CN104523530A - Anti-aging facial mask and preparation method thereof - Google Patents

Anti-aging facial mask and preparation method thereof Download PDF

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Publication number
CN104523530A
CN104523530A CN201510011382.2A CN201510011382A CN104523530A CN 104523530 A CN104523530 A CN 104523530A CN 201510011382 A CN201510011382 A CN 201510011382A CN 104523530 A CN104523530 A CN 104523530A
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water
subsequent use
phase component
oil
plant
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陈勇
张鹏
黄卉芬
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HUNAN XINJINHAO TEA OIL Co Ltd
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HUNAN XINJINHAO TEA OIL Co Ltd
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Abstract

The invention discloses an anti-aging facial mask and a preparation method of the anti-aging facial mask and relates to the technical field of cosmetic processing in the daily-use chemical industry. The anti-aging facial mask is prepared from the following raw materials of oil phase components, aqueous phase components, functional components, assistant agents and deionized water, wherein the oil phase components comprise cetanol, tea oil, stearic acid, vitamin E, caprylic/capric triglyceride and carbomer; the aqueous phase components comprise 1,3-butanediol, glycerol, plant extract, tea seed polysaccharide hydrolysate and triethanolamine; the functional components comprise tea polyphenol, collagen and hyaluronic acid; the assistant agents comprise carboxymethylcellulose, methylparaben and Kathon. The preparation process includes the following steps of A, material preparation, B, oil phase component mixture, C, aqueous phase component mixture, D, mixture of the oil phase components and the aqueous phase components, E, addition of the functional components, and F, addition of the assistant agents. The anti-aging facial mask has the good moisturizing and moistening effects and the anti-aging effect and suitable for being used by people with skin of different types and people at different ages.

Description

A kind of anti-ageing face mask and preparation method thereof
Technical field
The present invention relates to the cosmetics processing technique field in daily-use chemical industry, particularly a kind of anti-ageing face mask and preparation method thereof.
Technical background
Facial film is a kind of skin care item containing maintenance composition, and its using method is mainly covered in face, by the contact of a period of time, improves skin.The type of facial film has various ways such as peeling off facial film, powder face pack, cream pack and molding facial film, and according to the difference of its composition, effect is different.People are along with growth in the living standard, more and more higher to the both effectiveness requirement of facial film.At present, the facial film of commercial type, various in style, but effective aging ingredient in most products is too low, or use the composition of easy sensitization, on the contrary skin nursing is had a negative impact.As Chinese patent (number of patent application 201110087520.7) disclosed " a kind of anti-ageing face mask ", the raw material of this facial film comprises the component of following quality proportioning: 25 grams, Flos Carthami, Radix Angelicae Sinensis 25 grams, Radix Salviae Miltiorrhizae 25 grams, Herba Leonuri 25 grams, Margarita powder 25 grams, Catergen 5 grams of dough-making powder 150 grams, and the degree of accuracy of this constituent mass proportioning is ± 5 grams; Flos Carthami, Radix Angelicae Sinensis, Radix Salviae Miltiorrhizae, Herba Leonuri, Margarita powder and vitamin C are worn into 100 to 200 object powderies, then add flour mix well in the ratio of 1: 1, be in harmonious proportion with water, the consumption of water is to be as the criterion mentioned component furnishing pasty state; This facial film can whitening skin and preserving moisture, nourishes rough skin, desalination microgroove, defying age, Be very effective.And for example Chinese patent (number of patent application 201310462009.X) disclosed " a kind of anti aging effect facial film and preparation method thereof ", its formula is: Aloe 50 ~ 100 parts, 30 ~ 70 parts, Semen Armeniacae Amarum, Cortex Mori 20 ~ 50 parts, 30 ~ 70 parts, Folium olive, green tea 20 ~ 50 parts, Radix Et Rhizoma Nardostachyos 15 ~ 25 parts, 10 ~ 20 parts, Radix Glycyrrhizae; Its preparation method is: 1) squeeze Aloe seminal fluid; 2) take other raw material in formula by weight, decoct with water, filter, after adsorption bleaching, filtrate is adjusted to concentration is 0.5 ~ 1.5g medical material/mL, obtained Chinese medicine extraction liquid; 3) by Aloe seminal fluid and Chinese medicine extraction liquid mixing, obtained mixed liquor, carrying 100mL mixed liquor by often opening facial film, evenly applying on face mask substrate material according to a conventional method; This this anti aging effect facial film is from multi-level, many-sided solution skin aging, supplementary skin-nourishing problem of substance.
Technology contents
The object of the present invention is to provide a kind of existing good moisturizing, moisturizing effect, there is again the facial-care product of senile-resistant efficacy; And its preparation method is provided.
For realizing its object, the technical solution used in the present invention is a kind of anti-ageing face mask of invention, is be prepared from by following raw material by weight:
(i), oil-phase component:
Hexadecanol 1-10 Oleum Camelliae 1-10 stearic acid 0.1-0.5 vitamin E 0.5-2
Caprylic/capric triglyceride 1-2 carbomer 0.2-0.5;
(ii), water-phase component:
1,3 butylene glycol 5-10 glycerol 5-15 plant extraction liquid 10-20
Camellia Oleifera polysaccharide hydrolyzed solution 1-10 triethanolamine 0.2-0.6;
(iii), functional component:
Tea polyphenols 0.1-0.5 collagen protein 1-3 hyaluronic acid 1-5;
(iv), adjuvant:
Carboxymethyl cellulose 1-5 methyl hydroxybenzoate 0.1-0.2 Kazon 0.1-0.2;
(v), surplus is deionized water, adds up to 100 parts;
Described plant extraction liquid is by one or more mixed extraction in following plant, and when for time two or more, the weight proportion between each plant is equal portions or other ratio:
Herba Rosmarini Officinalis 1-10 Herba Saxifragae 10-15 Radix Salviae Miltiorrhizae 5-20 Camellia Leaves 10-50
Shell of Camelliaoleifera Abel 1-40 Fructus Litseae pungentis 1-20 green tea 10-20 Qiyang Herba Asari 1-10.
Described plant extraction liquid can extract with adopting conventional method, following methods also can be adopted to prepare: choose clean, free of contamination plant material, by rinsed with deionized water 2-3 time, dry to moisture lower than 10% at 30-45 DEG C again, then pulverize, cross 80-120 mesh sieve, obtain plant powder; Add in plant powder again account for plant powder weight 4-6 doubly, volumetric concentration is the ethanol of 40-60%, at 70-90 DEG C, filter after water-bath reflux, extract, 5-6h, add in filtering residue again account for plant powder weight 2-3 doubly, volumetric concentration is the ethanol of 40-60%, at 70-90 DEG C, filter after water-bath reflux, extract, 1-3h, merge twice filtrate, be evaporated to the half of original volume again, obtain plant extraction liquid, under being stored in aseptic condition.
Described Camellia Oleifera polysaccharide hydrolyzed solution can with the product adopting commercial type, also following methods can be adopted to prepare: pulverized by the tea dregs of rice, cross 50-70 mesh sieve, then, deionized water is added according to the solid-liquid ratio of 1:10-15,3-5h is extracted under 60-80 DEG C of condition, more centrifugal with the rotating speed of 3000-5000r/min, get supernatant, be concentrated into the 1/6-1/4 of original volume, add the dehydrated alcohol precipitate polysaccharides with concentrated solution equal volume again, then with 3000-5000r/min centrifugalize, obtain Camellia Oleifera polysaccharide crude product; Again Camellia Oleifera polysaccharide crude product is removed protein, hydrogen peroxide for decoloration and acid hydrolysis through Savage method, obtain Camellia Oleifera polysaccharide hydrolyzed solution.
Above-mentioned anti-ageing face mask, the method directly mixed by all raw materials can be adopted to prepare, also can adopt following methods to prepare, its preparation process is as follows:
A, to get the raw materials ready: by above-mentioned weight proportion, take each raw material, for subsequent use;
B, oil-phase component mix: mixed by oil phase raw material for subsequent use, then, dissolve, obtain oil-phase component in the water-bath of 80-90 DEG C, for subsequent use;
C, water-phase component mix: mixed by Aqueous Phase Raw Material for subsequent use, obtain water-phase component, for subsequent use;
D, profit mix mutually: by for subsequent use, dissolve after oil-phase component add in water-phase component rapidly while hot, and to stir rapidly, and 10-20min at remaining on 40-60 DEG C; Then, under rotating speed 400-800r/min condition, emulsifying 5-10min; Adjusting rotary speed is to 100-200r/min again, stirs and is cooled to 30-40 DEG C, obtain oil mixing with water material, for subsequent use;
E, functional component are added: functional component for subsequent use joined in oil mixing with water material, under rotating speed 100-200r/min condition, stir, obtain fuel, for subsequent use;
F, adjuvant add: by carboxymethyl cellulose deionized water dissolving for subsequent use, then, be mixed together with methyl hydroxybenzoate and Kazon, join again in fuel, under rotating speed 100-200r/min condition, stir 10-20min, after being cooled to room temperature, obtain anti-ageing face mask.
This anti-ageing face mask is the mask product with cream frost or emulsion appearance characteristic, meets the regulation of QB/T2872-2007.
Anti-ageing face mask of the present invention, the main raw material(s) adopted comprises:
A, hexadecanol: mainly for the manufacture of spice, cosmetics, detergent, plasticizer etc., be the substrate in all kinds of cosmetics, in the present invention as lubricant and surfactant;
B, Oleum Camelliae: the liquid of pale yellow transparent, it is the oils and fats being squeezed gained by the kernel of oil tea section plant oil tea (Camellia oleifera Abel), containing the unsaturated fatty acid of more than 85%, be the effective ingredient in the present invention, use as softening agent;
C, glycerol: i.e. glycerol, be used as wetting agent in the present invention;
D, 1,3 butylene glycol: have another name called 1,3-dihydroxy butane are the one of polyhydric alcohol, in the present invention as wetting agent and solvent;
E, stearic acid: be used as emulsifying agent in the present invention;
F, caprylic/capric triglyceride: be easy to be absorbed by the skin, play good effect to the uniform and smooth of cosmetics, makes skin lubrication glossy; In the present invention as the base material of Moisture factor, also double as stabilizing agent, antifreezing agent, homogeneous agent;
G, vitamin E: be a kind of important antioxidant, promoting skin healing and reduce cicatrization, is one of antidotal effective ingredient in the present invention;
H, carbomer: carbomer is the copolymer of poly-alkyl sucrose or poly-alkyl tetramethylolmethane and acrylic crosslinking polymer, in cosmetics as stabilising emulsifier and gel;
I, Camellia Oleifera polysaccharide hydrolyzed solution: be a kind of polysaccharose substance extracted from the tea dregs of rice, have scavenging free radicals, antioxidative effect;
J, tea polyphenols: have very strong non-oxidizability and physiologically active are the scavengers of human free radical, have blocking-up lipid peroxidation, the effect of scavenging capacity enzyme, are one of antidotal effective ingredient in the present invention;
K, collagen protein: be a kind of effective cosmetic material, can Glycerin, gives it and smoothly feels;
L, hyaluronic acid: be the best material of the occurring in nature moisture retention that finds at present, be called as desirable nature moisturizing factor; It can improve skin-nourishing metabolism, and make that skin is tender, smooth, wrinkle removing, increase elasticity, prevent aging, be again good Percutaneous absorption enhancer while moisturizing;
M, carboxymethyl cellulose: be used as thickening agent and emulsifying agent in the present invention;
N, Kazon: be called for short isothiazolone, soluble in water and low-carbon alcohols, best use pH value 4-8, toxicity is low, has the advantage that antibacterial action is in extensive range and antibacterial effect is strong, better with the use of effect with methyl hydroxybenzoate;
O, methyl hydroxybenzoate: have another name called methyl parahydroxybenzoate, be white crystalline powder or colourless crystallization, be soluble in alcohol, ether and acetone, have phenolic hydroxyl structure, antibacterium superior performance;
P, triethanolamine: regulate acid-base value, in the present invention as nertralizer.
Q, Herba Rosmarini Officinalis extracting solution: extract from Herba Rosmarini Officinalis (Rosmarinus officinalis), have the effect eliminating fat, Rosemary Extract and delaying senility.
R, Herba Saxifragae extracting solution: extract from Herba Saxifragae (Saxifraga stolonifera Curt.), micro-bitter, acrid, cold, dispel the wind, heat clearing away, removing pathogenic heat from blood and toxic substance from the body.
S, Radix Salviae Miltiorrhizae extract: extract from Radix Salviae Miltiorrhizae (Salvia miltiorrhiza Bunge.), there is promoting blood flow to regulate menstruation, stasis-dispelling and pain-killing, removing heat from blood eliminating carbuncle, clear away heart-fire the effect such as relieving restlessness, nourishing blood to tranquillize the mind.
T, Camellia Leaves extracting solution: extract from Camellia Leaves, have the effect such as astringing to arrest bleeding, removing toxic substances.
U, shell of Camelliaoleifera Abel extracting solution: extract from shell of Camelliaoleifera Abel, have antioxidative effect;
V, Fructus Litseae pungentis extracting solution: extract from Fructus Litseae pungentis (Litsea cubeba (Lour.) Pers.), there is spleen invigorating, dampness, regulating QI, help digestion, the effect such as pain relieving and removing toxic substances and promoting subsidence of swelling.
W, green tea extractive liquor: extract from green tea (greentea), green tea has blood fat reducing and antiobesity action, wherein contained tea polyphenols has very strong non-oxidizability and physiologically active, is the scavenger of human free radical.
X, Qiyang Herba Asari extracting solution: extract from Qiyang Herba Asari (Asarum magnificum Tsiang exC.Y.Cheng et C.S.Yang var.magnificum), have dry, effect of pleasant, pain relieving.
Anti-ageing face mask of the present invention, system adopts gentle moisture retention composition and adjuvant, add natural anti-oxidation composition tea polyphenols and various plants extracting solution, and the natural tea seed polysaccharide hydrolyzed solution extracted from the tea dregs of rice, moisture of skin can be supplemented rapidly while use, repair impaired skin, and there is the effect of slowing down skin aging speed.
Anti-ageing face mask of the present invention, every organoleptic indicator and sanitary index all meet the standard of QB/T2872-2007 facial film and " cosmetics health specification 2007 " after testing.
Following table 1 is sanitary index and the sense organ physical and chemical index of anti-ageing face mask of the present invention.
The sanitary index of table 1 anti-ageing face mask of the present invention and sense organ physical and chemical index
The aging of human body skin is a complexity and very long process, and to this researcher, opinions vary, and free-radical theory is one of them.Free radical has numerous species, and modal is active oxygen ion, comprises DPPH (DPPH.free radical), superoxide anion and hydroxy radical etc.And free radical scavenger can by blocking or reverse the Oxidation disturbing free radical.Therefore, for antidotal skin care item, the method measuring free radical scavenger scavenging capacity oxonium ion in tested material can be adopted to identify whether it has anti-aging effects.By the change of spectrophotography light absorption value after specific absorption wavelength place mensuration adds tested material, the clearance rate of tested material scavenging capacity oxonium ion can be drawn.
Under the wavelength 520nm condition measured, anti-ageing face mask of the present invention is 78.94% to the clearance rate of DPPH free radical; Under mensuration wavelength 325nm condition, anti-aging face cream is 69.61% to the clearance rate of superoxide anion; Under mensuration wavelength 584nm condition, anti-aging face cream is 56.08% to the clearance rate of hydroxy radical.It can thus be appreciated that anti-ageing face mask of the present invention, the free radical produced with skin during energy is effective, protection skin, possesses preferably anti-aging effects.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplified, but protection scope of the present invention is not limited thereto.
Below in conjunction with embodiment, the present invention is further illustrated.Explanation is below the mode exemplified, but protection scope of the present invention is not limited thereto.
Embodiment one:
The anti-ageing face mask of the present embodiment, be prepared from by oil-phase component, water-phase component, functional component and adjuvant and deionized water, each composition is made up of following raw material by weight:
Oil-phase component: hexadecanol 2 parts, Oleum Camelliae 2 parts, stearic acid 0.1 part, vitamin E 1.5 parts, caprylic/capric triglyceride 1 part, carbomer 0.2 part;
Water-phase component: 1,3 butylene glycol 6 parts, glycerol 10 parts, plant extraction liquid 15 parts, Camellia Oleifera polysaccharide hydrolyzed solution 5 parts, triethanolamine 0.3 part;
Functional component: tea polyphenols 0.2 part, collagen protein 1 part, hyaluronic acid 1.5 parts;
Adjuvant: carboxymethyl cellulose 2.5 parts, methyl hydroxybenzoate 0.1 part, Kazon 0.2 part;
Surplus is deionized water, adds up to 100 parts.
Plant extraction liquid wherein adopts following methods to extract:
Choose clean, free of contamination Herba Rosmarini Officinalis 5 parts, Herba Saxifragae 10 parts, Camellia Leaves 20 parts, Radix Salviae Miltiorrhizae 5 parts, shell of Camelliaoleifera Abel 20 parts, green tea 10 parts, Qiyang Herba Asari 5 parts, Fructus Litseae pungentis 15 parts by weight, by rinsed with deionized water 3 times, dry to moisture lower than 10% at 40 DEG C again, then pulverize, cross 100 mesh sieves, obtain plant powder; Add in plant powder again account for plant powder weight 5 times, volumetric concentration is the ethanol of 50%, at 80 DEG C, filter after water-bath reflux, extract, 4h, add to filtering residue again account for plant powder weight 2.5 times, volumetric concentration is the ethanol of 50%, at 80 DEG C, filter after water-bath reflux, extract, 2h, merge twice filtrate, be evaporated to the half of former concentrated solution volume again, obtain plant extraction liquid, under being stored in aseptic condition;
The preparation process of Camellia Oleifera polysaccharide hydrolyzed solution is wherein as follows:
The tea dregs of rice are pulverized, cross 60 mesh sieves, then, add deionized water according to the solid-liquid ratio of 1:12, under 60 DEG C of conditions, extract 4h, centrifugal at the rotating speed of 4000r/min again, get supernatant, be concentrated into 1/5 of original volume, then add and concentrated solution same volume dehydrated alcohol precipitate polysaccharides, again with 4000r/min centrifugalize, obtain Camellia Oleifera polysaccharide crude product; Again Camellia Oleifera polysaccharide crude product is removed protein, hydrogen peroxide for decoloration and acid hydrolysis through Savage method, obtain Camellia Oleifera polysaccharide hydrolyzed solution;
The preparation process of anti-ageing face mask is as follows:
A, to get the raw materials ready: by above-mentioned weight proportion, take each raw material, for subsequent use;
B, oil-phase component mix: mixed by oil phase raw material for subsequent use, then, dissolve, obtain oil-phase component in the water-bath of 85 DEG C, for subsequent use;
C, water-phase component mix: mixed by Aqueous Phase Raw Material for subsequent use, obtain water-phase component, for subsequent use;
D, profit mix mutually: by for subsequent use, dissolve after oil-phase component add in water-phase component rapidly while hot, and to stir rapidly, and 15min at remaining on 50 DEG C; Then, under rotating speed 600r/min condition, emulsifying 8min; Adjusting rotary speed is to 150r/min again, stirs and is cooled to 30 DEG C, obtain oil mixing with water material, for subsequent use;
E, functional component are added: functional component for subsequent use joined in oil mixing with water material, under rotating speed 150r/min condition, stir, obtain fuel, for subsequent use;
F, adjuvant add: by carboxymethyl cellulose deionized water dissolving for subsequent use, then, be mixed together with methyl hydroxybenzoate and Kazon, then join in fuel, stir 15min, after being cooled to room temperature, obtain anti-ageing face mask under rotating speed 150r/min condition.
The anti-ageing face mask of the present embodiment, is the mask product with cream frost or emulsion appearance characteristic, meets the regulation of QB/T 2872-2007.
Embodiment two:
The anti-ageing face mask of the present embodiment, be prepared from by oil-phase component, water-phase component, functional component and adjuvant and deionized water, each composition is made up of following raw material by weight:
Oil-phase component: hexadecanol 5 parts, Oleum Camelliae 5 parts, stearic acid 0.3 part, vitamin E 1 part, caprylic/capric triglyceride 1 part, carbomer 0.4 part;
Water-phase component: 1,3 butanediols 8 parts, glycerol 10 parts, plant extraction liquid 15 parts, camellia oleosa seed protein hydrolyzate 5 parts, triethanolamine 0.4 part;
Functional component: tea polyphenols 0.2 part, collagen protein 1.5 parts, hyaluronic acid 2 parts;
Adjuvant: carboxymethyl cellulose 3 parts, methyl hydroxybenzoate 0.2 part, Kazon 0.1 part;
Surplus is deionized water, and add up to 100 parts, other is identical with embodiment one.
Embodiment three:
The anti-ageing face mask of the present embodiment, be prepared from by oil-phase component, water-phase component, functional component and adjuvant four kinds of compositions, each composition is made up of following raw material by weight:
Oil-phase component: hexadecanol 9 parts, Oleum Camelliae 4 parts, stearic acid 0.1 part, vitamin E 2 parts, caprylic/capric triglyceride 1 part, carbomer 0.5 part;
Water-phase component: 1,3 butanediols 9 parts, glycerol 12 parts, plant extraction liquid 10 parts, camellia oleosa seed protein hydrolyzate 8 parts, triethanolamine 0.6 part;
Functional component: tea polyphenols 0.4 part, collagen protein 2 parts, hyaluronic acid 4 parts;
Adjuvant: carboxymethyl cellulose 3.5 parts, methyl hydroxybenzoate 0.2 part, Kazon 0.2 part;
Surplus is deionized water, and add up to 100 parts, other is identical with embodiment one.
Above-described embodiment is the present invention's preferably embodiment, but embodiments of the present invention are not restricted to the described embodiments.
Anti-ageing face mask of the present invention, its using method is: get appropriate facial film, and uniform application, after facial 15-20min, is cleaned with proper amount of clear water.
Anti-ageing face mask of the present invention, is suitable for crowd's use of different skin quality, all ages and classes.

Claims (4)

1. an anti-ageing face mask, it is characterized in that being prepared from by following raw material by weight:
(i), oil-phase component:
Hexadecanol 1-10 Oleum Camelliae 1-10 stearic acid 0.1-0.5 vitamin E 0.5-2
Caprylic/capric triglyceride 1-2 carbomer 0.2-0.5;
(ii), water-phase component:
1,3 butylene glycol 5-10 glycerol 5-15 plant extraction liquid 10-20
Camellia Oleifera polysaccharide hydrolyzed solution 1-10 triethanolamine 0.2-0.6;
(iii), functional component:
Tea polyphenols 0.1-0.5 collagen protein 1-3 hyaluronic acid 1-5;
(iv), adjuvant:
Carboxymethyl cellulose 1-5 methyl hydroxybenzoate 0.1-0.2 Kazon 0.1-0.2;
(v), surplus is deionized water, adds up to 100 parts;
Described plant extraction liquid is by one or more mixed extraction in following plant, and when for time two or more, the weight proportion between each plant is equal portions or other ratio:
2. anti-ageing face mask according to claim 1, it is characterized in that, the preparation method of described plant extraction liquid is: choose clean, free of contamination plant material, by rinsed with deionized water 2-3 time, dry to moisture lower than 10% at 30-45 DEG C again, then pulverize, cross 80-120 mesh sieve, obtain plant powder; Add in plant powder again account for plant powder weight 4-6 doubly, volumetric concentration is the ethanol of 40-60%, at 70-90 DEG C, filter after water-bath reflux, extract, 5-6h, again to filtering residue add account for plant powder weight 2-3 doubly, volumetric concentration is the ethanol of 40-60%, at 70-90 DEG C, filter after water-bath reflux, extract, 1-3h, merge twice filtrate, be evaporated to the half of original volume again, obtain plant extraction liquid, under being stored in aseptic condition.
3. anti-ageing face mask according to claim 1 and 2, is characterized in that, the preparation method of described Camellia Oleifera polysaccharide hydrolyzed solution is: pulverized by the tea dregs of rice, cross 50-70 mesh sieve, then, add deionized water according to the solid-liquid ratio of 1:10-15, under 60-80 DEG C of condition, extract 3-5h, centrifugal, get supernatant, be concentrated into the 1/6-1/4 of original volume, then add the dehydrated alcohol precipitate polysaccharides with concentrated solution equal volume, centrifugalize, obtains Camellia Oleifera polysaccharide crude product; Again Camellia Oleifera polysaccharide crude product is removed protein, decolouring and acid hydrolysis, obtain Camellia Oleifera polysaccharide hydrolyzed solution.
4. the preparation method of anti-ageing face mask according to any one of claim 1-3, is characterized in that preparation process is as follows:
A, to get the raw materials ready: by above-mentioned weight proportion, take each raw material, for subsequent use;
B, oil-phase component mix: mixed by oil phase raw material for subsequent use, then, dissolve, obtain oil-phase component in the water-bath of 80-90 DEG C, for subsequent use;
C, water-phase component mix: mixed by Aqueous Phase Raw Material for subsequent use, obtain water-phase component, for subsequent use;
D, profit mix mutually: by for subsequent use, dissolve after oil-phase component add in water-phase component rapidly while hot, and to stir rapidly, and 10-20min at remaining on 40-60 DEG C; Then, emulsifying 5-10min; Stir again and be cooled to 30-40 DEG C, obtain oil mixing with water material, for subsequent use;
E, functional component are added: functional component for subsequent use joined in oil mixing with water material, stir, obtain fuel, for subsequent use;
F, adjuvant add: by carboxymethyl cellulose deionized water dissolving for subsequent use, then, be mixed together with methyl hydroxybenzoate and Kazon, then join in fuel, stir 10-20min, after being cooled to room temperature, obtain anti-ageing face mask.
CN201510011382.2A 2015-01-09 2015-01-09 Anti-aging facial mask and preparation method thereof Pending CN104523530A (en)

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CN105055187B (en) * 2015-09-14 2018-02-09 广州赛莱拉干细胞科技股份有限公司 A kind of face rejuvenation cosmetic formulation and preparation method thereof
CN106038380A (en) * 2016-05-27 2016-10-26 江西联锴新材料有限公司 Complex enzyme tea bran mask powder and preparation method thereof
CN106038380B (en) * 2016-05-27 2020-09-08 江西联锴科技有限公司 Complex enzyme tea bran mask powder and preparation method thereof
CN109125111A (en) * 2018-09-30 2019-01-04 广州优刻生物科技有限公司 A kind of two-form Pure natural mask and preparation method thereof
WO2020252866A1 (en) * 2019-06-19 2020-12-24 杭州雅生生物科技有限公司 Glacial clay ecological skin cleansing and renewing mask and preparation method therefor

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Application publication date: 20150422