CN106468016B - A kind of removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract and preparation method thereof - Google Patents
A kind of removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract and preparation method thereof Download PDFInfo
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- CN106468016B CN106468016B CN201610838924.8A CN201610838924A CN106468016B CN 106468016 B CN106468016 B CN 106468016B CN 201610838924 A CN201610838924 A CN 201610838924A CN 106468016 B CN106468016 B CN 106468016B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
- D06M13/03—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons with unsaturated hydrocarbons, e.g. alkenes, or alkynes
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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Abstract
The present invention provides a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract, the following steps are included: fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, peach leaf powder is formed, for use, by peach leaf powder, it immerses in ethanol water respectively, in methanol solution and petroleum ether solution, extracts an extract, second extract and extract three times is obtained by filtration respectively；By an extract, second extract, extract is mixed to form peach leaf extract three times, and rotary evaporation concentration, is added cellulose whiskers and Chitosan-coated forms finishing agent；Fluffy cotton fiber is impregnated into finishing agent, constant temperature oscillation, is taken out, washed, drying weaves to form fabric with colorful cotton fibre.The comfortable moisture absorption of fabric prepared by the present invention is ventilative, also has effects that removing miliaria and relieving itching mosquito repellent.
Description
Technical field
The invention belongs to textile material technical fields, and in particular to a kind of removing miliaria and relieving itching mosquito repellent cotton of cherry apple leaf extract is knitted
Object and preparation method thereof.
Background technique
Prickly heat is also known as sweat spore rash, is to be discharged due to sweat unsmooth, is stranded in intradermal, causes the sudoriferous duct of skin by skin
Cutin and dead cell when blocking, the sweat in sweat gland can be risen brokenly, cause sudoriferous duct wall flow into around block, it is caused
Inflammation around sweat gland.Due to summer high temperature sweltering heat, the skin of baby or children are tender, and sweat gland is undeveloped, are easy to produce prickly heat,
And prickly heat scratchy, burning heat sensation again, it is easy to make baby or children to have the fidgets, therefore, is suitable for the production of the miliaria of dispelling of baby or children
Product are particularly important.
Miliaria product of dispelling on the market is mostly liniment, ointment and emulsifiable paste at present, but for baby or the spy of the delicate skin of children
Different property, need to select it is pure natural, without irritating to infant and have the ingredient of potential risk, additionally need to meet middle national treasure
Precious skin and system, cannot select excessively refrigerant product.One kind disclosed in Chinese patent CN 102860967A has miliaria of dispelling
The baby skin protection product formula of antipruritic function, the skin care item formula in contain honeysuckle, lavender, folium artemisiae argyi, kuh-seng, borneol, peppermint
The natural plants such as brain, camphor, jojoba oil, macadimia nut oil, honey, shea butter, licorice root extract, oat beta-glucan at
Point.A kind of baby's skin toner removing miliaria and relieving itching condensation disclosed in Chinese patent CN 103720617B and preparation method thereof, the product is main
Including deionized water, carbomer, triethanolamine, antiallergic antipruritic, baby's liquid distilled from honeysuckle flowers or lotus leaves stoste, mung bean activity stoste, preservative, second
Alcohol, essence and solubilizer.By the above-mentioned prior art it is found that miliaria plant extracts of dispelling is as major function substance and other auxiliary agent phases
In conjunction with being prepared watery, emulsus and product paste, but the ingredient of these products and it is not all all-natural product, Er Qienan
Long-term protection is carried out with the skin to baby or children.
Peach leaf belongs to the medicinal material of early stage, contains sugared two, naringenin, quininic acid, lycopene, almond folic acid phthalein in peach leaf
Amine, cyanogen glycosides etc., can extracting through different reagents, main function is sweating eliminating phlegm, and disappear wet desinsection, controls intermittent headache and other effects, peach
Leaf external application is for oral administration with clearing heat and detoxicating, antipruritic effect of desinsection.Product based on peach leaf at present also there are many, such as peach leaf drug
Toothpaste, peach leaf are dispelled miliaria water, peach leaf suppository etc., but are not much and are seen for application of the peach leaf in terms of weaving.
The present invention miliaria plant extracts that will dispel is combined with cotton fabric, providing cotton fabric removing miliaria and relieving itching function of driving mosquitoes, and
Do not influence soft, the ventilative and moisture pick-up properties of cotton fabric, can the skin to baby or children prevented and treated for a long time.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract, functions
Material is peach leaf extract, and the effective component in peach leaf is sufficiently extracted as extracting solution by ethyl alcohol, methanol and petroleum ether, will be had
The inside and surface of ingredient attachment with fibrous crystal palpus are imitated, then forms stabilised finish agent with Chitosan-coated, is refilled in raising
In cotton fiber, weave to form fabric with colorful cotton fibre.The present invention makes full use of the effective component in peach leaf, and substance used is all
Pure natural substance, no potential danger ingredient non-stimulated to baby or child skin have environmentally protective safety, and removing miliaria and relieving itching is driven
The effect of mosquito, can the skin to baby or children carry out permanent protection and a variety of skin diseases of prevention.
In order to solve the above technical problems, the technical scheme is that
A kind of removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract, the removing miliaria and relieving itching mosquito repellent cotton of the cherry apple leaf extract
Fabric includes cotton fabric and finishing agent, includes peach leaf extract, cellulose whiskers and chitosan in the finishing agent, the cotton is knitted
Object includes fluffy cotton fiber and colorful cotton fibre.
As a preferred embodiment of the above technical solution, the peach leaf extract includes lycopene, naringenin, flavonoids and tannin
Class, the fluffy cotton fiber are the cotton fiber of surface nappy.
The present invention also provides a kind of preparation methods of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract, including following step
It is rapid:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, and sieving forms peach leaf powder, for use, by peach
Leaf powder is immersed in ethanol water and is stood with solid-liquid ratio 1g:30-40ml, heating extraction, be obtained by filtration an extract and
Filter residue immerses a filter residue in methanol solution, secondary mention is obtained by filtration in heating extraction with solid-liquid ratio 1g:40-50ml
Object and secondary filter residue are taken, secondary filter residue is immersed in petroleum ether solution, ultrasonic extraction filters with solid-liquid ratio 1g:40-50ml
To extract three times and three times filter residue；
(2) by step (1) preparation an extract second extract, extract is mixed to form peach leaf extract three times,
Rotary evaporation concentration, is added cellulose whiskers, and stirring adds Chitosan-coated and forms finishing agent；
(3) fluffy cotton fiber being impregnated into the finishing agent of step (2) preparation, constant temperature oscillation takes out, it washes, drying, with
Colorful cotton fibre weaves the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract.
As a preferred embodiment of the above technical solution, in the step (1), the partial size of peach leaf powder is 1-20 μm.
As a preferred embodiment of the above technical solution, in the step (1), extract is flavonoids and naringenin, secondary
Extract is quininic acid, and extract is lycopene three times.
As a preferred embodiment of the above technical solution, in the step (1), the volume ratio of ethanol water is 1:0.5-0.8.
As a preferred embodiment of the above technical solution, in the step (2), the mass fraction of peach leaf extract is 15-30%.
As a preferred embodiment of the above technical solution, in the step (2), peach leaf extract, cellulose whiskers and chitosan
Mass ratio is 1:1.2-1.5:0.5-2.
As a preferred embodiment of the above technical solution, in the step (3), the temperature of constant temperature oscillation is 60-70 DEG C, and the time is
20-30min。
As a preferred embodiment of the above technical solution, in the step (3), the bath raio of dipping is 1:30-50.
Compared with prior art, the invention has the following advantages:
(1) functional material is peach leaf extraction in the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract prepared by the present invention
Object sufficiently extracts as extracting solution the effective component in peach leaf by ethyl alcohol, methanol and petroleum ether, such as flavone compound, shaddock
Pi Su, peaceful acids and lycopene, flavone compound and naringenin all have very strong antioxidation, can eliminate oxygen freedom
Base and anti-inflammatory, moreover it is possible to safeguard that metabolic balance, peaceful acids can interact with the protein of skin surface, have very strong disease-resistant
Cytotoxic activity, lycopene can improve the immunity of body, play the role of prevention to multiple dermatosis, the present invention also added fibre
Plain whisker and chitosan are tieed up, plurality of active ingredients is attached to the inside and surface of fibrous crystal palpus, then formed with Chitosan-coated
Stabilised finish agent improves the action time of peach leaf effective component, lowers the loss of effective component, keeps effective component uniformly lasting
The surface for acting on skin, play the purpose of removing miliaria and relieving itching mosquito repellent.
(2) contain fluffy cotton fiber in the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract prepared by the present invention, it is fluffy
The cotton fiber of pine is the cotton fiber of surface nappy, and peach leaf finishing agent can be filled, be formed steady by the villus on cotton fiber surface
Fixed environment avoids fabric in use, because friction, washing and wrinkle factor caused by effective component excessive loss,
The stress degree for reducing effective component, improves the utilization rate of effective component.Then it weaves to form fabric with colorful cotton fibre, not shadow
Ring the performances such as feel, the ventilative, moisture-inhibiting of fabric.
(3) it is made full use of in the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract prepared by the present invention effective in peach leaf
Ingredient, substance used are all pure natural substance, non-stimulated to baby or child skin, no potential danger ingredient, have green ring
Ensure safety, the effect of removing miliaria and relieving itching mosquito repellent, can the skin to baby or children carry out permanent protection and a variety of skins of prevention
Disease.
Specific embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail, herein illustrative examples and explanation of the invention
For explaining the present invention, but it is not as a limitation of the invention.
Embodiment 1:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:30ml, immerses in the ethanol water that volume ratio is 1:0.5 for use and stands 6h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in heating extraction 2h at 60 DEG C, by a filter residue, with material
Liquor ratio 1g:40ml immerses in methanol solution, and the second extract and two of quininic acid is obtained by filtration in the heating extraction 3h at 50 DEG C
Secondary filter residue immerses secondary filter residue in petroleum ether solution, the ultrasonic extraction 30min under 200W power with solid-liquid ratio 1g:40ml,
The extract three times and filter residue three times of lycopene is obtained by filtration.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
15% peach leaf extract will be added 1.2 parts of cellulose whiskers, stir 30min, add 0.5 in 1 part of peach leaf extract
The Chitosan-coated of part, is sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:30 with bath raio, is impregnated into finishing agent, constant temperature oscillation 20min, takes at 60 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 2:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:40ml, immerses in the ethanol water that volume ratio is 1:0.8 for use and stands 10h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in the heating extraction 3h at 60 DEG C, by a filter residue, with
Solid-liquid ratio 1g:50ml, immerse methanol solution in, the heating extraction 4h at 50 DEG C, be obtained by filtration quininic acid second extract and
Secondary filter residue immerses secondary filter residue in petroleum ether solution, the ultrasonic extraction under 500W power with solid-liquid ratio 1g:50ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 60min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
30% peach leaf extract will be added 1.5 cellulose whiskers, stir 60min, add 2 parts in 1 part of peach leaf extract
Chitosan-coated is sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:50 with bath raio, is impregnated into finishing agent, constant temperature oscillation 30min, takes at 70 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 3:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:35ml, immerses in the ethanol water that volume ratio is 1:0.6 for use and stands 8h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in heating extraction 2.5h at 60 DEG C, by a filter residue, with
Solid-liquid ratio 1g:45ml immerses in methanol solution, and the second extract of quininic acid is obtained by filtration in the heating extraction 3.5h at 50 DEG C
With secondary filter residue, secondary filter residue is immersed in petroleum ether solution, the ultrasonic extraction under 300W power with solid-liquid ratio 1g:45ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 50min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
25% peach leaf extract will be added 1.3 cellulose whiskers, stir 40min, add 1.5 parts in 1 part of peach leaf extract
Chitosan-coated, be sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:45 with bath raio, is impregnated into finishing agent, constant temperature oscillation 25min, takes at 65 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 4:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:30ml, immerses in the ethanol water that volume ratio is 1:0.8 for use and stands 6-
10h, the heating extraction 2h at 60 DEG C are obtained by filtration the extract and a filter residue of flavonoids and naringenin, will once filter
Slag is immersed in methanol solution, the second extraction of quininic acid is obtained by filtration in the heating extraction 3h at 50 DEG C with solid-liquid ratio 1g:50ml
Object and secondary filter residue immerse secondary filter residue in petroleum ether solution, the ultrasonic extraction under 200W power with solid-liquid ratio 1g:50ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 60min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
30% peach leaf extract will be added 1.2 cellulose whiskers, stir 40min, add 1.5 parts in 1 part of peach leaf extract
Chitosan-coated, be sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:45 with bath raio, is impregnated into finishing agent, constant temperature oscillation 20min, takes at 60 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 5:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:35ml, immerses in the ethanol water that volume ratio is 1:0.6 for use and stands 8h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in heating extraction 2.5h at 60 DEG C, by a filter residue, with
Solid-liquid ratio 1g:50ml immerses in methanol solution, and the second extract of quininic acid is obtained by filtration in the heating extraction 3.5h at 50 DEG C
With secondary filter residue, secondary filter residue is immersed in petroleum ether solution, the ultrasonic extraction under 400W power with solid-liquid ratio 1g:50ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 50min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
25% peach leaf extract will be added 1.4 cellulose whiskers, stir 50min, add 1.5 parts in 1 part of peach leaf extract
Chitosan-coated, be sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:45 with bath raio, is impregnated into finishing agent, constant temperature oscillation 20min, takes at 65 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 6:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:40ml, immerses in the ethanol water that volume ratio is 1:0.6 for use and stands 6h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in heating extraction 3h at 60 DEG C, by a filter residue, with material
Liquor ratio 1g:50ml, immerse methanol solution in, the heating extraction 3.5h at 50 DEG C, be obtained by filtration quininic acid second extract and
Secondary filter residue immerses secondary filter residue in petroleum ether solution, the ultrasonic extraction under 450W power with solid-liquid ratio 1g:45ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 60min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
23% peach leaf extract will be added 1.3 cellulose whiskers, stir 50min, add 1 part in 1 part of peach leaf extract
Chitosan-coated is sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:40 with bath raio, is impregnated into finishing agent, constant temperature oscillation 30min, takes at 70 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 7:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:40ml, immerses in the ethanol water that volume ratio is 1:0.8 for use and stands 8h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in heating extraction 3h at 60 DEG C, by a filter residue, with material
Liquor ratio 1g:40ml immerses in methanol solution, and the second extract and two of quininic acid is obtained by filtration in the heating extraction 4h at 50 DEG C
Secondary filter residue immerses secondary filter residue in petroleum ether solution, the ultrasonic extraction 60min under 350W power with solid-liquid ratio 1g:40ml,
The extract three times and filter residue three times of lycopene is obtained by filtration.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration, forming mass fraction is
20% peach leaf extract will be added 1.4 cellulose whiskers, stir 50min, add 1 part in 1 part of peach leaf extract
Chitosan-coated is sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:40 with bath raio, is impregnated into finishing agent, constant temperature oscillation 25min, takes at 65 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Embodiment 8:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, sieving, forms the peach leaf that partial size is 1-20 μm
Powder by peach leaf powder, with solid-liquid ratio 1g:30ml, immerses in the ethanol water that volume ratio is 1:0.7 for use and stands 10h,
The extract and a filter residue of flavonoids and naringenin is obtained by filtration in the heating extraction 3h at 60 DEG C, by a filter residue, with
Solid-liquid ratio 1g:50ml immerses in methanol solution, and the second extract of quininic acid is obtained by filtration in the heating extraction 3.5h at 50 DEG C
With secondary filter residue, secondary filter residue is immersed in petroleum ether solution, the ultrasonic extraction under 450W power with solid-liquid ratio 1g:50ml
The extract three times and filter residue three times of lycopene is obtained by filtration in 40min.
(2) by an extract, second extract, three times extract mixing, rotary evaporation concentration forms mass fraction
25% peach leaf extract will be added 1.5 cellulose whiskers, stir 50min, add 1 part in 1 part of peach leaf extract
Chitosan-coated is sufficiently stirred to form uniform finishing agent.
(3) by fluffy cotton fiber, it is 1:50 with bath raio, is impregnated into finishing agent, constant temperature oscillation 20min, takes at 70 DEG C
Out, it washes, the removing miliaria and relieving itching mosquito repellent cotton fabric to form cherry apple leaf extract is weaved in drying with colorful cotton fibre.
Through detecting, embodiment 1-8 preparation cherry apple leaf extract removing miliaria and relieving itching mosquito repellent cotton fabric antibacterial, it is anti-oxidant,
Mosquito repellent, ventilative, the result of moisture-inhibiting is as follows:
As seen from the above table, the breathable moisture permeability of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract prepared by the present invention
Variation is little, but antibacterial, anti-oxidant and repelling effect are good.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology all without departing from the spirit and scope of the present invention, carries out modifications and changes to above-described embodiment.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should be covered by the claims of the present invention.
Claims (8)
1. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract, it is characterised in that: described to be mentioned containing peach leaf
The removing miliaria and relieving itching mosquito repellent cotton fabric for taking object includes cotton fabric and finishing agent, includes peach leaf extract, cellulose in the finishing agent
Whisker and chitosan, the cotton fabric include fluffy cotton fiber and colorful cotton fibre, the peach leaf extract include lycopene,
Naringenin, quininic acid and flavonoids, the fluffy cotton fiber are the cotton fiber of surface nappy；
The preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of the cherry apple leaf extract, comprising the following steps:
(1) fresh wild peach leaf is cleaned, vapor sterilant dries in the shade, and crushes, and sieving forms peach leaf powder, for use, by peach leaf powder
End is immersed in ethanol water and is stood with solid-liquid ratio 1g:30-40mL, heating extraction, and extract and primary is obtained by filtration
Filter residue immerses a filter residue in methanol solution, second extract is obtained by filtration in heating extraction with solid-liquid ratio 1g:40-50mL
With secondary filter residue, secondary filter residue is immersed in petroleum ether solution, ultrasonic extraction is obtained by filtration three with solid-liquid ratio 1g:40-50mL
Secondary extract and three times filter residue；
(2) by step (1) preparation an extract, second extract, extract is mixed to form peach leaf extract three times, rotation
It is concentrated by evaporation, cellulose whiskers is added, stirring adds Chitosan-coated and forms finishing agent；
(3) fluffy cotton fiber is impregnated into the finishing agent of step (2) preparation, constant temperature oscillation takes out, and washes, drying, with colour
The removing miliaria and relieving itching mosquito repellent cotton fabric of cotton fiber woven formation cherry apple leaf extract.
2. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (1), the partial size of peach leaf powder is 1-20 μm.
3. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (1), one time extract is flavonoids and naringenin, and second extract is quininic acid, three times extract
For lycopene.
4. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (1), the volume ratio of ethanol water is 1:0.5-0.8.
5. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (2), the mass fraction of peach leaf extract is 15-30%.
6. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (2), the mass ratio of peach leaf extract, cellulose whiskers and chitosan is 1:1.2-1.5:0.5-2.
7. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (3), the temperature of constant temperature oscillation is 60-70 DEG C, time 20-30min.
8. a kind of preparation method of the removing miliaria and relieving itching mosquito repellent cotton fabric of cherry apple leaf extract according to claim 1, special
Sign is: in the step (3), the bath raio of dipping is 1:30-50.
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| CN107653674A (en) * | 2017-11-13 | 2018-02-02 | 湖州佳伟纺织品有限公司 | Textile antimosquito finishing agent and preparation method thereof |
| CN111150688A (en) * | 2020-01-10 | 2020-05-15 | 广州贝玛生物科技有限公司 | Mosquito-repellent prickly heat-removing spray and preparation method thereof |
| CN111218821B (en) * | 2020-02-28 | 2022-03-11 | 南通大学 | Preparation method of cotton fabric with mosquito repelling function |
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| CN101021023A (en) * | 2007-03-20 | 2007-08-22 | 浙江华孚色纺有限公司 | Mosquito preventing fiber dyed yarn and its production process |
| CN102008572B (en) * | 2010-10-28 | 2012-05-09 | 陕西科技大学 | Method for preparing effective ingredient extracts of peach leaves |
| IT1403145B1 (en) * | 2010-11-22 | 2013-10-04 | Elia | USE OF AN ANTIZANZAR COMPOSITION AS A WASHING ADDITIVE TO PROVIDE AN ANTIZANZAR PROPERTIES TO A FABRIC. |
| CN102154841B (en) * | 2011-01-13 | 2012-09-12 | 福建众和股份有限公司 | Anti-mosquito finishing process of textile fabric |
| CN104480724A (en) * | 2014-12-05 | 2015-04-01 | 南通大学 | Functional natural plant mosquito repelling ecological home textile product |
| CN105926114A (en) * | 2016-06-16 | 2016-09-07 | 东莞市联洲知识产权运营管理有限公司 | Long-acting mosquito-repellent thermal-moisture comfortable hemp fabric and preparation method thereof |
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Effective date of registration: 20190605 Address after: 515100 Small Western Ocean in Simapu Town, Chaonan District, Shantou City, Guangdong Province Applicant after: Shantou Dola Garment Industry Co., Ltd. Address before: 523000 productivity building 406, high tech Industrial Development Zone, Songshan Lake, Dongguan, Guangdong Applicant before: Dongguan Lianzhou Intellectual Property Operation Management Co.,Ltd. |
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