CN106468016A - A kind of removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract and preparation method thereof - Google Patents
A kind of removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract and preparation method thereof Download PDFInfo
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- CN106468016A CN106468016A CN201610838924.8A CN201610838924A CN106468016A CN 106468016 A CN106468016 A CN 106468016A CN 201610838924 A CN201610838924 A CN 201610838924A CN 106468016 A CN106468016 A CN 106468016A
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- extract
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/02—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons
- D06M13/03—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with hydrocarbons with unsaturated hydrocarbons, e.g. alkenes, or alkynes
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/11—Compounds containing epoxy groups or precursors thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Abstract
The present invention provides a kind of preparation method of the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract, comprises the following steps：Fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form Folium Persicae powder, stand-by, by Folium Persicae powder, respectively in immersion ethanol water, in methanol solution and petroleum ether solution, extract respectively and be filtrated to get extract, second extract and three extracts；Extract, second extract, three extracts are mixed to form Folium Persicae extract, rotary evaporation concentrates, add cellulose whiskers and Chitosan-coated to form finishing agent；Fluffy cotton fiber is impregnated in finishing agent, constant temperature oscillation, takes out, washing, dry, weave with colorful cotton fibre and form fabric.The comfortable moisture absorption of fabric of present invention preparation is breathed freely, and also has functions that removing miliaria and relieving itching anophelifuge.
Description
Technical field
The invention belongs to textile material technical field is and in particular to a kind of removing miliaria and relieving itching anophelifuge cotton of cherry apple leaf extract is knitted
Thing and preparation method thereof.
Background technology
Miliaria, also known as antiperspirant spore rash, is because perspiration is discharged freely, is stranded in Intradermal, the sudoriferous duct leading to skin is by skin
Cutin and dead cell blocking when, the perspiration in sweat gland can be risen brokenly, lead to sudoriferous duct wall flow into around block, cause
Inflammation around sweat gland.Because summer high temperature is hot, the skin of baby or child is tender, and sweat gland is undeveloped, easily produces miliaria,
And miliaria scratchy, burning sensation again, easily make baby or child's dysphoria, therefore, be suitable for the product of the miliaria of dispelling of baby or child
Product are particularly important.
Miliaria product of dispelling on the market mostly is liniment, ointment and emulsifiable paste at present, but the spy for baby or the tender and lovely skin of child
Different property, needs to select pure natural, stimulates and have the composition of potential risk without having to infant, also need in addition meet middle national treasure
Precious skin is with system it is impossible to select excessively refrigerant product.One kind disclosed in Chinese patent CN 102860967A has miliaria of dispelling
The baby skin protection product formula of antipruritic function, contains Flos Lonicerae, lavandula angustifolia, Folium Artemisiae Argyi, Radix Sophorae Flavescentiss, Borneolum Syntheticum, Herba Menthae in this skin care item formula
The natural plants such as brain, Camphora, Jojoba oil, macadimia nut oil, Mel, shea butter, licorice root extract, oat beta-glucan become
Point.A kind of baby's skin smoothing removing miliaria and relieving itching condensation and preparation method thereof disclosed in Chinese patent CN 103720617B, this product is main
Including deionized water, Carbomer, triethanolamine, antipruritic and antipruritic agent, baby's liquid distilled from honeysuckle flowers or lotus leaves stock solution, Semen phaseoli radiati activity stock solution, preservative, second
Alcohol, essence and solubilizing agent.From above-mentioned prior art, miliaria plant extract of dispelling is as major function material and other auxiliary agent phases
In conjunction with the product preparing watery, emulsus and paste, but the composition of these products be not all all-natural product, Er Qienan
Long-term protection is carried out with the skin to baby or child.
Folium Persicae belongs to the medical material of early stage, contains sugar two, naringenin, quininic acid, lycopene, almond Folic Acid phthalein in Folium Persicae
Amine, cyanogen glycosides etc., can extracting through different reagent, Main Function is diaphoresis expectorant, and disappear wet parasite killing, the effects such as control wind syndrome of head, Fructus Persicae
Leaf external or for oral administration there is heat-clearing and toxic substances removing, effect of killing parasites for relieving itching.Product based on Folium Persicae also has multiple, such as Folium Persicae medicine at present
Toothpaste, Folium Persicae is dispelled miliaria water, Folium Persicae suppository etc., but also rare for application in terms of weaving for the Folium Persicae.
Present invention miliaria plant extract of dispelling is combined with bafta, providing cotton fabric removing miliaria and relieving itching function of driving mosquitoes, and
Do not affect the soft, ventilative of bafta and moisture pick-up propertiess, the skin of baby or child can be prevented and treated for a long time.
Content of the invention
The technical problem to be solved in the present invention is to provide a kind of removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract, function
Material is Folium Persicae extract, fully extracts the effective ingredient in Folium Persicae by ethanol, methanol and petroleum ether as extracting solution, will have
The inside of effect composition attachment and fibrous crystal palpus and surface, then form stabilised finish agent with Chitosan-coated, refill in raising
In cotton fiber, weave with colorful cotton fibre and form fabric.The present invention makes full use of the effective ingredient in Folium Persicae, and material used is all
Pure natural substance, no potential danger composition non-stimulated to baby or child skin, there is environmental protection safety, removing miliaria and relieving itching is driven
Effect of mosquito, can carry out permanent protection and prevent multiple dermatosis to the skin of baby or child.
For solving above-mentioned technical problem, the technical scheme is that：
A kind of removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract, the removing miliaria and relieving itching anophelifuge cotton of described cherry apple leaf extract
Fabric includes bafta and finishing agent, and described finishing agent includes Folium Persicae extract, cellulose whiskers and shitosan, and described cotton is knitted
Thing includes fluffy cotton fiber and colorful cotton fibre.
Preferred as technique scheme, described Folium Persicae extract includes lycopene, naringenin, flavonoid and tannin
Class, described fluffy cotton fiber is the cotton fiber of surface nappy.
The present invention also provides a kind of preparation method of the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract, walks including following
Suddenly：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form Folium Persicae powder, stand-by, by Fructus Persicae
Leaf powder, with solid-liquid ratio 1g:30-40ml, stands in immersion ethanol water, heating extraction, be filtrated to get extract and
Filtering residue, by a filtering residue, with solid-liquid ratio 1g:40-50ml, in immersion methanol solution, heating extraction, it is filtrated to get secondary carrying
Take thing and secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:40-50ml, in immersion petroleum ether solution, supersound extraction, filters
To three extracts and three filtering residues；
(2) an extract second extract preparing step (1), three extracts are mixed to form Folium Persicae extract,
Rotary evaporation concentrates, and adds cellulose whiskers, stirring, adds Chitosan-coated and forms finishing agent；
(3) fluffy cotton fiber is impregnated in finishing agent prepared by step (2), constant temperature oscillation, takes out, washing, dry, with
Colorful cotton fibre weaving forms the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract.
Preferred as technique scheme, in described step (1), the particle diameter of Folium Persicae powder is 1-20 μm.
Preferred as technique scheme, in described step (1), an extract is flavonoid and naringenin, secondary
Extract is quininic acid, and three extracts are lycopene.
Preferred as technique scheme, in described step (1), the volume ratio of ethanol water is 1:0.5-0.8.
Preferred as technique scheme, in described step (2), the mass fraction of Folium Persicae extract is 15-30%.
Preferred as technique scheme, in described step (2), Folium Persicae extract, cellulose whiskers and shitosan
Mass ratio is 1:1.2-1.5:0.5-2.
Preferred as technique scheme, in described step (3), the temperature of constant temperature oscillation is 60-70 DEG C, and the time is
20-30min.
Preferred as technique scheme, in described step (3), the bath raio of dipping is 1:30-50.
Compared with prior art, the invention has the advantages that：
(1) in the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract of present invention preparation, functional material extracts for Folium Persicae
Thing, fully extracts the effective ingredient in Folium Persicae by ethanol, methanol and petroleum ether as extracting solution, such as flavone compound, Fructus Citri grandiss
Pi Su, thujic acid class and lycopene, flavone compound and naringenin all have very strong antioxidation, can eliminate oxygen freely
, moreover it is possible to safeguard metabolic balance, thujic acid class can have very strong disease-resistant with the protein interaction of skin surface for base and antiinflammatory
Cytotoxic activity, lycopene can improve the immunity of body, and multiple dermatosis are played with the effect of prevention, and the present invention also added fibre
The plain whisker of dimension and shitosan, plurality of active ingredients are attached to inside and the surface of fibrous crystal palpus, then are formed with Chitosan-coated
Stabilised finish agent, improves the action time of Folium Persicae effective ingredient, lowers the loss of effective ingredient, enables effective ingredient uniformly lasting
The surface acting on skin, play the purpose of removing miliaria and relieving itching anophelifuge.
(2) containing fluffy cotton fiber in the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract of present invention preparation, fluffy
The cotton fiber of pine is the cotton fiber of surface nappy, and the filling of Folium Persicae finishing agent can be entered by the fine hair on cotton fiber surface, is formed steady
Fixed environment, it is to avoid fabric in use, because the factor of friction, washing and wrinkle causes the excessive loss of effective ingredient,
Reduce the stress degree of effective ingredient, improve the utilization rate of effective ingredient.Then weave with colorful cotton fibre and form fabric, not shadow
Ring the performances such as the feel of fabric, ventilative, moisture-inhibiting.
(3) present invention preparation the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract in make full use of effective in Folium Persicae
Composition, material used is all pure natural substance, non-stimulated to baby or child skin, no potential danger composition, has green ring
Ensure safety, effect of removing miliaria and relieving itching anophelifuge, the skin of baby or child can be carried out with permanent protection and prevent multiple skins
Disease.
Specific embodiment
To describe the present invention, the illustrative examples of the here present invention and explanation below in conjunction with specific embodiment in detail
It is used for explaining the present invention, but not as a limitation of the invention.
Embodiment 1：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:30ml, immersion volume ratio is 1:6h is stood in 0.5 ethanol water,
Heating extraction 2h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, to expect
Liquor ratio 1g:40ml, in immersion methanol solution, heating extraction 3h at 50 DEG C, it is filtrated to get the second extract and two of quininic acid
Secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:40ml, in immersion petroleum ether solution, supersound extraction 30min under 200W power,
It is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
15% Folium Persicae extract, will add 1.2 parts of cellulose whiskers, stirs 30min, add 0.5 in 1 part of Folium Persicae extract
The Chitosan-coated of part, is sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:30, it is impregnated in finishing agent, at 60 DEG C, constant temperature oscillation 20min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 2：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:40ml, immersion volume ratio is 1:10h is stood in 0.8 ethanol water,
Heating extraction 3h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, with
Solid-liquid ratio 1g:50ml, immersion methanol solution in, heating extraction 4h at 50 DEG C, be filtrated to get quininic acid second extract and
Secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:50ml, in immersion petroleum ether solution, supersound extraction under 500W power
60min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
30% Folium Persicae extract, will add 1.5 cellulose whiskers, stirs 60min, add 2 parts in 1 part of Folium Persicae extract
Chitosan-coated, is sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:50, it is impregnated in finishing agent, at 70 DEG C, constant temperature oscillation 30min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 3：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:35ml, immersion volume ratio is 1:8h is stood in 0.6 ethanol water,
Heating extraction 2.5h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, with
Solid-liquid ratio 1g:45ml, in immersion methanol solution, heating extraction 3.5h at 50 DEG C, it is filtrated to get the second extract of quininic acid
With secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:45ml, in immersion petroleum ether solution, supersound extraction under 300W power
50min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
25% Folium Persicae extract, will add 1.3 cellulose whiskers, stirs 40min, add 1.5 parts in 1 part of Folium Persicae extract
Chitosan-coated, be sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:45, it is impregnated in finishing agent, at 65 DEG C, constant temperature oscillation 25min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 4：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:30ml, immersion volume ratio is 1:6- is stood in 0.8 ethanol water
10h, heating extraction 2h at 60 DEG C, it is filtrated to get an extract of flavonoid and naringenin and a filtering residue, will once filter
Slag, with solid-liquid ratio 1g:50ml, in immersion methanol solution, heating extraction 3h at 50 DEG C, it is filtrated to get the second extraction of quininic acid
Thing and secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:50ml, in immersion petroleum ether solution, supersound extraction under 200W power
60min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
30% Folium Persicae extract, will add 1.2 cellulose whiskers, stirs 40min, add 1.5 parts in 1 part of Folium Persicae extract
Chitosan-coated, be sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:45, it is impregnated in finishing agent, at 60 DEG C, constant temperature oscillation 20min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 5：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:35ml, immersion volume ratio is 1:8h is stood in 0.6 ethanol water,
Heating extraction 2.5h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, with
Solid-liquid ratio 1g:50ml, in immersion methanol solution, heating extraction 3.5h at 50 DEG C, it is filtrated to get the second extract of quininic acid
With secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:50ml, in immersion petroleum ether solution, supersound extraction under 400W power
50min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
25% Folium Persicae extract, will add 1.4 cellulose whiskers, stirs 50min, add 1.5 parts in 1 part of Folium Persicae extract
Chitosan-coated, be sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:45, it is impregnated in finishing agent, at 65 DEG C, constant temperature oscillation 20min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 6：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:40ml, immersion volume ratio is 1:6h is stood in 0.6 ethanol water,
Heating extraction 3h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, to expect
Liquor ratio 1g:50ml, immersion methanol solution in, heating extraction 3.5h at 50 DEG C, be filtrated to get quininic acid second extract and
Secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:45ml, in immersion petroleum ether solution, supersound extraction under 450W power
60min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
23% Folium Persicae extract, will add 1.3 cellulose whiskers, stirs 50min, add 1 part in 1 part of Folium Persicae extract
Chitosan-coated, is sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:40, it is impregnated in finishing agent, at 70 DEG C, constant temperature oscillation 30min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 7：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:40ml, immersion volume ratio is 1:8h is stood in 0.8 ethanol water,
Heating extraction 3h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, to expect
Liquor ratio 1g:40ml, in immersion methanol solution, heating extraction 4h at 50 DEG C, it is filtrated to get the second extract and two of quininic acid
Secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:40ml, in immersion petroleum ether solution, supersound extraction 60min under 350W power,
It is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forming mass fraction is
20% Folium Persicae extract, will add 1.4 cellulose whiskers, stirs 50min, add 1 part in 1 part of Folium Persicae extract
Chitosan-coated, is sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:40, it is impregnated in finishing agent, at 65 DEG C, constant temperature oscillation 25min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
Embodiment 8：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form the Folium Persicae that particle diameter is 1-20 μm
Powder, stand-by, by Folium Persicae powder, with solid-liquid ratio 1g:30ml, immersion volume ratio is 1:10h is stood in 0.7 ethanol water,
Heating extraction 3h at 60 DEG C, is filtrated to get an extract of flavonoid and naringenin and a filtering residue, by a filtering residue, with
Solid-liquid ratio 1g:50ml, in immersion methanol solution, heating extraction 3.5h at 50 DEG C, it is filtrated to get the second extract of quininic acid
With secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:50ml, in immersion petroleum ether solution, supersound extraction under 450W power
40min, is filtrated to get three extracts of lycopene and three filtering residues.
(2) by extract, second extract, three extract mixing, rotary evaporation concentrates, and forms mass fraction
25% Folium Persicae extract, will add 1.5 cellulose whiskers, stirs 50min, add 1 part in 1 part of Folium Persicae extract
Chitosan-coated, is sufficiently stirred for forming homogeneous finishing agent.
(3) by fluffy cotton fiber, with bath raio for 1:50, it is impregnated in finishing agent, at 70 DEG C, constant temperature oscillation 20min, takes
Go out, washing, dry, weave, with colorful cotton fibre, the removing miliaria and relieving itching anophelifuge bafta forming cherry apple leaf extract.
After testing, embodiment 1-8 preparation the antibacterial of removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract, antioxidation,
Anophelifuge, ventilative, moisture-inhibiting result are as follows：
As seen from the above table, the breathable moisture permeability of the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract of present invention preparation
Change is little, but antibacterial, antioxidation and repelling effect are good.
Above-described embodiment only principle of the illustrative present invention and its effect, not for the restriction present invention.Any ripe
The personage knowing this technology all can carry out modifications and changes without prejudice under the spirit and the scope of the present invention to above-described embodiment.Cause
This, those of ordinary skill in the art is complete with institute under technological thought without departing from disclosed spirit such as
All equivalent modifications becoming or change, must be covered by the claim of the present invention.
Claims (10)
1. a kind of cherry apple leaf extract removing miliaria and relieving itching anophelifuge bafta it is characterised in that：The miliaria of dispelling of described cherry apple leaf extract
Antipruritic anophelifuge bafta includes bafta and finishing agent, and described finishing agent includes Folium Persicae extract, cellulose whiskers and shell and gathers
Sugar, described bafta includes fluffy cotton fiber and colorful cotton fibre.
2. a kind of cherry apple leaf extract according to claim 1 removing miliaria and relieving itching anophelifuge bafta it is characterised in that：Described
Folium Persicae extract includes lycopene, naringenin, flavonoid and tanninses, and described fluffy cotton fiber is that the cotton of surface nappy is fine
Dimension.
3. a kind of preparation method of the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract is it is characterised in that comprise the following steps：
(1) fresh Radix Fici Hirtae leaf is cleaned, vapor sterilant, dry in the shade, pulverize, sieve, form Folium Persicae powder, stand-by, by Folium Persicae powder
End, with solid-liquid ratio 1g:30-40ml, stands in immersion ethanol water, heating extraction, is filtrated to get an extract and once
Filtering residue, by a filtering residue, with solid-liquid ratio 1g:40-50ml, in immersion methanol solution, heating extraction, it is filtrated to get second extract
With secondary filtering residue, by secondary filtering residue, with solid-liquid ratio 1g:40-50ml, in immersion petroleum ether solution, supersound extraction, it is filtrated to get three
Secondary extract and three filtering residues；
(2) an extract second extract preparing step (1), three extracts are mixed to form Folium Persicae extract, rotation
Evaporation and concentration, adds cellulose whiskers, stirring, adds Chitosan-coated and forms finishing agent；
(3) fluffy cotton fiber is impregnated in finishing agent prepared by step (2), constant temperature oscillation, takes out, washing, dry, with colour
Cotton fiber woven forms the removing miliaria and relieving itching anophelifuge bafta of cherry apple leaf extract.
4. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (1), the particle diameter of Folium Persicae powder is 1-20 μm.
5. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (1), an extract is flavonoid and naringenin, and second extract is quininic acid, three extracts
For lycopene.
6. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (1), the volume ratio of ethanol water is 1:0.5-0.8.
7. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (2), the mass fraction of Folium Persicae extract is 15-30%.
8. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (2), the mass ratio of Folium Persicae extract, cellulose whiskers and shitosan is 1:1.2-1.5:0.5-2.
9. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (3), the temperature of constant temperature oscillation is 60-70 DEG C, and the time is 20-30min.
10. the preparation method of the removing miliaria and relieving itching anophelifuge bafta of a kind of cherry apple leaf extract according to claim 3, it is special
Levy and be：In described step (3), the bath raio of dipping is 1:30-50.
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| CN111218821A (en) * | 2020-02-28 | 2020-06-02 | 南通大学 | Preparation method of cotton fabric with mosquito repelling function |
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