CN105951453B - A kind of tranquilizing the mind based on double-walled microcapsules is calmed fabric and preparation method thereof - Google Patents
A kind of tranquilizing the mind based on double-walled microcapsules is calmed fabric and preparation method thereof Download PDFInfo
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- CN105951453B CN105951453B CN201610443847.6A CN201610443847A CN105951453B CN 105951453 B CN105951453 B CN 105951453B CN 201610443847 A CN201610443847 A CN 201610443847A CN 105951453 B CN105951453 B CN 105951453B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/49—Oxides or hydroxides of elements of Groups 8, 9, 10 or 18 of the Periodic System; Ferrates; Cobaltates; Nickelates; Ruthenates; Osmates; Rhodates; Iridates; Palladates; Platinates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
Abstract
The present invention provides a kind of preparation method of calm fabric of the tranquilizing the mind based on double-walled microcapsules, the following steps are included: Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos are cleaned, it dries, freeze-drying, it shreds to form plant powder, plant powder is placed in processing in critical carbon dioxide extractor and obtains plant extracts；Plant extracts is added in macromolecule emulsion agent solution, stirring and emulsifying, chitosan wall material, heating stirring is added, cooling obtains the solution of the microcapsules containing tranquilizing the mind；Calcined MAGNETITUM powder and aloe gel are added in microcapsule solution containing tranquilizing the mind, stirring, Arabic gum wall material is added, heating stirring is cooling, adds auxiliary agent and obtains calm finishing agent of calming the nerves；After the activated processing of fabric, after the calm finishing agent processing of tranquilizing the mind, preliminary drying, washing dries and obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules.
Description
Technical field
The invention belongs to textile material technical fields, and in particular to a kind of tranquilizing the mind based on double-walled microcapsules calm fabric and
Preparation method.
Background technique
With the high speed development of science and technology, people's lives are getting faster with work rhythm, the spirit pressure of more and more people
Power is impacted, and natural, stable, health life is increasingly by the yearning of people.Along with being constantly progressive for science, people
The mode of self-control is also more and more, and people begin to focus on the conditioning of details in daily life, has effects that tranquilizing the mind was calmed
Textile fabric has also complied with this trend.
All containing calm the effect of calming the nerves in the various plants of the Nature, the chemical component of main function is complex,
There are bases, glycoside, alcohols etc..It is also had been reported that at present by aromatics plant and is used to play the role of in textile calm tranquilizing the mind.
A kind of production technology of tranquilizing the mind textile fabric disclosed in Chinese patent CN 105088478A, will place raw material cotton thread and spandex soaks
Stain takes out heating, drying as filling yarn, obtains tranquilizing the mind textile fabric through weaving in the solution of lavender and Jasmine.In
A kind of pajama fabric preparation method with complex function disclosed in state patent CN 103938400B, with Vitwas E and
Lavender is wall material, and titanium dioxide-silver antibacterial agent is added as core material, polyurethane, prepares two-component through spray
The microcapsules of complex function, then microcapsules and thickener, binder are mixed to form finishing fluid, finally silk fabric is soaked
Roll to obtain have calm the nerves cook noodles, the pajama fabric of health-care and skin-care, antibiotic effect.One disclosed in Chinese patent CN 104179023B
The processing technology of kind tranquilizing and allaying excitement natural feather, after natural feather is carried out secondary washing second dehydration, drying sterilization is led in high-temperature steam
Enter the tranquilizing and allaying excitement agent containing semen ziziphi spinosae, the seed of Oriental arborvitae, tuber fleeceflower stem, Radix Polygalae, cortex albiziae, keel, dens draconis, lavender, rose and water, makes
Medicament and flavouring agent rest on the surface of natural feather, play the role of calm for a long time calm the nerves.
By the above-mentioned prior art it is found that being at present by direct impregnation or preparation by the effective component with tranquilizing the mind
The gimmick for forming microcapsules is attached to the surface of textile raw material, the fabric of direct impregnation finishing technique preparation, and effective component is held
Volatile, long term effect and water-wash resistance are also poor, and its microcapsules of fabric of Single-layer microcapsules preparation are easy breakage, lead
Cause the stability of tranquilizing the mind effect of fabric also poor.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of calm fabric of tranquilizing the mind based on double-walled microcapsules and its preparations
Method is utilized using the extract of Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos, calcined MAGNETITUM powder and aloe gel as raw material
Chitosan and Arabic gum prepare double-walled microcapsules as wall material, and the surface attachment double-walled microcapsules of fabric are obtained based on double-walled
The calm fabric of the tranquilizing the mind of microcapsules.The fabric of this method preparation contains multiple calm effect of calming the nerves, and microcapsules use double-walled
Form, finishing effect is more significant lasting, water-fastness.
In order to solve the above technical problems, the technical scheme is that
A kind of calm fabric of the tranquilizing the mind based on double-walled microcapsules, the table of the calm fabric of the tranquilizing the mind based on double-walled microcapsules
Face includes calm finishing agent of calming the nerves, and includes microcapsules and auxiliary agent in the calm finishing agent of calming the nerves, contains sieve in the microcapsules
Cloth bluish dogbane leaf extract, Lignum Aquilariae Resinatum extract, Wild jujube seeds extract, tuckahoe extracts, calcined MAGNETITUM powder and aloe extract and wall
Material, the wall material are chitosan and Arabic gum, and the microcapsules are double-walled microcapsules, and the Apocynum venetum Linn leaf extract sinks
Fragrant extract, Wild jujube seeds extract and tuckahoe extracts are that critical carbon dioxide extracts to obtain.
As a preferred embodiment of the above technical solution, the double-walled microcapsules include tranquilizing the mind microcapsules and calcined MAGNETITUM powder, aloe
Gel and Arabic gum wall material are extracted containing Apocynum venetum Linn leaf extract, Lignum Aquilariae Resinatum extract, semen ziziphi spinosae in the tranquilizing the mind microcapsules
Object, tuckahoe extracts and chitosan wall material.
The preparation method of the calm fabric of the tranquilizing the mind that the present invention also provides a kind of based on double-walled microcapsules, comprising the following steps:
(1) Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos are cleaned, is dried, be lyophilized, shred to form plant powder, will plant
Object powder is placed in processing in critical carbon dioxide extractor and obtains plant extracts；
(2) plant extracts by step (1) preparation is added in macromolecule emulsion agent solution, with 800-1000r/min's
Revolving speed stirring and emulsifying 1-2h, is added chitosan wall material, and the heating stirring 1-2h at 60-65 DEG C is cooled to room temperature to obtain containing tranquilizing the mind
The solution of microcapsules；
(3) calcined MAGNETITUM powder and aloe gel are added in the microcapsule solution containing tranquilizing the mind of step (2) preparation, with 500-
The revolving speed of 700r/min stirs, and Arabic gum wall material is added, and heating stirring 1.5-2h, is cooled to room temperature at 60-70 DEG C, then plus
Enter auxiliary agent and obtains calm finishing agent of calming the nerves；
(4) by after the activated processing of fabric, after finishing agent processing is calmed in the tranquilizing the mind of step (3) preparation, preliminary drying is washed,
Drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules.
As a preferred embodiment of the above technical solution, in the step (1), Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos matter
Amount is than being 4-5:2-2.5:1-1.5:0.5-1.
As a preferred embodiment of the above technical solution, in the step (2), macromolecule emulsion agent solution is acrylic acid ester emulsion,
Chitosan wall material is the chitosan solution that mass fraction is 10-25%.
As a preferred embodiment of the above technical solution, in the step (2), plant extracts, macromolecule emulsion agent solution and shell
The volume ratio of glycan wall material is 0.5-2:5-10:15-25.
As a preferred embodiment of the above technical solution, in the step (3), the partial size of calcined MAGNETITUM powder is 50-100 mesh.
As a preferred embodiment of the above technical solution, in the step (3), calcined MAGNETITUM powder, aloe gel, microcapsules containing tranquilizing the mind
Solution and the solid-liquid ratio of Arabic gum wall material are 0.5-2g:3-5g:8-16ml:4-6g.
As a preferred embodiment of the above technical solution, in the step (3), auxiliary agent can be in dispersing agent, softening agent, thickener
It is one or several kinds of.
As a preferred embodiment of the above technical solution, in the step (4), activation processing can be at alkali process or plasma
Reason.
Compared with prior art, the invention has the following advantages:
(1) the calm web surface of the tranquilizing the mind prepared by the present invention based on double-walled microcapsules is attached to double-walled microcapsules, double-walled
The wall material of microcapsules selects chitosan and Arabic gum, and chitosan has excellent sustained release performance, and Arabic gum has outstanding
Emulsifiability, selects Arabic gum as outer layer wall material, and Arabic gum can carry out good protective effect, mobility to core material
It is good, the surface for being attached to fabric of uniform microcapsule can be made, select chitosan as internal layer wall material, keep inner sandwich layer slow
Release, guarantees the effect of the long duration of microcapsule dressing agent, and is both natural green environment-friendly materials, and the two is selected to make
For wall material, guarantee the environmentally protective of finishing agent.
(2) contain Apocynum venetum Linn leaf, agalloch eaglewood, wild jujube in the calm fabric of the tranquilizing the mind prepared by the present invention based on double-walled microcapsules
Extract, calcined MAGNETITUM powder and the aloe gel of Renhe Poria cocos, calcined MAGNETITUM powder, agalloch eaglewood have the effect of tranquilizing the mind quelling, Poria cocos,
Apocynum venetum Linn leaf and semen ziziphi spinosae, which have the function of calming the nerves, falls asleep, and aloe has the function of antibacterial bacteriostatic, promotes blood circulation, by this
A little substances are all plant extracts, in conjunction with microcapsules prepared by chitosan and Arabic gum, so that user is calmed the nerves, town
It is fixed, sleep, and make fabric bacteria can be prevented from growing, it is green, safe and healthy.
(3) plant extracts in the fabric of the calm fabric of the tranquilizing the mind prepared by the present invention based on double-walled microcapsules is through critical
Carbon dioxide abstraction obtains, precision and pure more preferable, compound with microcapsules again after the activated processing of fabric, raising microcapsules and fibre
Binding force between dimension, and binder is not used, it is environmentally protective.
(4) the calm fabric fragrant of the tranquilizing the mind prepared by the present invention based on double-walled microcapsules, antibacterial bacteriostatic, tranquilizing the mind are calm
It falls asleep, effect is long-acting, water-fastness and environmentally protective, can be used for preparing textile garment or family's textile fabric.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail, herein illustrative examples and explanation of the invention
For explaining the present invention, but it is not as a limitation of the invention.
Embodiment 1:
(1) in parts by mass, 4 parts of Apocynum venetum Linn leaf, 2 parts of agalloch eaglewood, 1 part of semen ziziphi spinosae and 0.5 part of Poria cocos are washed
Only, it dries, is lyophilized, shreds the plant powder to form 50 mesh, plant powder is placed in critical carbon dioxide extractor and is handled
To plant extracts.
(2) it counts, 0.5 part of plant extracts is added in 5 parts of acrylic acid ester emulsion, with 800r/min's by volume
Revolving speed stirring and emulsifying 1h, the chitosan solution that the mass fraction for being added 15 parts is 10%, heating stirring 1h, is cooled at 60 DEG C
Room temperature obtains the solution of the microcapsules containing tranquilizing the mind.
(3) aloe gel of the calcined MAGNETITUM powder of 50 mesh of 0.5g and 3g are added in the microcapsule solution containing tranquilizing the mind of 8ml,
It stirring with the revolving speed of 500r/min, the Arabic gum wall material of 4g is added, heating stirring 1.5h, is cooled to room temperature at 60- DEG C, then
Dispersing agent, softening agent, thickener is added and obtains calm finishing agent of calming the nerves.
(4) by fabric after plasma-activated processing, the calm finishing agent of dipping tranquilizing the mind, preliminary drying 10min, water at 50 DEG C
It washes, drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at 65 DEG C.
Embodiment 2:
(1) in parts by mass, by 5 parts of Apocynum venetum Linn leaf, 2.5 parts of agalloch eaglewood, 1.5 parts of semen ziziphi spinosae and 1 part of Poria cocos
It cleans, dries, be lyophilized, shred the plant powder to form 100 mesh, plant powder is placed in critical carbon dioxide extractor and is handled
Obtain plant extracts.
(2) it counts, 02 part of plant extracts is added in 10 parts of acrylic acid ester emulsion, with 1000r/min by volume
Revolving speed stirring and emulsifying 2h, the chitosan solution that the mass fraction for being added 25 parts is 25%, the heating stirring 2h at 65 DEG C is cooling
The solution of the microcapsules containing tranquilizing the mind is obtained to room temperature.
(3) aloe gel of the calcined MAGNETITUM powder of 100 mesh of 2g and 5g are added in the microcapsule solution containing tranquilizing the mind of 16ml,
It stirring with the revolving speed of 700r/min, the Arabic gum wall material of 6g is added, heating stirring 2h, is cooled to room temperature at 70 DEG C, then plus
Enter dispersing agent and thickener obtains calm finishing agent of calming the nerves.
(4) by fabric after alkali process is handled, the calm finishing agent of tranquilizing the mind is padded, the preliminary drying 15min at 50 DEG C is washed, 65
Drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at DEG C.
Embodiment 3:
(1) in parts by mass, by 4.5 parts of Apocynum venetum Linn leaf, 2.2 parts of agalloch eaglewood, 1.3 parts of semen ziziphi spinosae and 0.7 part
Poria cocos is cleaned, and is dried, and is lyophilized, is shredded the plant powder to form 80 mesh, plant powder is placed in critical carbon dioxide extractor
Processing obtains plant extracts.
(2) it counts, 0.9 part of plant extracts is added in 7 parts of acrylic acid ester emulsion, with 900r/min's by volume
Revolving speed stirring and emulsifying 1.5h, the chitosan solution that the mass fraction for being added 20 parts is 15%, heating stirring 1.5h, cold at 62 DEG C
But the solution of the microcapsules containing tranquilizing the mind is obtained to room temperature.
(3) aloe gel of the calcined MAGNETITUM powder of 80 mesh of 1g and 4g are added in the microcapsule solution containing tranquilizing the mind of 10ml,
It stirring with the revolving speed of 550r/min, the Arabic gum wall material of 5g is added, heating stirring 1.5h, is cooled to room temperature at 65 DEG C, then
Dispersing agent is added and softening agent obtains calm finishing agent of calming the nerves.
(4) by fabric after plasma-activated processing, the calm finishing agent of coating tranquilizing the mind, preliminary drying 12min, water at 50 DEG C
It washes, drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at 65 DEG C.
Embodiment 4:
(1) in parts by mass, by 5 parts of Apocynum venetum Linn leaf, 2 parts of agalloch eaglewood, 1.5 parts of semen ziziphi spinosae and 0.5 part of Poria cocos
It cleans, dries, be lyophilized, shred the plant powder to form 100 mesh, plant powder is placed in critical carbon dioxide extractor and is handled
Obtain plant extracts.
(2) it counts, 2 parts of plant extracts is added in 5 parts of acrylic acid ester emulsion by volume, with turning for 850r/min
Fast stirring and emulsifying 2h, the chitosan solution that the mass fraction for being added 15 parts is 25%, heating stirring 1h, is cooled to room at 65 DEG C
Temperature obtains the solution of the microcapsules containing tranquilizing the mind.
(3) aloe gel of the calcined MAGNETITUM powder of 50 mesh of 2g and 5g are added in the microcapsule solution containing tranquilizing the mind of 8ml, with
The revolving speed of 700r/min stirs, and the Arabic gum wall material of 4g is added, and heating stirring 1.5h, is cooled to room temperature at 70 DEG C, then plus
Enter softening agent and thickener obtains calm finishing agent of calming the nerves.
(4) it by fabric after plasma-activated processing, impregnates, pad, coating the calm finishing agent of tranquilizing the mind, it is pre- at 50 DEG C
12min is dried, is washed, drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at 65 DEG C.
Embodiment 5:
(1) in parts by mass, 5 parts of Apocynum venetum Linn leaf, 2 parts of agalloch eaglewood, 1 part of semen ziziphi spinosae and 0.6 part of Poria cocos are washed
Only, it dries, is lyophilized, shreds the plant powder to form 60 mesh, plant powder is placed in critical carbon dioxide extractor and is handled
To plant extracts.
(2) it counts, 1.5 parts of plant extracts is added in 6 parts of acrylic acid ester emulsion, with 900r/min's by volume
Revolving speed stirring and emulsifying 1h, the chitosan solution that the mass fraction for being added 15 parts is 15%, heating stirring 2h, is cooled at 60 DEG C
Room temperature obtains the solution of the microcapsules containing tranquilizing the mind.
(3) aloe gel of the calcined MAGNETITUM powder of 100 mesh of 1.5g and 3g are added to the microcapsule solution containing tranquilizing the mind of 15ml
In, it stirring with the revolving speed of 600r/min, the Arabic gum wall material of 6g is added, heating stirring 1.5h, is cooled to room temperature at 60 DEG C,
It adds dispersing agent, softening agent and thickener and obtains calm finishing agent of calming the nerves.
(4) by fabric after plasma-activated processing, the calm finishing agent of coating tranquilizing the mind, preliminary drying 15min, water at 50 DEG C
It washes, drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at 65 DEG C.
Embodiment 6:
(1) in parts by mass, 5 parts of Apocynum venetum Linn leaf, 2 parts of agalloch eaglewood, 1.5 parts of semen ziziphi spinosae and 1 part of Poria cocos are washed
Only, it dries, is lyophilized, shreds the plant powder to form 100 mesh, plant powder is placed in critical carbon dioxide extractor and is handled
To plant extracts.
(2) it counts, 1.5 parts of plant extracts is added in 10 parts of acrylic acid ester emulsion, with 800r/min by volume
Revolving speed stirring and emulsifying 1.5h, be added 20 parts mass fraction be 15% chitosan solution, heating stirring 1h, cold at 65 DEG C
But the solution of the microcapsules containing tranquilizing the mind is obtained to room temperature.
(3) aloe gel of the calcined MAGNETITUM powder of the 50- mesh of 1g and 5g are added in the microcapsule solution containing tranquilizing the mind of 10ml,
It stirring with the revolving speed of 600r/min, the Arabic gum wall material of 4g is added, heating stirring 1.5h, is cooled to room temperature at 70 DEG C, then
Dispersing agent is added and softening agent obtains calm finishing agent of calming the nerves.
(4) by fabric after plasma-activated processing, the calm finishing agent of coating tranquilizing the mind, preliminary drying 15min, water at 50 DEG C
It washes, drying obtains the calm fabric of the tranquilizing the mind based on double-walled microcapsules at 65 DEG C.
Through detecting, the result of the lasting rate of the calm fabric of the tranquilizing the mind based on double-walled microcapsules of embodiment 1-6 preparation is as follows
It is shown:
As seen from the above table, the tranquilizing the mind prepared by the present invention based on double-walled microcapsules is calmed, and fabric is water-fastness, crocking resistance
It is excellent, it can act on for a long time and play the role of tranquilizing the mind quelling.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (9)
- A kind of fabric 1. tranquilizing the mind based on double-walled microcapsules is calmed, it is characterised in that: the tranquilizing the mind town based on double-walled microcapsules The surface for determining fabric includes calm finishing agent of calming the nerves, and includes microcapsules and auxiliary agent, micro- glue in the calm finishing agent of calming the nerves Contain Apocynum venetum Linn leaf extract, Lignum Aquilariae Resinatum extract, Wild jujube seeds extract, tuckahoe extracts, calcined MAGNETITUM powder and aloe in capsule Gel and wall material, the wall material are chitosan and Arabic gum, and the microcapsules are double-walled microcapsules, and the Apocynum venetum Linn leaf mentions Taking object, Lignum Aquilariae Resinatum extract, Wild jujube seeds extract and tuckahoe extracts is that critical carbon dioxide extracts to obtain, the double-walled microcapsules It is red containing spreading out in the tranquilizing the mind microcapsules comprising tranquilizing the mind microcapsules and calcined MAGNETITUM powder, aloe gel and Arabic gum wall material Sesame slices extract, Lignum Aquilariae Resinatum extract, Wild jujube seeds extract, tuckahoe extracts and chitosan wall material.
- 2. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules, it is characterised in that: the following steps are included:(1) Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos are cleaned, is dried, be lyophilized, shred to form plant powder, by Plant Powder End is placed in processing in critical carbon dioxide extractor and obtains plant extracts；(2) plant extracts by step (1) preparation is added in macromolecule emulsion agent solution, with the revolving speed of 800-1000r/min Stirring and emulsifying 1-2h, is added chitosan wall material, and the heating stirring 1-2h at 60-65 DEG C is cooled to room temperature to obtain containing micro- glue of calming the nerves The solution of capsule；(3) calcined MAGNETITUM powder and aloe gel are added in the microcapsule solution containing tranquilizing the mind of step (2) preparation, with 500-700r/ The revolving speed of min stirs, and Arabic gum wall material is added, heating stirring 1.5-2h, is cooled to room temperature at 60-70 DEG C, adds and helps Agent obtains calm finishing agent of calming the nerves；(4) by after the activated processing of fabric, after finishing agent processing is calmed in the tranquilizing the mind of step (3) preparation, preliminary drying is washed, drying Obtain the calm fabric of the tranquilizing the mind based on double-walled microcapsules.
- 3. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (1), Apocynum venetum Linn leaf, agalloch eaglewood, semen ziziphi spinosae and Poria cocos mass ratio be 4-5:2-2.5:1-1.5:0.5-1.
- 4. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (2), macromolecule emulsion agent solution is acrylic acid ester emulsion, and chitosan wall material is that mass fraction is 10-25% Chitosan solution.
- 5. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (2), the volume ratio of plant extracts, macromolecule emulsion agent solution and chitosan wall material is 0.5-2:5-10: 15-25。
- 6. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (3), the partial size of calcined MAGNETITUM powder is 50-100 mesh.
- 7. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (3), calcined MAGNETITUM powder, aloe gel, microcapsule solution containing tranquilizing the mind and Arabic gum wall material solid-liquid ratio be 0.5-2g:3-5g:8-16ml:4-6g.
- 8. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (3), auxiliary agent can be one of dispersing agent, softening agent, thickener or several.
- 9. a kind of preparation method of the calm fabric of tranquilizing the mind based on double-walled microcapsules according to claim 2, feature exist In: in the step (4), activation processing can be alkali process or corona treatment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610443847.6A CN105951453B (en) | 2016-06-16 | 2016-06-16 | A kind of tranquilizing the mind based on double-walled microcapsules is calmed fabric and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610443847.6A CN105951453B (en) | 2016-06-16 | 2016-06-16 | A kind of tranquilizing the mind based on double-walled microcapsules is calmed fabric and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105951453A CN105951453A (en) | 2016-09-21 |
| CN105951453B true CN105951453B (en) | 2019-03-22 |
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| CN111012831A (en) * | 2018-10-10 | 2020-04-17 | 泰州医药城国科化物生物医药科技有限公司 | Wild jujube kernel oil microcapsule powder and preparation method and application thereof |
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| CN109925983B (en) * | 2019-03-08 | 2021-12-28 | 紫罗兰家纺科技股份有限公司 | Shea butter-based double-layer microcapsule and method for finishing same into textile fabric |
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