of shirts, underwear, baby linen or handkerchiefs not provided for in other groups of this subclass
- A41B2400/36—Deodorising or perfuming
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Socks And Pantyhose (AREA)
Abstract
The present invention relates to socks production field, a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil is disclosed, is comprised the following steps：（1）Get the raw materials ready：Cotton or cotton are formed into spun yarn with terylene mixing twisting；Terylene, polyamide fibre, spandex are twisted to form filament yarn respectively.（2）Knit socks：Spun yarn, filament yarn feeding footwear machine are woven, base socks are made.（3）Arrange：Base socks are impregnated into water, while adding plants essential oil antimosquito finishing agent, the 25min of washing process 3 into water；The plants essential oil antimosquito finishing agent includes：The 82wt% of plants essential oil 3, the 97wt% of water 18.（4）Sizing：By base ankle socks on socks plate, steam heating, pressurization, drying, obtain finished product quilted stockings at 101 185 DEG C.The mosquito-proof quilted stockings prepared using the present invention, being thrown away after repeatedly wearing, washing can keep effectively mosquito-proof, while having the gas permeability and soft comfortable of quilted stockings.
Description
Technical field
The present invention relates to the preparation method in socks production field, more particularly to a kind of mosquito-proof quilted stockings of plants essential oil.
Background technology
Summer is mosquito most season, and can use the methods such as mosquito-repellent incense, pesticide spray when usual people's household, travelling goes out
Mosquito, but this mode exist safety and sanitation, smell excessively be pungent and a period of time after its effect faded away with air flow
The problems such as.With the development of textile technology, fabric, the dress ornament of some mosquito proofs obtain exploitation and application.
China Patent Publication No. CN 203234042U are related to a kind of mosquito-proof socks, including socks body, and socks body includes stocking blank and socks
Pin, stocking foot includes being lined with one layer of rubber membrane on socks face and the stocking sole, described socks body, and rubber membrane and socks body connect on stocking blank
Connect, it is described be located at the stocking sole obtain rubber membrane provided with air-vent, with while comfortableness that socks are worn is not influenceed,
The advantage of the ventilative radiating of bite by mosquitos and appropriateness can effectively be prevented.But the technical scheme is by setting rubber membrane and air-vent
It is less than normal, there is the easy aging of rubber membrane, socks production environment-protective process difficulty and wear comfortableness problem.
China Patent Publication No. CN 205161905U be related to it is a kind of there are the mosquito-proof socks of antibacterial, including mosquito-proof layer, antibiotic layer,
Socks face, stocking blank, the stocking sole, socks face bottom are connected with above the stocking sole, the socks face and are connected with the stocking blank, the stocking sole
Lower section is bonded with slipmat, and the stocking sole is dispersed with outside base cloth layer, the mosquito-proof layer, the antibiotic layer, deodorization from outside to inside
Layer, internal precoat, the socks face are dispersed with the outside base cloth layer, the mosquito-proof layer, the internal precoat from outside to inside.
The utility model has the functions such as effective mosquito-proof, antibacterial, deodorization, protects the health of user foot, and the stocking sole has been bonded anti-
Skidding has anti-skidding effect, effective protection socks skidding, it is to avoid user is injured.But, the technical scheme passes through folded
Plus, compound mode stocking foot is thickened, unfavorable ventilation and perspiration function.
The content of the invention
In order to solve, the mosquito-proof persistence effect of quilted stockings is poor, mosquito-proof quilted stockings wears comfortableness and poor air permeability, stimulate skin
Problem, the present invention proposes a kind of its preparation method of the mosquito-proof quilted stockings of plants essential oil, the mosquito-proof quilted stockings prepared using the present invention, warp
Repeatedly (10-20 times) wear, wash after throw away can keep effectively it is mosquito-proof, while having the gas permeability and soft comfortable of quilted stockings
Property.
The present invention concrete technical scheme be：A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton or cotton are formed into spun yarn with terylene mixing twisting；Terylene, polyamide fibre, spandex are twisted into shape respectively
Into filament yarn；The line density of spun yarn and filament yarn is 145dtex-330dtex, and the spun yarn twist is 301-1069 twists/m, long
The gauze twist is below 150 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, filament yarn is carried out spun yarn, filament yarn feeding footwear machine as inner yarn
Braiding, is made base socks.
The present invention is using spun yarn as table yarn, and filament yarn is as inner yarn, and advantage is that the main component of inner yarn is terylene, ammonia
Synthetic fibre, polyamide fibre, its hygroscopicity are poor, and regain is low, and the main component of table yarn is cotton, good hygroscopicity, therefore moisture is mainly by table
The cotton of yarn absorbs, after table yarn and air contact, and moisture easily scatters and disappears, volatilized.So as to which the gas permeability and dress that improve socks are relaxed
Adaptive.
(3) arrange：In the water that base socks are impregnated into its 4-8 times of quality, while adding base socks and water gross mass into water
1.5-15.9% plants essential oil antimosquito finishing agent, is heated up with 5-30 DEG C/min speed, and final temperature is controlled in 61-98
DEG C, washing process 3-25min；The plants essential oil antimosquito finishing agent includes：Plants essential oil 3-82wt%, water 18-97wt%.
Base socks progress dipping is just arranged, because the hygroscopicity of cotton is preferable, therefore also there is appearance using cotton as table yarn raw material
The plants essential oil in finishing agent is easily absorbed, so that plants essential oil largely can be supported on fabric.
(4) shape：The base ankle socks completed steam on respective model socks plate and at 101-185 DEG C will be arranged to heat, add
Pressure, drying, processing time 15-180 second, obtain finished product quilted stockings；Wherein Stress control is in 0.8-2.2kg.
Preferably, in step (2), stocking blank is using 1 every 1 rib construction, and ammonification synthetic fibre filament yarn is padded；Socks body, socks
With, the stocking sole, toe plain weave, figured texture weave；Stocking blank is long using 21S/1 cotton staple yarn+70D chinlon filament yarn double-contracting 180D spandexs
Gauze；Socks body, the stocking sole, heel, toe use 21S/1 cotton staple yarn+70D chinlon filament yarn looping 30D spandex filament yarns.
Using the base socks of said structure, be conducive to the absorption of finishing agent, and finishing agent can be made to keep permanent.Using washing
Synthetic fibre, polyamide fibre or cotton coat to spandex, spandex wearability can be overcome poor and shortcoming.
Preferably, during socks are knitted, from 108 pins, 144 pins, 168 pins footwear machine, the program finished is imported
Footwear machine, footwear machine is woven according to programmed instruction.
Preferably, cotton content is 60-70wt% in the base socks, terylene content is 10-20wt%, and polyamide fibre content is
10-20wt%, spandex content is 1-10wt%.
Preferably, the plants essential oil includes：Wormwood extract 3-97wt%, peppermint extract 3-97wt%.
Preferably, the extracting method of the wormwood extract is：Wormwood is mixed with the water of its 10-20 times of quality and ground
Mill, obtains wormwood slurries, and wormwood slurries are added into concentration to carry out ultrasonic extraction in 70-80wt% ethanol solutions, wherein
The volume ratio of wormwood slurries and ethanol solution is 1:2-3,55-65 DEG C of extraction temperature, ultrasonic frequency 40-50KHz, ultrasonic wave work(
Rate 400-500W, extraction time 1-2h；Wormwood extract is filtrated to get after extraction.
Preferably, the extracting method of the peppermint extract is：Dried peppermint leaf is mixed with the water of its 8-12 times of quality and ground
Mill, obtains peppermint slurries, and peppermint slurries are added into concentration to carry out ultrasonic extraction in 70-80wt% ethanol solutions, wherein
The volume ratio of peppermint slurries and ethanol solution is 1:3-5,70-80 DEG C of extraction temperature, ultrasonic frequency 40-50KHz, ultrasonic wave work(
Rate 400-500W, extraction time 0.5-1.5h；Peppermint extract is filtrated to get after extraction.
Preferably, base socks pass through spraying treatment before step (3)：With spray liquid base socks are carried out with spraying treatment, is sprayed
By base socks, 1-3h is placed in tiling in the environment that temperature is 40-50 DEG C, humidity is 80-90% afterwards, then to base socks spray concentration
For 3-5wt% Sodium Borohydride ethanol solution, base socks are continued into tiling at room temperature and placed after 10-20h, base socks are cleaned and dried
It is dry；Wherein the consumption of spray liquid is 1-2mL/cm3, Sodium Borohydride ethanol solution consumption be 0.1-0.3mL/cm3。
Preferably, the preparation method of the spray liquid is as follows：Beta-schardinger dextrin, o- iodoxy phenylpropenoic acid potassium, dimethyl is sub-
Sulfone 3-5 in mass ratio:1-3:100 mixing, stirring reaction 4-8h, is filtrated to get filtered fluid at 45-55 DEG C, with acetone to filtering
Liquid dilutes 20-30 times, and secondary filter after stirring takes solid and is dissolved in the water of 30-50 times of quality, and three filterings are simultaneously dried
Modified beta-schardinger dextrin is made afterwards；Will modified beta-schardinger dextrin, algal polysaccharides, glutaraldehyde, ethylene glycol diglycidylether, citric acid and
Water 1-3 in mass ratio:0.1-0.5:0.04-0.06:0.1-0.2:30-40:100 mixing, are made spray liquid after stirring.
In spray process, modified beta-schardinger dextrin, algal polysaccharides can be passed through glutaraldehyde, ethylene glycol diglycidylether
And other chemical reactions are grafted to fiber surface, because modified beta-schardinger dextrin, algal polysaccharides have preferably to plants essential oil
Embedding effect, therefore, it is possible to improve the load capacity and load fastness of plants essential oil, plants essential oil is stored in modified beta-schardinger dextrin
In the cavity in portion, due to permeable pressure head inside and outside cavity so that plants essential oil has slow-release function, plants essential oil is improved on fabric
Retention time, be difficult to wash away.On the other hand, while the also tensile strength of fiber, and make fiber that there is preferable compliance.
It is compared with the prior art, the beneficial effects of the invention are as follows：
(1) there is certain fragrance, after wearing, washing repeatedly, remain to keep preferably mosquito-proof effect；
(2) preparation method environmental protection, stably, maintains and the original gas permeability of quilted stockings and wears comfortableness.
Embodiment
With reference to embodiment, the invention will be further described.
Embodiment 1
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Terylene, polyamide fibre, spandex are twisted to form filament yarn respectively；Spun yarn
Line density with filament yarn is 238dtex, and the spun yarn twist is 685 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, filament yarn is as inner yarn, from the footwear machine of 144 pins, by the journey finished
Sequence imports footwear machine, spun yarn, filament yarn is sent into footwear machine, footwear machine is woven according to programmed instruction, and base socks are made.Institute
It is 65wt% to state cotton content in base socks, and terylene content is 15wt%, and polyamide fibre content is 15wt%, and spandex content is 5wt%.
Wherein, stocking blank is using 1 every 1 rib construction, and ammonification synthetic fibre filament yarn is padded；Socks body, heel, the stocking sole, toe are used flat
Line, figured texture weave；Stocking blank uses 21S/1 cotton staple yarn+70D chinlon filament yarn double-contracting 180D spandex filament yarns；Socks body, the stocking sole,
Heel, toe use 21S/1 cotton staple yarn+70D chinlon filament yarn looping 30D spandex filament yarns.
(3) arrange：In the water that base socks are impregnated into its 6 times of quality, while adding base socks and water gross mass 8.7% into water
Plants essential oil antimosquito finishing agent, heated up with 18 DEG C/min speed, final temperature control in 80 DEG C, washing process
14min；The plants essential oil antimosquito finishing agent includes：Plants essential oil 42.5wt%, water 57.5wt%.The plants essential oil bag
Include：Wormwood extract 50wt%, peppermint extract 50wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 15 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 75wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:2.5,60 DEG C of extraction temperature, ultrasonic frequency 45KHz, ultrasonic power 450W, extraction time 1.5h；Extraction
Wormwood extract is filtrated to get after taking.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 10 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 75wt% ethanol solutions
The volume ratio of solution is 1:4,75 DEG C of extraction temperature, ultrasonic frequency 45KHz, ultrasonic power 450W, extraction time 1h；Extraction
After be filtrated to get peppermint extract.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 143 DEG C will be arranged
It is dry, 98 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.5kg.
Embodiment 2
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is formed into spun yarn with terylene mixing twisting；Terylene, polyamide fibre, spandex are twisted to form long filament respectively
Yarn；The line density of spun yarn and filament yarn is 145dtex, and the spun yarn twist is 301 twists/m, and long filament twist per unit is at 50 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, filament yarn is as inner yarn, from the footwear machine of 108 pins, by the journey finished
Sequence imports footwear machine, spun yarn, filament yarn is sent into footwear machine, footwear machine is woven according to programmed instruction, and base socks are made.Institute
It is 60wt% to state cotton content in base socks, and terylene content is 20wt%, and polyamide fibre content is 19wt%, and spandex content is 1wt%.
Wherein, stocking blank is using 1 every 1 rib construction, and ammonification synthetic fibre filament yarn is padded；Socks body, heel, the stocking sole, toe are used flat
Line, figured texture weave；Stocking blank uses 21S/1 cotton staple yarn+70D chinlon filament yarn double-contracting 180D spandex filament yarns；Socks body, the stocking sole,
Heel, toe use 21S/1 cotton staple yarn+70D chinlon filament yarn looping 30D spandex filament yarns.
(3) arrange：In the water that base socks are impregnated into its 4 times of quality, while adding base socks and water gross mass 1.5% into water
Plants essential oil antimosquito finishing agent, heated up with 5 DEG C/min speed, final temperature control in 61 DEG C, washing process
25min；The plants essential oil antimosquito finishing agent includes：Plants essential oil 3wt%, water 97wt%.The plants essential oil includes：Wormwood
Extract 3wt%, peppermint extract 97wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 10 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:2,55 DEG C of extraction temperature, ultrasonic frequency 40KHz, ultrasonic power 400W, extraction time 2h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 8 times of quality, peppermint slurry is obtained
Peppermint slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein peppermint slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,70 DEG C of extraction temperature, ultrasonic frequency 40KHz, ultrasonic power 400W, extraction time 1.5h；Extraction
After be filtrated to get peppermint extract.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 101 DEG C will be arranged
It is dry, 180 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 0.8kg.
Embodiment 3
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Terylene, polyamide fibre, spandex are twisted to form filament yarn respectively；Spun yarn
Be 330dtex with the line density of filament yarn, the spun yarn twist is 1069 twists/m, 145 twists/m of long filament twist per unit with.
(2) socks are knitted：Using spun yarn as table yarn, filament yarn is as inner yarn, from the footwear machine of 168 pins, by the journey finished
Sequence imports footwear machine, spun yarn, filament yarn is sent into footwear machine, footwear machine is woven according to programmed instruction, and base socks are made.Institute
It is 70wt% to state cotton content in base socks, and terylene content is 10wt%, and polyamide fibre content is 10wt%, and spandex content is 10wt%.
Wherein, stocking blank is using 1 every 1 rib construction, and ammonification synthetic fibre filament yarn is padded；Socks body, heel, the stocking sole, toe are used flat
Line, figured texture weave；Stocking blank uses 21S/1 cotton staple yarn+70D chinlon filament yarn double-contracting 180D spandex filament yarns；Socks body, the stocking sole,
Heel, toe use 21S/1 cotton staple yarn+70D chinlon filament yarn looping 30D spandex filament yarns.
(3) arrange：In the water that base socks are impregnated into its 8 times of quality, while adding base socks and water gross mass into water
15.9% plants essential oil antimosquito finishing agent, is heated up with 30 DEG C/min speed, and final temperature is controlled at 98 DEG C, at washing
Manage 3min；The plants essential oil antimosquito finishing agent includes：Plants essential oil 82wt%, water 18wt%.The plants essential oil includes：Chinese mugwort
Careless extract 97wt%, peppermint extract 3wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 20 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 80wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,65 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 1h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 12 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 80wt% ethanol solutions
The volume ratio of solution is 1:5,80 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 0.5h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 185 DEG C will be arranged
It is dry, 15 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 2.2kg.
Embodiment 4
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Terylene, polyamide fibre, spandex are twisted to form filament yarn respectively；Spun yarn
182dtex, the line density of filament yarn is 33.3dtex, and the spun yarn twist is 500 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, filament yarn is as inner yarn, from the footwear machine of 108 pins, by the journey finished
Sequence imports footwear machine, spun yarn, filament yarn is sent into footwear machine, footwear machine is woven according to programmed instruction, and base socks are made.Institute
It is 65wt% to state cotton content in base socks, and terylene content is 12wt%, and polyamide fibre content is 20wt%, and spandex content is 3wt%.
(3) arrange：In the water that base socks are impregnated into its 4-8 times of quality, while adding base socks and water gross mass 5% into water
Plants essential oil antimosquito finishing agent, heated up with 5 DEG C/min speed, final temperature control in 90 DEG C, washing process 8min；
The plants essential oil antimosquito finishing agent includes：Plants essential oil 5wt%, water 95wt%.The plants essential oil includes：Wormwood extract
30wt%, peppermint extract 70wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 12 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 75wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:2,60 DEG C of extraction temperature, ultrasonic frequency 45KHz, ultrasonic power 500W, extraction time 1.5h；Extraction
After be filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 11 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 75wt% ethanol solutions
The volume ratio of solution is 1:3.5,75 DEG C of extraction temperature, ultrasonic frequency 45KHz, ultrasonic power 500W, extraction time 1h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 125 DEG C will be arranged
It is dry, 70 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.6kg.
Embodiment 5
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Terylene, spandex are twisted to form filament yarn；The line density of spun yarn is
182dtex, the spun yarn twist is 800 twists/m, and long filament twist per unit is below 150 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, 33.3dtex polyester filament yarn coats 77.8dtex spandex filament yarn
As inner yarn, from the footwear machine of 168 pins, the program finished is imported into footwear machine, spun yarn, filament yarn are sent into footwear machine,
Footwear machine is woven according to programmed instruction, and base socks are made.Cotton content is 70wt% in the base socks, and terylene content is
20wt%, spandex content is 10wt%.
(3) arrange：In the water that base socks are impregnated into its 5 times of quality, while adding base socks and water gross mass 6% into water
Plants essential oil antimosquito finishing agent, is heated up with 5 DEG C/min speed, and final temperature is controlled in 85 DEG C, washing process 5min；Institute
Stating plants essential oil antimosquito finishing agent includes：Plants essential oil 35wt%, water 65wt%.The plants essential oil includes：Wormwood extract
60wt%, peppermint extract 40wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 16 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 80wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:2,55 DEG C of extraction temperature, ultrasonic frequency 40KHz, ultrasonic power 400W, extraction time 1h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 9 times of quality, peppermint slurry is obtained
Peppermint slurries are added to concentration to carry out ultrasonic extraction in 80wt% ethanol solutions, wherein peppermint slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,70 DEG C of extraction temperature, ultrasonic frequency 40KHz, ultrasonic power 400W, extraction time 0.5h；Extraction
After be filtrated to get peppermint extract.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 120 DEG C will be arranged
It is dry, 45 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.2kg.
Embodiment 6
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Polyamide fibre, spandex are twisted to form filament yarn respectively；The line of spun yarn is close
Spend for 182dtex, the spun yarn twist is 301 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, the cladding 77.8dtex spandex filament yarn conducts of 33.3dtex polyester filaments yarn
In yarn, from the footwear machine of 168 pins, the program finished is imported into footwear machine, spun yarn, filament yarn are sent into footwear machine, socks are knitted
Machine is woven according to programmed instruction, and base socks are made.Cotton content is 70wt% in the base socks, and polyamide fibre content is 20wt%, ammonia
Synthetic fibre content is 10wt%.
(3) arrange：In the water that base socks are impregnated into its 7 times of quality, while adding base socks and water gross mass 6% into water
Plants essential oil antimosquito finishing agent, is heated up with 10 DEG C/min speed, and final temperature is controlled in 88 DEG C, washing process 4min；
The plants essential oil antimosquito finishing agent includes：Plants essential oil 50wt%, water 50wt%.The plants essential oil includes：Wormwood extracts
Liquid 10wt%, peppermint extract 90wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 12 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,65 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 2h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 11 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 70wt% ethanol solutions
The volume ratio of solution is 1:5,80 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 1.5h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 130 DEG C will be arranged
It is dry, 40 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.6kg.
Embodiment 7
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Polyamide fibre, spandex are twisted to form filament yarn respectively；The line of spun yarn is close
Spend for 182dtex, the spun yarn twist is 301 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, the cladding 77.8dtex spandex filament yarn conducts of 33.3dtex polyester filaments yarn
In yarn, from the footwear machine of 168 pins, the program finished is imported into footwear machine, spun yarn, filament yarn are sent into footwear machine, socks are knitted
Machine is woven according to programmed instruction, and base socks are made.Cotton content is 70wt% in the base socks, and polyamide fibre content is 20wt%, ammonia
Synthetic fibre content is 10wt%.
(3) arrange：Spraying treatment is carried out to base socks with spray liquid, after spraying by base socks temperature be 45 DEG C, humidity be
2h is placed in tiling in 85% environment, and then to the Sodium Borohydride ethanol solution that base socks spray concentration is 4wt%, base socks are existed
Continue to tile at room temperature to place after 15h, base socks are cleaned into drying；Wherein the consumption of spray liquid is 1.5mL/cm3, Sodium Borohydride
The consumption of ethanol solution is 0.2mL/cm3。
The preparation method of the spray liquid is as follows：Beta-schardinger dextrin, o- iodoxy phenylpropenoic acid potassium, dimethyl sulfoxide (DMSO) are pressed into quality
Than 4:2:100 mixing, stirring reaction 6h, is filtrated to get filtered fluid at 50 DEG C, and 25 times, after stirring are diluted to filtered fluid with acetone
Secondary filter, takes solid and is dissolved in the water of 40 times of quality, filters and be made after drying modified beta-schardinger dextrin three times；It will change
Property beta-schardinger dextrin, algal polysaccharides, glutaraldehyde, ethylene glycol diglycidylether, citric acid and water in mass ratio 2:0.3:0.05:
0.15:35:100 mixing, are made spray liquid after stirring.
In the water that base socks are impregnated into its 7 times of quality, while adding base socks and the plants essential oil of water gross mass 6% into water
Antimosquito finishing agent, is heated up with 10 DEG C/min speed, and final temperature is controlled in 88 DEG C, washing process 4min；The plant
Essential oil antimosquito finishing agent includes：Plants essential oil 50wt%, water 50wt%.The plants essential oil includes：Wormwood extract 10wt%,
Peppermint extract 90wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 12 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,65 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 2h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 11 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 70wt% ethanol solutions
The volume ratio of solution is 1:5,80 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 1.5h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 130 DEG C will be arranged
It is dry, 40 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.6kg.
Embodiment 8
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Polyamide fibre, spandex are twisted to form filament yarn respectively；The line of spun yarn is close
Spend for 182dtex, the spun yarn twist is 301 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, the cladding 77.8dtex spandex filament yarn conducts of 33.3dtex polyester filaments yarn
In yarn, from the footwear machine of 168 pins, the program finished is imported into footwear machine, spun yarn, filament yarn are sent into footwear machine, socks are knitted
Machine is woven according to programmed instruction, and base socks are made.Cotton content is 70wt% in the base socks, and polyamide fibre content is 20wt%, ammonia
Synthetic fibre content is 10wt%.
(3) arrange：Spraying treatment is carried out to base socks with spray liquid, after spraying by base socks temperature be 40 DEG C, humidity be
3h is placed in tiling in 80% environment, and then to the Sodium Borohydride ethanol solution that base socks spray concentration is 3wt%, base socks are existed
Continue to tile at room temperature to place after 10h, base socks are cleaned into drying；Wherein the consumption of spray liquid is 1mL/cm3, Sodium Borohydride second
The consumption of alcoholic solution is 0.1mL/cm3。
The preparation method of the spray liquid is as follows：Beta-schardinger dextrin, o- iodoxy phenylpropenoic acid potassium, dimethyl sulfoxide (DMSO) are pressed into quality
Than 3:1:100 mixing, stirring reaction 8h, is filtrated to get filtered fluid at 45 DEG C, and 20 times, after stirring are diluted to filtered fluid with acetone
Secondary filter, takes solid and is dissolved in the water of 30 times of quality, filters and be made after drying modified beta-schardinger dextrin three times；It will change
Property beta-schardinger dextrin, algal polysaccharides, glutaraldehyde, ethylene glycol diglycidylether, citric acid and water in mass ratio 1:0.1:0.04:
0.1:30:100 mixing, are made spray liquid after stirring.
In the water that base socks are impregnated into its 7 times of quality, while adding base socks and the plants essential oil of water gross mass 6% into water
Antimosquito finishing agent, is heated up with 10 DEG C/min speed, and final temperature is controlled in 88 DEG C, washing process 4min；The plant
Essential oil antimosquito finishing agent includes：Plants essential oil 50wt%, water 50wt%.The plants essential oil includes：Wormwood extract 10wt%,
Peppermint extract 90wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 12 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,65 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 2h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 11 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 70wt% ethanol solutions
The volume ratio of solution is 1:5,80 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 1.5h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 130 DEG C will be arranged
It is dry, 40 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.6kg.
Embodiment 9
A kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, comprises the following steps：
(1) get the raw materials ready：Cotton is twisted to form spun yarn；Polyamide fibre, spandex are twisted to form filament yarn respectively；The line of spun yarn is close
Spend for 182dtex, the spun yarn twist is 301 twists/m, and long filament twist per unit is at 100 twists/m.
(2) socks are knitted：Using spun yarn as table yarn, the cladding 77.8dtex spandex filament yarn conducts of 33.3dtex polyester filaments yarn
In yarn, from the footwear machine of 168 pins, the program finished is imported into footwear machine, spun yarn, filament yarn are sent into footwear machine, socks are knitted
Machine is woven according to programmed instruction, and base socks are made.Cotton content is 70wt% in the base socks, and polyamide fibre content is 20wt%, ammonia
Synthetic fibre content is 10wt%.
(3) arrange：Spraying treatment is carried out to base socks with spray liquid, after spraying by base socks temperature be 50 DEG C, humidity be
1h is placed in tiling in 90% environment, and then to the Sodium Borohydride ethanol solution that base socks spray concentration is 5wt%, base socks are existed
Continue to tile at room temperature to place after 20h, base socks are cleaned into drying；Wherein the consumption of spray liquid is 2mL/cm3, Sodium Borohydride second
The consumption of alcoholic solution is 0.3mL/cm3。
The preparation method of the spray liquid is as follows：Beta-schardinger dextrin, o- iodoxy phenylpropenoic acid potassium, dimethyl sulfoxide (DMSO) are pressed into quality
Than 5:3:100 mixing, stirring reaction 4h, is filtrated to get filtered fluid at 55 DEG C, and 30 times, after stirring are diluted to filtered fluid with acetone
Secondary filter, takes solid and is dissolved in the water of 50 times of quality, filters and be made after drying modified beta-schardinger dextrin three times；It will change
Property beta-schardinger dextrin, algal polysaccharides, glutaraldehyde, ethylene glycol diglycidylether, citric acid and water in mass ratio 3:0.5:0.06:
0.2:40:100 mixing, are made spray liquid after stirring.
In the water that base socks are impregnated into its 7 times of quality, while adding base socks and the plants essential oil of water gross mass 6% into water
Antimosquito finishing agent, is heated up with 10 DEG C/min speed, and final temperature is controlled in 88 DEG C, washing process 4min；The plant
Essential oil antimosquito finishing agent includes：Plants essential oil 50wt%, water 50wt%.The plants essential oil includes：Wormwood extract 10wt%,
Peppermint extract 90wt%.
The extracting method of the wormwood extract is：By wormwood and the water mixed grinding of its 12 times of quality, wormwood slurry is obtained
Wormwood slurries are added to concentration to carry out ultrasonic extraction in 70wt% ethanol solutions, wherein wormwood slurries and ethanol are molten by liquid
The volume ratio of liquid is 1:3,65 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 2h；After extraction
It is filtrated to get wormwood extract.
The extracting method of the peppermint extract is：By dried peppermint leaf and the water mixed grinding of its 11 times of quality, peppermint is obtained
Slurries, peppermint slurries are added to concentration to carry out ultrasonic extraction, wherein peppermint slurries and ethanol in 70wt% ethanol solutions
The volume ratio of solution is 1:5,80 DEG C of extraction temperature, ultrasonic frequency 50KHz, ultrasonic power 500W, extraction time 1.5h；Extraction
Peppermint extract is filtrated to get after taking.
(4) shape：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 130 DEG C will be arranged
It is dry, 40 seconds processing times, obtain finished product quilted stockings；Wherein Stress control is in 1.6kg.
Comparative example
A kind of quilted stockings preparation method, step is as follows：
(1) get the raw materials ready：Table yarn uses 182dtex cotton yarns, and inner yarn coats 77.8dtex spandex yarns using 33.3dtex terylene；
(2) socks are knitted：Yarn feeding footwear machine is woven, base socks are made；Base socks include stocking blank, the stocking leg, heel, socks
Pin, toe；
(3) wash：The base socks woven are put into water washing device, temperature is heated up with 5 DEG C/min, after heating terminates, control
Temperature processed is handled 10 minutes at 80 DEG C；
(4) shape：The base ankle socks completed 160 DEG C of steam heating, drying on socks plate will be arranged, finished product quilted stockings is obtained.
Method of testing：
Experiment prepares six french heels, and (three pairs are that embodiment 4-6 is arranged by mosquito-proof, and three pairs are comparative example without anti-in addition
Mosquito arranges), a pair of is taken out by arranging to obtain mosquito-proof quilted stockings and the common quilted stockings of a pair of, is then placed in the case raised and there are about 100 mosquitoes
Inside body, four socks are individually positioned in four diagonal, timing three minutes, observe and record during this period mosquito in sample cloth cover
On stop fall number of times, in triplicate, embodiment and comparative example are identical using color.
Test result is as follows：
| Washing times | Mosquito sum | Stop falling number of times | |
| Embodiment 4 | 0 | 100 | 7±1 |
| 10 | 100 | 8±2 | |
| 20 | 100 | 10±2 | |
| Embodiment 5 | 0 | 100 | 8±2 |
| 10 | 100 | 10±2 | |
| 20 | 100 | 12±2 | |
| Embodiment 6 | 0 | 100 | 8±2 |
| 10 | 100 | 9±2 | |
| 20 | 100 | 11±2 | |
| Comparative example | 0 | 100 | 32±3 |
| Comparative example | 0 | 100 | 38±4 |
| Comparative example | 0 | 100 | 31±3 |
As seen from table, using the mosquito-proof quilted stockings of plants essential oil of the present invention, have to mosquito and significantly kill repellent action, and
By repeatedly washing (more than 10 times), all there is not excessive decline in mosquito-proof effect, there is good stability.
Raw materials used in the present invention, equipment, is the conventional raw material, equipment of this area unless otherwise noted；In the present invention
Method therefor, is the conventional method of this area unless otherwise noted.
It is described above, only it is presently preferred embodiments of the present invention, not the present invention is imposed any restrictions, it is every according to the present invention
Any simple modification, change and equivalent transformation that technical spirit is made to above example, still fall within the technology of the present invention side
The protection domain of case.
Claims (7)
1. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil, it is characterised in that comprise the following steps：
（1）Get the raw materials ready：Cotton or cotton are formed into spun yarn with terylene mixing twisting；Terylene, polyamide fibre, spandex are twisted respectively to form length
Gauze；The line density of spun yarn and filament yarn is 145dtex-330dtex, and the spun yarn twist is 301-1069 twists/m, filament yarn
The twist is below 150 twists/m；
（2）Knit socks：Using spun yarn as table yarn, filament yarn is compiled spun yarn, filament yarn feeding footwear machine as inner yarn
Knit, base socks are made；
（3）Arrange：Spraying treatment is carried out to base socks with spray liquid, after spraying by base socks temperature be 40-50 DEG C, humidity be 80-
1-3h is placed in tiling in 90% environment, then to the Sodium Borohydride ethanol solution that base socks spray concentration is 3-5wt%, by base socks
Continue to tile at room temperature to place after 10-20h, base socks are cleaned into drying；Wherein the consumption of spray liquid is 1-2mL/cm3, tetrahydrochysene
The consumption of boric acid sodium ethoxide solution is 0.1-0.3mL/cm3；The preparation method of the spray liquid is as follows：By beta-schardinger dextrin, o- iodine
Acyl group benzoic acid potassium, dimethyl sulfoxide (DMSO) 3-5 in mass ratio:1-3:100 mixing, stirring reaction 4-8h, is filtrated to get at 45-55 DEG C
Filtered fluid, dilutes 20-30 times to filtered fluid, secondary filter after stirring takes solid and is dissolved in 30-50 times of quality with acetone
In water, modified beta-schardinger dextrin is filtered and is made after drying three times；Will modified beta-schardinger dextrin, algal polysaccharides, glutaraldehyde, ethylene glycol two
Glycidol ether, citric acid and water 1-3 in mass ratio:0.1-0.5:0.04-0.06:0.1-0.2:30-40:100 mixing, stirring
Obtained spray liquid after uniform；
In the water that base socks are impregnated into its 4-8 times of quality, while adding base socks and water gross mass 1.5-15.9% plant into water
Essential oil antimosquito finishing agent, is heated up with 5-30 DEG C/min speed, and final temperature is controlled in 61-98 DEG C, washing process 3-
25min；The plants essential oil antimosquito finishing agent includes：Plants essential oil 3-82wt%, water 18-97wt%；
（4）Sizing：The base ankle socks completed steam heating, pressurization, baking on respective model socks plate and at 101-185 DEG C will be arranged
It is dry, processing time 15-180 second, obtain finished product quilted stockings；Wherein Stress control is in 0.8-2.2kg.
2. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 1, it is characterised in that in step（2）In,
Stocking blank is using 1 every 1 rib construction, and ammonification synthetic fibre filament yarn is padded；Socks body, heel, the stocking sole, toe plain weave, figured texture weave；Socks
Mouth uses 21S/1 cotton staple yarn+70D chinlon filament yarn double-contracting 180D spandex filament yarns；Socks body, the stocking sole, heel, toe are used
21S/1 cotton staple yarn+70D chinlon filament yarn looping 30D spandex filament yarns.
3. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 2, it is characterised in that knitting socks process
In, from 108 pins, 144 pins, 168 pins footwear machine, the program finished is imported into footwear machine, footwear machine enters according to programmed instruction
Row braiding.
4. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 1, it is characterised in that cotton in the base socks
Content is 60-70wt%, and terylene content is 10-20wt%, and polyamide fibre content is 10-20wt%, and spandex content is 1-10wt%.
5. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 1, it is characterised in that the plants essential oil
Including：Wormwood extract 3-97wt%, peppermint extract 3-97wt%.
6. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 5, it is characterised in that the wormwood extraction
The extracting method of liquid is：By wormwood and the water mixed grinding of its 10-20 times of quality, wormwood slurries are obtained, wormwood slurries are added
Ultrasonic extraction is carried out in being 70-80wt% ethanol solutions to concentration, the wherein volume ratio of wormwood slurries and ethanol solution is 1:2-
3,55-65 DEG C of extraction temperature, ultrasonic frequency 40-50KHz, ultrasonic power 400-500W, extraction time 1-2h；Mistake after extraction
Filter obtains wormwood extract.
7. a kind of preparation method of the mosquito-proof quilted stockings of plants essential oil as claimed in claim 5, it is characterised in that the peppermint extraction
The extracting method of liquid is：By dried peppermint leaf and the water mixed grinding of its 8-12 times of quality, peppermint slurries are obtained, peppermint slurries are added
Ultrasonic extraction is carried out in being 70-80wt% ethanol solutions to concentration, the wherein volume ratio of peppermint slurries and ethanol solution is 1:3-
5,70-80 DEG C of extraction temperature, ultrasonic frequency 40-50KHz, ultrasonic power 400-500W, extraction time 0.5-1.5h；Extraction
After be filtrated to get peppermint extract.
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| CN110106614A (en) * | 2019-02-26 | 2019-08-09 | 浙江鹏飞针织有限公司 | The weaving method of non-skid care function sock |
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| CN102792974A (en) * | 2012-08-16 | 2012-11-28 | 绍兴文理学院元培学院 | Mosquito repelling composition and mosquito repelling sports socks |
| CN203072909U (en) * | 2013-01-15 | 2013-07-24 | 浙江梦娜袜业股份有限公司 | Long rib-top socks |
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