CN109423701A - A kind of antibacterial textile material and preparation method thereof - Google Patents
A kind of antibacterial textile material and preparation method thereof Download PDFInfo
- Publication number
- CN109423701A CN109423701A CN201710727637.4A CN201710727637A CN109423701A CN 109423701 A CN109423701 A CN 109423701A CN 201710727637 A CN201710727637 A CN 201710727637A CN 109423701 A CN109423701 A CN 109423701A
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- China
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- parts
- fiber
- degrees celsius
- textile material
- antibacterial textile
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/08—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyacrylonitrile as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
Abstract
The invention discloses a kind of antibacterial textile materials and preparation method thereof, are made of following raw material according to parts by weight: 0.5-2 parts of methylcellulose, 8-15 parts of cotton fiber, 4-8 parts of wool fibre, 2-5 parts of acrylic fibers, 5-10 parts of flaxen fiber, 1-3 parts of bamboo charcoal fiber, 2-6 parts of chitin fiber, 3-5 parts of Eichhornia crassipes, 2-6 parts of Fructus Corni, 2-5 parts of zinc borate, 0.5-3 parts of calcium carbonate powder and 0.5-2 parts of polycaprolactone.The preparation method of the material is also disclosed in the present invention.Raw material sources of the present invention are extensive, and preparation process is simple, are suitable for large-scale industrial production；It is immersed in the soak of Eichhornia crassipes and Fructus Corni in the present invention by cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber, cooperate zinc borate and polycaprolactone again, so that product has good anti-microbial property, meet the use demand of people.
Description
Technical field
The present invention relates to textile material field, specifically a kind of antibacterial textile material.
Background technique
Weaving is the general name of spinning with woven fabric.The weaving of ancient Chinese and printing technology have very long history, early
In primitive society period, ancients have understood and have gathered materials on the spot for the variation of acclimatization, using natural resources as weaving and print
The raw material of dye, and the textile tool being simple to manufacture.Until today, our daily clothing, certain daily necessities and arts work is all
It is the product of weaving and printing technology.
Textile fabric has highly embodied the feature of the novelty of product, plyability, diversification, functionalization, to high-performance, height
Added value, the clothes of specific function, dress ornament and family's textile fabric generate great demand.In recent years, functional textile product in the world
Development is swift and violent, and in addition to the functional products such as common Water-proof and oil-proof, antifouling, fire-retardant, uvioresistant, antibacterial, is born far-infrared warm
The functional performances such as ion product also comes out successively, is greatly enriched piece market, more meets the different purposes of people
The expection of people is not achieved with the antibacterial effect of special consumption demand, but existing textile, this is just that the use of people is brought
Inconvenience.
Summary of the invention
The purpose of the present invention is to provide a kind of antibacterial textile materials, to solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of antibacterial textile material is made of following raw material according to parts by weight: 0.5-2 parts of methylcellulose, 8-15 parts of cotton fiber,
4-8 parts of wool fibre, 2-5 parts of acrylic fibers, 5-10 parts of flaxen fiber, 1-3 parts of bamboo charcoal fiber, 2-6 parts of chitin fiber, 3-5 parts of Eichhornia crassipes,
2-6 parts of Fructus Corni, 2-5 parts of zinc borate, 0.5-3 parts of calcium carbonate powder and 0.5-2 parts of polycaprolactone.
As a further solution of the present invention: wool fibre is using at least one of sheep's wool, the rabbit hair and goats hair.
As a further solution of the present invention: calcium carbonate powder uses nano-calcium carbonate calcium powder.
As a further solution of the present invention: the material further includes 0.1-1.2 parts of glass microballoon.
The preparation method of the antibacterial textile material, the specific steps are as follows:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 10-30 minutes, then are decocted 30-50 minutes, are decocted
When stir medicinal material, stirring number is 2-3 time, the elimination dregs of a decoction after the completion of decocting, and taking liquid and is stirred evenly, and the first mixing is obtained
Solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in 45-60 degrees Celsius by step 2
The first mixed solution in and kept for 1-3 hours, the said components that finish will be impregnated and air-dried at low temperature, first is then added
It base cellulose and polycaprolactone and stirs evenly, is then added in double screw extruder under 50-75 degrees Celsius；
Step 3, then zinc borate and calcium carbonate powder are added twin-screw extrude under agitation, it melts, squeeze out, do
Dry and pelletizing, can be obtained finished product.
As a further solution of the present invention: twin-screw extruder section temperature are as follows: an area temperature 160-175 is Celsius
Degree, two 170-200 degrees Celsius of area's temperature, three 185-205 degrees Celsius of area's temperature, four 170-180 degrees Celsius of area's temperature.
Compared with prior art, the beneficial effects of the present invention are: raw material sources of the present invention are extensive, preparation process is simple, is suitable for
Large-scale industrial production；Pass through cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber in the present invention
It is immersed in the soak of Eichhornia crassipes and Fructus Corni, then cooperates zinc borate and polycaprolactone, so that product has good antibacterial
Performance meets the use demand of people.
Specific embodiment
The technical solution of the patent is explained in further detail With reference to embodiment.
Embodiment 1
A kind of antibacterial textile material is made of following raw material according to parts by weight: 0.5 part of methylcellulose, 8 part, mao fibre of cotton fiber
Tie up 4 parts, 2 parts of acrylic fibers, 5 parts of flaxen fiber, 1 part of bamboo charcoal fiber, 2 parts of chitin fiber, 3 parts of Eichhornia crassipes, 2 parts of Fructus Corni, zinc borate 2
Part, 0.5 part of calcium carbonate powder and 0.5 part of polycaprolactone.Wool fibre uses the mixture of sheep's wool and the rabbit hair.
The preparation method of the antibacterial textile material, the specific steps are as follows:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 12 minutes, then are decocted 35 minutes, stirring when decocting
Medicinal material, stirring number are 2 times, filter off the dregs of a decoction after the completion of decocting, taking liquid and stir evenly, obtain the first mixed solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in the of 48 degrees Celsius by step 2
It in one mixed solution and is kept for 1.5 hours, the said components finished will be impregnated and air-dried at low temperature, methyl fibre is then added
It ties up element and polycaprolactone and is stirred evenly under 55 degrees Celsius, is then added in double screw extruder；
Step 3, then zinc borate and calcium carbonate powder are added twin-screw extrude under agitation, it melts, squeeze out, do
Dry and pelletizing, can be obtained finished product.
Embodiment 2
A kind of antibacterial textile material is made of following raw material according to parts by weight: 1 part of methylcellulose, 11 parts of cotton fiber, wool fibre
6 parts, 3.5 parts of acrylic fibers, 7 parts of flaxen fiber, 1.8 parts of bamboo charcoal fiber, 4.5 parts of chitin fiber, 4 parts of Eichhornia crassipes, 3.5 parts of Fructus Corni,
4 parts of zinc borate, 1.5 parts of nano-calcium carbonate calcium powder and 1 part of polycaprolactone.
The preparation method of the antibacterial textile material, the specific steps are as follows:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 18 minutes, then are decocted 42 minutes, stirring when decocting
Medicinal material, stirring number are 3 times, filter off the dregs of a decoction after the completion of decocting, taking liquid and stir evenly, obtain the first mixed solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in the of 51 degrees Celsius by step 2
It in one mixed solution and is kept for 2 hours, the said components finished will be impregnated and air-dried at low temperature, Methyl cellulose is then added
It element and polycaprolactone and stirs evenly, is then added in double screw extruder at 62 c；
Step 3, then zinc borate and nano-calcium carbonate calcium powder are added twin-screw extrude under agitation, it melts, squeeze
Out, dry and pelletizing, can be obtained finished product.
Embodiment 3
A kind of antibacterial textile material is made of following raw material according to parts by weight: 1.5 parts of methylcellulose, 13 part, mao fibre of cotton fiber
Dimension 7 parts, 4.5 parts of acrylic fibers, 9 parts of flaxen fiber, 2.5 parts of bamboo charcoal fiber, 5 parts of chitin fiber, 4.5 parts of Eichhornia crassipes, 5 parts of Fructus Corni,
4.5 parts of zinc borate, 2.5 parts of calcium carbonate powder, 0.8 part of glass microballoon and 1.5 parts of polycaprolactone.
The preparation method of the antibacterial textile material, the specific steps are as follows:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 24 minutes, then are decocted 45 minutes, stirring when decocting
Medicinal material, stirring number are 2 times, filter off the dregs of a decoction after the completion of decocting, taking liquid and stir evenly, obtain the first mixed solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in the of 56 degrees Celsius by step 2
It in one mixed solution and is kept for 2 hours, the said components finished will be impregnated and air-dried at low temperature, Methyl cellulose is then added
It element and polycaprolactone and stirs evenly, is then added in double screw extruder under 70 degrees Celsius；
Step 3, then zinc borate, glass microballoon and calcium carbonate powder are added twin-screw extrude under agitation, it melts
Melt, squeeze out, drying and pelletizing, twin-screw extruder section temperature are as follows: 160-175 degrees Celsius of area's temperature, two area's temperature
170-200 degrees Celsius, finished product can be obtained in three 185-205 degrees Celsius of area's temperature, four 170-180 degrees Celsius of area's temperature.
Embodiment 4
A kind of antibacterial textile material is made of following raw material according to parts by weight: 2 parts of methylcellulose, 15 parts of cotton fiber, wool fibre
8 parts, 5 parts of acrylic fibers, 10 parts of flaxen fiber, 3 parts of bamboo charcoal fiber, 6 parts of chitin fiber, 5 parts of Eichhornia crassipes, 6 parts of Fructus Corni, zinc borate 5
Part, 3 parts of nano-calcium carbonate calcium powder, 1.2 parts of glass microballoon and 2 parts of polycaprolactone.Wool fibre uses sheep's wool, the rabbit hair and goats hair
Mixture.
The preparation method of the antibacterial textile material, the specific steps are as follows:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 30 minutes, then are decocted 48 minutes, stirring when decocting
Medicinal material, stirring number are 3 times, filter off the dregs of a decoction after the completion of decocting, taking liquid and stir evenly, obtain the first mixed solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in the of 60 degrees Celsius by step 2
It in one mixed solution and is kept for 3 hours, the said components finished will be impregnated and air-dried at low temperature, Methyl cellulose is then added
It element and polycaprolactone and stirs evenly, is then added in double screw extruder under 72 degrees Celsius；
Step 3, then zinc borate and calcium carbonate powder are added twin-screw extrude under agitation, it melts, squeeze out, do
Dry and pelletizing, twin-screw extruder section temperature are as follows: 160-175 degrees Celsius of area's temperature, two area temperature 170-200 are Celsius
Finished product can be obtained in degree, three 185-205 degrees Celsius of area's temperature, four 170-180 degrees Celsius of area's temperature.
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in Eichhornia crassipes and Fructus Corni
Decoction liquor in so that these components come into full contact with decoction liquor, bamboo charcoal fiber inherently has ventilative and antibacterial with moisture absorption
The advantages of antibacterial, chitin fiber has good moisture absorption, ventilative, deodorizing capability, then sufficiently infiltrates with decoction liquor, enhances it
The ability of antibacterial bacteriostatic, zinc borate and polycaprolactone are used cooperatively, and enhance the anti-microbial property of textile material.Methylcellulose and
Calcium carbonate powder is used cooperatively, so that material has good mechanical property.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (6)
1. a kind of antibacterial textile material, which is characterized in that be made of following raw material according to parts by weight: 0.5-2 parts of methylcellulose,
8-15 parts of cotton fiber, 4-8 parts of wool fibre, 2-5 parts of acrylic fibers, 5-10 parts of flaxen fiber, 1-3 parts of bamboo charcoal fiber, chitin fiber 2-6
Part, 3-5 parts of Eichhornia crassipes, 2-6 parts of Fructus Corni, 2-5 parts of zinc borate, 0.5-3 parts of calcium carbonate powder and 0.5-2 parts of polycaprolactone.
2. antibacterial textile material according to claim 1, which is characterized in that the wool fibre using sheep's wool, the rabbit hair and
At least one of goats hair.
3. antibacterial textile material according to claim 1 or 2, which is characterized in that the calcium carbonate powder uses nano-sized carbon
Sour calcium powder.
4. antibacterial textile material according to claim 1, which is characterized in that further include 0.1-1.2 parts of glass microballoon.
5. a kind of preparation method of the antibacterial textile material as described in claim 1-4 is any, which is characterized in that specific steps are such as
Under:
Eichhornia crassipes and Fructus Corni are placed in casserole by step 1, after impregnating 10-30 minutes, then are decocted 30-50 minutes, are decocted
When stir medicinal material, stirring number is 2-3 time, the elimination dregs of a decoction after the completion of decocting, and taking liquid and is stirred evenly, and the first mixing is obtained
Solution；
Cotton fiber, wool fibre, acrylic fibers, flaxen fiber, bamboo charcoal fiber and chitin fiber are immersed in 45-60 degrees Celsius by step 2
The first mixed solution in and kept for 1-3 hours, the said components that finish will be impregnated and air-dried at low temperature, first is then added
It base cellulose and polycaprolactone and stirs evenly, is then added in double screw extruder under 50-75 degrees Celsius；
Step 3, then zinc borate and calcium carbonate powder are added twin-screw extrude under agitation, it melts, squeeze out, do
Dry and pelletizing, can be obtained finished product.
6. the preparation method of antibacterial textile material according to claim 5, which is characterized in that the double screw extruder is each
Zone temperatures are as follows: 160-175 degrees Celsius of area's temperature, two 170-200 degrees Celsius of area's temperature, three 185-205 degrees Celsius of area's temperature,
Four 170-180 degrees Celsius of area's temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710727637.4A CN109423701A (en) | 2017-08-23 | 2017-08-23 | A kind of antibacterial textile material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710727637.4A CN109423701A (en) | 2017-08-23 | 2017-08-23 | A kind of antibacterial textile material and preparation method thereof |
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| CN109423701A true CN109423701A (en) | 2019-03-05 |
Family
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| CN201710727637.4A Pending CN109423701A (en) | 2017-08-23 | 2017-08-23 | A kind of antibacterial textile material and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111235868A (en) * | 2020-03-04 | 2020-06-05 | 荆门市诺维英新材料科技有限公司 | Preparation method of decomposable environment-friendly textile material |
| TWI710678B (en) * | 2019-10-30 | 2020-11-21 | 國立雲林科技大學 | Composite nanofiber, its preparation method and its application |
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Application publication date: 20190305 |