CN109505139A - A kind of warming warming fabric microcapsule dressing agent and its preparation method and application - Google Patents
A kind of warming warming fabric microcapsule dressing agent and its preparation method and application Download PDFInfo
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- CN109505139A CN109505139A CN201811475718.0A CN201811475718A CN109505139A CN 109505139 A CN109505139 A CN 109505139A CN 201811475718 A CN201811475718 A CN 201811475718A CN 109505139 A CN109505139 A CN 109505139A
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- Prior art keywords
- warming
- fabric
- temperature
- microcapsule dressing
- temperature sensing
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a kind of warming warming fabric microcapsule dressing agents and its preparation method and application.By selecting the wormwood essential oil with warm, health care and capsicum oil for composite core material, using high critical inversion temperature (UCST) be 25-30 DEG C temperature sensing material and natural polymer as wall material, a kind of warming warm, health care microcapsules have been obtained using complex coacervation.Core material in the microcapsules only can just be discharged when environment temperature is lower than UCST, and the lower rate of release of temperature is faster.Housekeeping liquid is made with super soft adhesive cooperation, by the way that the fabric with lasting warm, health care function can be obtained to one immersing and rolling of fabric.When taking in winter, fabric plays the role of Intelligent thermal-protection, creates good sleep environment.And fabric is not in the case where core material is revealed when high-temperature shaping and summer are stored, assurance function is organized in making full use of when taking.
Description
Technical field
The invention belongs to finishing functions of textile fabrics technical fields, and in particular to a kind of warming warming fabric microcapsule dressing agent
And its preparation method and application.
Background technique
With the increasing and the accelerating rhythm of life of operating pressure, people increasingly focus on the sleep quality of oneself, for
The functional requirement of winter bed necessaries is also higher and higher, and assigning the certain warm, health care function of fabric is a kind of side that consumer is favored
Formula.CN102605625A, which is disclosed, a kind of to be formed with capsaicine, nonionic surfactant, organic siliconresin, chitosan etc.
Heat sensitizer, heat sensitizer, which can be stablized, to be bonded on fabric and absorbs moisture and generate heat；CN108677539A is with camomile extract and peppery
Green pepper extract is heat preserving agent, and sodium hyaluronate and collagen are moisturizer, is kept the temperature using polyurethane as adhesive by infusion process
Moisturizing fabric；CN102628215A is with MoO3, medical stone nanometer is seperated, acrylic resin and dispersing agent are that raw material is stored always
The warming finishing agent of heat, the fabric temperature after arrangement can be improved 3 DEG C or so.But it is not provided with restriction in these above-mentioned methods
The means of functional mass release, in dyeing and finishing, take, easily cause unnecessary waste in storage process, function utilization rate is not high.
Heat-sensible high polymer is a kind of important intellectual material, can be responded to temperature change.According to critical inversion temperature
The characteristics of spending, thermo-sensitive material can be divided into high critical inversion temperature (UCST) and have minimum critical inversion temperature
(LCST) two major classes.UCST class macromolecule is Amphiphatic high polymer or polyampholyte mostly, due to its unique molecular structure,
Material structure and characteristic are controlled using variation of ambient temperature, currently, about UCST class temperature sensing material in fabric functional arrangement
Application also rarely have research.
Summary of the invention
The object of the present invention is to provide a kind of warming warming fabric microcapsule dressing agents and its preparation method and application, select
Have effects that the wormwood essential oil of warm, health care and capsicum oil is composite core material, with high critical inversion temperature (UCST) for 25-
30 DEG C of temperature sensing material and natural polymer is wall material, has obtained warming warm, health care microcapsule dressing agent using complex coacervation,
By an immersing and rolling, the fabric with lasting warm, health care function can be obtained.
A kind of warming warming fabric microcapsule dressing agent, raw material include: 1-5 parts of wormwood essential oil in parts by weight, chilli extract
It is 1-5 parts oily, 0.5-2 parts of temperature sensing material, 0.5-2 parts of natural macromolecular material, 0.1-0.5 parts of curing agent.
Preferred wormwood essential oil is 1-2 parts, and capsicum oil is 1-2 parts, and temperature sensing material is 0.5-1 parts, and natural polymer is
0.5-1 parts, curing agent is 0.1-0.2 parts.
Further, the mass ratio of wormwood essential oil and capsicum oil is 1:1-5, temperature sensing material and natural macromolecular material matter
Amount is 1-5:1.
The mass ratio of preferred wormwood essential oil and capsicum oil is 1:1-2, and temperature sensing material and natural polymer protonatomic mass are 1-
2:1, core wall ratio are 1-2:1.
Further, the temperature sensing material is the polyampholyte with sulfonate radical and ammonium root, isoelectric point 4.5-
5.5, high critical inversion temperature UCST are 25-30 DEG C.
Further, it is poly- to be selected from sodium alginate, Arabic gum, carboxymethyl cellulose or shell for the natural macromolecular material
Sugar.
Further, the curing agent is selected from formaldehyde, glutaraldehyde or glutamine transaminage.
The preparation method of above-mentioned warming warming fabric microcapsule dressing agent, comprising the following steps:
Step 1, it takes wormwood essential oil, capsicum oil, natural macromolecular material to add in water, in 60-80 DEG C of stirring 1-2h, obtains O/
W lotion；
Step 2, the pH to 4-4.5 of temperature sensing material is adjusted；
Step 3, the temperature sensing material of step 2 is added dropwise in O/W lotion, curing agent, 20-30 DEG C of solidification 6-8h is then added；
Step 4, mixed liquor step 3 obtained is stood, and is then filtered, washed drying, obtains finishing agent.
Application of the above-mentioned warming warming fabric microcapsule dressing agent in the warming arrangement of fabric.
Further, the application is specifically that fabric is placed in an immersing and rolling in working solution, liquid carrying rate 70-75%, 120-
160 DEG C of sizing 30-60s,
The working solution is the mixed liquor of finishing agent and super soft adhesive, and the concentration of finishing agent is 50-80wt.%, super soft adhesive
Concentration be 2-3wt.%.
Further, the super soft adhesive is acrylate adhesive or polyurethane binding.
Further, the fabric is cotton, wool, cashmere, kapok, lyocell, Modal or viscose etc..
The present invention selects the wormwood essential oil with warm, health care and capsicum oil is composite core material, is turned with high critical phase
The temperature sensing material and natural polymer that temperature (UCST) is 25-30 DEG C are wall material, have obtained a kind of warming using complex coacervation
Warm, health care microcapsules.Core material in the microcapsules only can just be discharged when environment temperature is lower than UCST, and temperature is lower
Rate of release is faster.
Meanwhile by the way that a certain amount of super soft adhesive is added in the working solution of preparation, an immersing and rolling, can be obtained has
The fabric of lasting warm, health care function.When taking in winter, fabric plays the role of Intelligent thermal-protection, creates good sleep environment.
And fabric is not in the case where core material is revealed when high-temperature shaping and summer are stored, assurance function is organized in abundant when taking
It utilizes.
The beneficial effects of the present invention are:
1, wormwood essential oil has rationale blood, warm meridians, and dispellieg cold and dampness promotees circulation, promotes immunity function.Capsicum oil can promote
Blood circulation enhances the metabolism of body, accelerates the combustion decomposition of fat, improves the effect of obesity.With wormwood essential oil
The fabric that carrying out reasonable proportion with capsicum oil obtains the present invention has effects that natural warm, health care.
2, the super soft adhesive that uses of the present invention is on fabric hand feel without influence, and microcapsules can be stablized and anchor at fabric table
Face.
3, it is that wall material prepares microcapsules that the present invention, which selects the temperature sensing material with high critical inversion temperature,.Obtained micro- glue
Capsule cyst wall density is affected by temperature, and when environment temperature is lower than UCST, cyst wall ruptures Release of core material, and temperature is lower, and cyst wall is empty
Gap is bigger, and Release of core material rate is faster.
4, the temperature sensing material UCST value that the present invention selects, for the fabric that arrangement obtains, enters between 25-30 DEG C when winter
When sleeping, the core material sustained release with natural warm, health care function builds rapidly a good sleep environment for human body, when micro-
When environment temperature is reached between 32-34 DEG C of preference temperature of sleep, Release of core material channel is closed.When taking in winter, fabric is played
Intelligent thermal-protection effect, creates good sleep environment.And fabric is not in core material leakage when high-temperature shaping and summer are stored
The case where, assurance function is organized in making full use of when taking.
Specific embodiment
Embodiment 1
A kind of preparation method of warming warm, health care fabric finishing agent
(1) 10g wormwood essential oil, 10g capsicum oil are taken, 10g Arabic gum is added in 500g deionized water, 60 DEG C of high-speed stirreds
Obtain O/W lotion；
(2) 10g temperature sensing material is taken, pH is modulated 4 with 5% citric acid；
(3) temperature sensing material is slowly added dropwise to the mixing of O/W lotion, 2g TG enzyme, room temperature curing is added in 10 drops of drop rate/min
6h；
(4) it stands, be filtered, washed, 60 DEG C of vacuum drying.
The application method of finishing agent:
It configures 8% microcapsules working solution, the super soft adhesive of 3% acrylate is added, by one immersing and rolling of cotton fabric, liquid carrying rate 75%,
150 DEG C of sizing 40s.
Embodiment 2
A kind of preparation method of warming warm, health care fabric finishing agent
(1) 10g wormwood essential oil, 10g capsicum oil are taken, 5g Arabic gum is added in 400g deionized water, 60 DEG C of high-speed stirreds
Obtain O/W lotion；
(2) 5g temperature sensing material is taken, pH is modulated 4 with 5% citric acid；
(3) temperature sensing material is slowly added dropwise to the mixing of O/W lotion, 1.5g TG enzyme is added in 10 drops of drop rate/min, and room temperature is solid
Change 6h；
(4) it stands, be filtered, washed, 60 DEG C of vacuum drying.
The application method of finishing agent:
It configures 5% microcapsules working solution, the super soft adhesive of 2% acrylate is added, by one immersing and rolling of cotton fabric, liquid carrying rate 75%,
150 DEG C of sizing 40s.
Embodiment 3
A kind of preparation method of warming warm, health care fabric finishing agent
(1) 10g wormwood essential oil, 10g capsicum oil are taken, 10g carboxymethyl cellulose is added in 500g deionized water, 60 DEG C of high speeds
Stir to get O/W lotion；
(2) 10g temperature sensing material is taken, pH is modulated 4 with 5% citric acid；
(3) temperature sensing material is slowly added dropwise to the mixing of O/W lotion, 2g glutaraldehyde, room temperature curing is added in 10 drops of drop rate/min
6h；
(4) it stands, be filtered, washed, 60 DEG C of vacuum drying.
The application method of finishing agent:
It configures 8% microcapsules working solution, the super soft adhesive of 3% polyurethane is added, by one immersing and rolling of wool fabric, liquid carrying rate 70%,
150 DEG C of sizing 40s.
It is the fabric of 1g that the fabric arranged in embodiment 1, embodiment 2 and embodiment 3 is taken three parts of quality respectively, is added
Enter into the conical flask of 50% ethanol water containing 100mL, respectively sonic oscillation 60min under the conditions of 15 DEG C, 20 DEG C and 35 DEG C,
With the Release of core material amount in determined by ultraviolet spectrophotometry solution.As a result as shown in the table:
As seen from the above table, on fabric microcapsules discharge core material amount UCST or less with temperature decline and increase, and UCST with
Upper temperature is almost without Release of core material, and the release for finishing agent its core material for illustrating that the present invention obtains is temperature controlled, and arrangement is knitted
Object can play the role of Intelligent thermal-protection when taking in winter.
Claims (10)
1. a kind of warming warming fabric microcapsule dressing agent, it is characterised in that: raw material includes: wormwood essential oil 1-5 in parts by weight
Part, 1-5 parts of capsicum oil, 0.5-2 parts of temperature sensing material, 0.5-2 parts of natural macromolecular material, 0.1-0.5 parts of curing agent.
2. warming warming fabric microcapsule dressing agent according to claim 1, it is characterised in that: wormwood essential oil and chilli extract
The mass ratio of oil is 1:1-5, and temperature sensing material and natural macromolecular material quality are 1-5:1.
3. warming warming fabric microcapsule dressing agent according to claim 1, it is characterised in that: the temperature sensing material is tool
There is the polyampholyte of sulfonate radical and ammonium root, isoelectric point 4.5-5.5, high critical inversion temperature UCST are 25-30 DEG C.
4. warming warming fabric microcapsule dressing agent according to claim 1, it is characterised in that: the natural polymer material
Material is selected from sodium alginate, Arabic gum, carboxymethyl cellulose or chitosan.
5. warming warming fabric microcapsule dressing agent according to claim 1, it is characterised in that: the curing agent is selected from first
Aldehyde, glutaraldehyde or glutamine transaminage.
6. the preparation method of warming warming fabric microcapsule dressing agent described in claim 1, it is characterised in that: including following step
It is rapid:
Step 1, it takes wormwood essential oil, capsicum oil, natural macromolecular material to add in water, in 60-80 DEG C of stirring 1-2h, obtains O/
W lotion；
Step 2, the pH to 4-4.5 of temperature sensing material is adjusted；
Step 3, the temperature sensing material of step 2 is added dropwise in O/W lotion, curing agent, 20-30 DEG C of solidification 6-8h is then added；
Step 4, mixed liquor step 3 obtained is stood, and is then filtered, washed drying, obtains finishing agent.
7. application of the warming warming fabric microcapsule dressing agent described in claim 1 in the warming arrangement of fabric.
8. application according to claim 7, it is characterised in that: fabric is placed in an immersing and rolling in working solution, liquid carrying rate 70-
75%, 120-160 DEG C of sizing 30-60s,
The working solution is the mixed liquor of finishing agent and super soft adhesive, and the concentration of finishing agent is 50-80wt.%, super soft adhesive
Concentration be 2-3wt.%.
9. application according to claim 8, it is characterised in that: the super soft adhesive is acrylate adhesive or gathers
Ammonia ester adhesive.
10. application according to claim 7, it is characterised in that: the fabric be cotton, wool, cashmere, kapok, lyocell,
Modal or viscose etc..
Priority Applications (1)
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| CN201811475718.0A CN109505139A (en) | 2018-12-04 | 2018-12-04 | A kind of warming warming fabric microcapsule dressing agent and its preparation method and application |
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| CN201811475718.0A CN109505139A (en) | 2018-12-04 | 2018-12-04 | A kind of warming warming fabric microcapsule dressing agent and its preparation method and application |
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Cited By (8)
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|---|---|---|---|---|
| CN110804871A (en) * | 2019-09-27 | 2020-02-18 | 嘉兴市民华纺织有限公司 | Production process of filament rayon slub fabric |
| CN110884234A (en) * | 2019-11-20 | 2020-03-17 | 广东职业技术学院 | Intelligent medical temperature sensing fabric |
| CN110983790A (en) * | 2019-11-29 | 2020-04-10 | 江苏金太阳纺织科技股份有限公司 | Self-heating energy storage finishing agent for fabric and preparation method thereof |
| CN111851078A (en) * | 2019-04-28 | 2020-10-30 | 杭州诺邦无纺股份有限公司 | Aromatic non-woven fabric and preparation method thereof |
| CN112609467A (en) * | 2020-12-03 | 2021-04-06 | 武汉中科先进技术研究院有限公司 | Fabric capable of enhancing warm feeling and preparation method thereof |
| CN112609466A (en) * | 2020-11-27 | 2021-04-06 | 江苏金太阳纺织科技股份有限公司 | Stomach-invigorating bedding fabric and preparation method thereof |
| CN116905213A (en) * | 2023-09-07 | 2023-10-20 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell yarn with wormwood microcapsule slow-release function |
| CN116926945A (en) * | 2023-09-07 | 2023-10-24 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell fabric with wormwood microcapsule slow-release function |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111851078A (en) * | 2019-04-28 | 2020-10-30 | 杭州诺邦无纺股份有限公司 | Aromatic non-woven fabric and preparation method thereof |
| CN111851078B (en) * | 2019-04-28 | 2022-11-15 | 杭州诺邦无纺股份有限公司 | Aromatic non-woven fabric and preparation method thereof |
| CN110804871A (en) * | 2019-09-27 | 2020-02-18 | 嘉兴市民华纺织有限公司 | Production process of filament rayon slub fabric |
| CN110884234A (en) * | 2019-11-20 | 2020-03-17 | 广东职业技术学院 | Intelligent medical temperature sensing fabric |
| CN110983790A (en) * | 2019-11-29 | 2020-04-10 | 江苏金太阳纺织科技股份有限公司 | Self-heating energy storage finishing agent for fabric and preparation method thereof |
| CN112609466A (en) * | 2020-11-27 | 2021-04-06 | 江苏金太阳纺织科技股份有限公司 | Stomach-invigorating bedding fabric and preparation method thereof |
| CN112609467A (en) * | 2020-12-03 | 2021-04-06 | 武汉中科先进技术研究院有限公司 | Fabric capable of enhancing warm feeling and preparation method thereof |
| CN112609467B (en) * | 2020-12-03 | 2022-06-14 | 武汉中科先进技术研究院有限公司 | Fabric capable of enhancing warm feeling and preparation method thereof |
| CN116905213A (en) * | 2023-09-07 | 2023-10-20 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell yarn with wormwood microcapsule slow-release function |
| CN116926945A (en) * | 2023-09-07 | 2023-10-24 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell fabric with wormwood microcapsule slow-release function |
| CN116926945B (en) * | 2023-09-07 | 2024-03-29 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell fabric with wormwood microcapsule slow-release function |
| CN116905213B (en) * | 2023-09-07 | 2024-04-02 | 一木生态纺织品(江苏)有限公司 | Processing method of lyocell yarn with wormwood microcapsule slow-release function |
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Application publication date: 20190322 |