CN104120534B - Health-fitness home textile fabric rich in grape seed extract procyanidine and manufacturing method thereof - Google Patents
Health-fitness home textile fabric rich in grape seed extract procyanidine and manufacturing method thereof Download PDFInfo
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- CN104120534B CN104120534B CN201410390551.3A CN201410390551A CN104120534B CN 104120534 B CN104120534 B CN 104120534B CN 201410390551 A CN201410390551 A CN 201410390551A CN 104120534 B CN104120534 B CN 104120534B
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Abstract
The invention discloses health-fitness home textile fabric rich in grape seed extract procyanidine and a manufacturing method of the health-fitness home textile fabric. The health-fitness home textile fabric comprises warp yarn and weft yarn, the warp yarn is Siro spinning yarn formed by spinning Coolmax moisture adsorption and sweat releasing fibers and modal fibers, and the weft yarn is Siro spinning yarn formed by spinning bamboo charcoal fibers and TENCEL fibers. The grape seed extract procyanidine of the home textile fabric with the health-fitness function is printed on the home textile fabric in a microcapsule mode, and components of the grape seed extract procyanidine have the effect of beautifying skin, resisting wrinkles, removing beverage, preserving moisture, improving the sleeping and the like on the human body.
Description
Technical field
The invention belongs to a textile fabric field, be specifically related to one and be rich in Grape Seed Extract Procyanidin health care man textile fabric and preparation method thereof.
Background technology
In recent years, the research and development of functional health man textile fabric arouses great concern, and becomes the heat subject in weaving face fabric field of scientific study.The very big concern that the research of textiles also result in people is used for extracted form natural plant beneficiating ingredient.Grape Seed Extract Procyanidin is a kind of bioflavonoid having special molecular structure, is the most effective natural of removing people interior free yl of generally acknowledging in the world at present.In skin, OPC has unique chemistry and physiologically active, in skin care products, play multiple action, as anti-ageing, uvioresistant, radioresistance, brighten, moisturizing etc., have unique effect to the skin aging that many factors causes.
Summary of the invention
The object of the invention is: for the effect of existing Grape Seed Extract Procyanidin to skin beneficiating, preparation one is rich in Grape Seed Extract Procyanidin health care man textile fabric, endeavour to solve Grape Seed Extract Procyanidin health care man textile fabric crock fastness poor, wash that fastness is not high, adhesion strength is poor by rubbing with the hands, the technical problem that the low grade of slow release effect is long-term.Microcapsules technology is adopted to play a very good protection to Grape Seed Extract Procyanidin active component; and there is obvious slow release effect; extend the effective acting time of Grape Seed Extract Procyanidin, the aspects such as health-care textile product have a good application prospect.
For achieving the above object, the present invention is achieved by the following technical solutions:
One of the present invention is rich in Grape Seed Extract Procyanidin health care man textile fabric, described health care man textile fabric comprises warp thread and weft yarn, described warp thread is the siro-spinning yarn that Coolmax hygroscopic fibre and Modal fibre are spun into, described weft yarn is the siro-spinning yarn that bamboo-carbon fibre and TENCEL fiber are spun into, and described health care man textile fabric Grape Seed Extract Procyanidin prints with the form of microcapsules textile fabric of being in.
As optimization: in described warp thread, Coolmax hygroscopic fibre and Modal fibre weight ratio are 30-35:65-70.
As optimization: in described weft yarn, bamboo-carbon fibre and TENCEL fibre weight are than being 15-20:80-85.
As optimization: described Coolmax hygroscopic fibre fineness is 5-30dtex.
As optimization: described Modal fibre fineness is 10-20dtex.
As optimization: described bamboo-carbon fibre fineness is 1-15dtex.
As optimization: described TENCEL fibre fineness is 5-20dtex.
As optimization: during described siro-spinning yarn spinning, twist multiplier is 460-840.
Be rich in a preparation method for Grape Seed Extract Procyanidin health care man textile fabric, comprise the steps:
Step one:
Selecting carboxymethyl cellulose, ethyl cellulose, polyvinylamine to make composition A is dissolved in Sucrose Acetate ester solution, described carboxymethyl cellulose, ethyl cellulose, the consumption of polyvinylamine forms according to parts by weight: carboxymethyl cellulose: 2.0 ~ 3.0 parts, ethyl cellulose: 2.0 ~ 2.5 parts, polyvinylamine: 0.2-0.5 part; The mass concentration of control composition A in Sucrose Acetate ester solution is 20-40g/L; Grape Seed Extract Procyanidin, at 5-8 DEG C, adds in the Sucrose Acetate ester solution of composition A by control temperature, and it is 3g/L that Grape Seed Extract Procyanidin adds mass concentration in the Sucrose Acetate ester solution of composition A; Under 2000r/min condition, stir 5min, must organic phase B be clarified;
Step 2:
Emulsifying agent glycerin monostearate is selected to prepare 0.5% ~ 0.9% glycerin monostearate aqueous solution, organic phase B and 0.5% ~ 0.9% glycerin monostearate aqueous solution are joined in the High Rotation Speed stirred tank of 1800r/min, the consumption of described organic phase B and 0.5% ~ 0.9% glycerin monostearate aqueous solution forms according to parts by weight: organic phase B:3.4 ~ 6.8 part, 0.5% ~ 0.9% glycerin monostearate aqueous solution: 3.0 ~ 4.0 parts, in ice-water bath, carry out stirring reaction 10 minutes, vacuumize standing 1h, suction filtration, 45 DEG C of dryings, obtain Powdered microcapsules C;
Step 3:
Urea, adhesive, Powdered microcapsules C, water is selected to make finishing agent, the consumption of described urea, adhesive, Powdered microcapsules C and water forms according to parts by weight: urea: 0.1 ~ 0.5 part, thickener KT-501:0.2 ~ 0.6 part, adhesive: 1.2 ~ 1.5 parts, Powdered microcapsules C:3.4 ~ 4.5 part, water: 30 ~ 40 parts, fabric makes finished product by following steps
Padding method:
Technological process: fabric → pad (pick-up rate 80--100%) → oven dry (100 DEG C) → finished product.
Beneficial effect: the present invention is rich in Grape Seed Extract Procyanidin health care man textile fabric for the preparation of one, can Grape Seed Extract Procyanidin be imprinted on weaving face fabric, Grape Seed Extract Procyanidin in composition is in skin care, play multiple action, as anti-ageing, uvioresistant, radioresistance, brighten, moisturizing etc., also have facilitation to sleep.Endeavour to solve Grape Seed Extract Procyanidin health care man textile fabric crock fastness poor, wash that fastness is not high, adhesion strength is poor by rubbing with the hands, the technical problem that the low grade of slow release effect is long-term.Microcapsules technology is adopted to play a very good protection to Grape Seed Extract Procyanidin active component; and there is obvious slow release effect; extend the effective acting time of Grape Seed Extract Procyanidin, the aspects such as health-care textile product have a good application prospect.
Detailed description of the invention
Below in conjunction with detailed description of the invention, set forth the present invention further.
embodiment 1:
One is rich in Grape Seed Extract Procyanidin health care man textile fabric, described health care man textile fabric comprises warp thread and weft yarn, described warp thread is the siro-spinning yarn that Coolmax hygroscopic fibre and Modal fibre are spun into, in warp thread, Coolmax hygroscopic fibre and Modal fibre weight ratio are 30:65, described Coolmax hygroscopic fibre fineness is 5dtex, described Modal fibre fineness is 10dtex, described weft yarn is the siro-spinning yarn that bamboo-carbon fibre and TENCEL fiber are spun into, in weft yarn, bamboo-carbon fibre and TENCEL fibre weight are than being 15:80, described bamboo-carbon fibre fineness is 1dtex, described TENCEL fibre fineness is 5dtex, described health care man textile fabric Grape Seed Extract Procyanidin prints with the form of microcapsules textile fabric of being in.During described siro-spinning yarn spinning, twist multiplier is 460.
Be rich in a preparation method for Grape Seed Extract Procyanidin health care man textile fabric, comprise the steps:
Step one:
Selecting carboxymethyl cellulose, ethyl cellulose, polyvinylamine to make composition A is dissolved in Sucrose Acetate ester solution, described carboxymethyl cellulose, ethyl cellulose, the consumption of polyvinylamine forms according to parts by weight: carboxymethyl cellulose: 2.0 parts, ethyl cellulose: 2.0 parts, polyvinylamine: 0.2 part; The mass concentration of control composition A in Sucrose Acetate ester solution is 20g/L; Grape Seed Extract Procyanidin, at 5 DEG C, adds in the Sucrose Acetate ester solution of composition A by control temperature, and it is 3g/L that Grape Seed Extract Procyanidin adds mass concentration in the Sucrose Acetate ester solution of composition A; Under 2000r/min condition, stir 5min, must organic phase B be clarified;
Step 2:
Emulsifying agent glycerin monostearate is selected to prepare the 0.5% glycerin monostearate aqueous solution, organic phase B and the 0.5% glycerin monostearate aqueous solution are joined in the High Rotation Speed stirred tank of 1800r/min, the consumption of described organic phase B and the 0.5% glycerin monostearate aqueous solution forms according to parts by weight: organic phase B:3.4 part, the 0.5% glycerin monostearate aqueous solution: 3.0 parts, in ice-water bath, carry out stirring reaction 10 minutes, vacuumize standing 1h, suction filtration, 45 DEG C of dryings, obtain Powdered microcapsules C;
Step 3:
Urea, adhesive, Powdered microcapsules C, water is selected to make finishing agent, the consumption of described urea, adhesive, Powdered microcapsules C and water forms according to parts by weight: urea: 0.1 part, thickener KT-501:0.2 part, adhesive: 1.2 parts, Powdered microcapsules C:3.4 part, water: 30 parts, fabric makes finished product by following steps
Padding method:
Technological process: fabric → pad (pick-up rate 80%) → oven dry (100 DEG C) → finished product.
embodiment 2:
One is rich in Grape Seed Extract Procyanidin health care man textile fabric, described health care man textile fabric comprises warp thread and weft yarn, described warp thread is the siro-spinning yarn that Coolmax hygroscopic fibre and Modal fibre are spun into, in warp thread, Coolmax hygroscopic fibre and Modal fibre weight ratio are 35:70, described Coolmax hygroscopic fibre fineness is 30dtex, described Modal fibre fineness is 20dtex, described weft yarn is the siro-spinning yarn that bamboo-carbon fibre and TENCEL fiber are spun into, in weft yarn, bamboo-carbon fibre and TENCEL fibre weight are than being 20:85, described bamboo-carbon fibre fineness is 15dtex, described TENCEL fibre fineness is 20dtex, described health care man textile fabric Grape Seed Extract Procyanidin prints with the form of microcapsules textile fabric of being in.During described siro-spinning yarn spinning, twist multiplier is 840.
Be rich in a preparation method for Grape Seed Extract Procyanidin health care man textile fabric, comprise the steps:
Step one:
Selecting carboxymethyl cellulose, ethyl cellulose, polyvinylamine to make composition A is dissolved in Sucrose Acetate ester solution, described carboxymethyl cellulose, ethyl cellulose, the consumption of polyvinylamine forms according to parts by weight: carboxymethyl cellulose: 3.0 parts, ethyl cellulose: 2.5 parts, polyvinylamine: 0.5 part; The mass concentration of control composition A in Sucrose Acetate ester solution is 40g/L; Grape Seed Extract Procyanidin, at 8 DEG C, adds in the Sucrose Acetate ester solution of composition A by control temperature, and it is 3g/L that Grape Seed Extract Procyanidin adds mass concentration in the Sucrose Acetate ester solution of composition A; Under 2000r/min condition, stir 5min, must organic phase B be clarified;
Step 2:
Emulsifying agent glycerin monostearate is selected to prepare the 0.9% glycerin monostearate aqueous solution, organic phase B and the 0.9% glycerin monostearate aqueous solution are joined in the High Rotation Speed stirred tank of 1800r/min, the consumption of described organic phase B and the 0.9% glycerin monostearate aqueous solution forms according to parts by weight: organic phase B:6.8 part, the 0.9% glycerin monostearate aqueous solution: 4.0 parts, in ice-water bath, carry out stirring reaction 10 minutes, vacuumize standing 1h, suction filtration, 45 DEG C of dryings, obtain Powdered microcapsules C;
Step 3:
Urea, adhesive, Powdered microcapsules C, water is selected to make finishing agent, the consumption of described urea, adhesive, Powdered microcapsules C and water forms according to parts by weight: urea: 0.5 part, thickener KT-501:0.6 part, adhesive: 1.5 parts, Powdered microcapsules C:4.5 part, water: 40 parts, fabric makes finished product by following steps
Padding method:
Technological process: fabric → pad (pick-up rate 100%) → oven dry (100 DEG C) → finished product.
embodiment 3:
One is rich in Grape Seed Extract Procyanidin health care man textile fabric, described health care man textile fabric comprises warp thread and weft yarn, described warp thread is the siro-spinning yarn that Coolmax hygroscopic fibre and Modal fibre are spun into, in warp thread, Coolmax hygroscopic fibre and Modal fibre weight ratio are 33:67, described Coolmax hygroscopic fibre fineness is 19dtex, described Modal fibre fineness is 23dtex, described weft yarn is the siro-spinning yarn that bamboo-carbon fibre and TENCEL fiber are spun into, in weft yarn, bamboo-carbon fibre and TENCEL fibre weight are than being 18:83, described bamboo-carbon fibre fineness is 9dtex, described TENCEL fibre fineness is 14dtex, described health care man textile fabric Grape Seed Extract Procyanidin prints with the form of microcapsules textile fabric of being in.During described siro-spinning yarn spinning, twist multiplier is 710.
Be rich in a preparation method for Grape Seed Extract Procyanidin health care man textile fabric, comprise the steps:
Step one:
Selecting carboxymethyl cellulose, ethyl cellulose, polyvinylamine to make composition A is dissolved in Sucrose Acetate ester solution, described carboxymethyl cellulose, ethyl cellulose, the consumption of polyvinylamine forms according to parts by weight: carboxymethyl cellulose: 2.3 parts, ethyl cellulose: 2.2 parts, polyvinylamine: 0.4 part; The mass concentration of control composition A in Sucrose Acetate ester solution is 27g/L; Grape Seed Extract Procyanidin, at 6 DEG C, adds in the Sucrose Acetate ester solution of composition A by control temperature, and it is 3g/L that Grape Seed Extract Procyanidin adds mass concentration in the Sucrose Acetate ester solution of composition A; Under 2000r/min condition, stir 5min, must organic phase B be clarified;
Step 2:
Emulsifying agent glycerin monostearate is selected to prepare the 0.7% glycerin monostearate aqueous solution, organic phase B and the 0.6% glycerin monostearate aqueous solution are joined in the High Rotation Speed stirred tank of 1800r/min, the consumption of described organic phase B and the 0.8% glycerin monostearate aqueous solution forms according to parts by weight: organic phase B:3.9 part, the 0.8% glycerin monostearate aqueous solution: 3.4 parts, in ice-water bath, carry out stirring reaction 10 minutes, vacuumize standing 1h, suction filtration, 45 DEG C of dryings, obtain Powdered microcapsules C;
Step 3:
Urea, adhesive, Powdered microcapsules C, water is selected to make finishing agent, the consumption of described urea, adhesive, Powdered microcapsules C and water forms according to parts by weight: urea: 0.3 part, thickener KT-501:0.5 part, adhesive: 1.4 parts, Powdered microcapsules C:4.1 part, water: 36 parts, fabric makes finished product by following steps
Padding method:
Technological process: fabric → pad (pick-up rate 87%) → oven dry (100 DEG C) → finished product.
According to above 3 embodiments, Controlled-Release Capability of Microcapsules experiment is adopted to utilize dynamic dialysis method to test the release conditions of microcapsules.Record out every test data.The maximum drugloading rate of microcapsules is 23.8 %, has higher utilization rate of raw materials and medicine retention rate.Slowly-releasing experiment display, first 15 days Grape Seed Extract Procyanidin liquid rate of release and burst size are comparatively large, tend towards stability after 30 days.Active constituents of medicine is still had to exist after 90 days.Show that microcapsules technology plays a very good protection to Grape Seed Extract Procyanidin, and there is obvious slow release effect.
Claims (9)
1. be rich in a preparation method for Grape Seed Extract Procyanidin health care man textile fabric, it is characterized in that: comprise the steps:
Step one:
Selecting carboxymethyl cellulose, ethyl cellulose, polyvinylamine to make composition A is dissolved in Sucrose Acetate ester solution, described carboxymethyl cellulose, ethyl cellulose, the consumption of polyvinylamine forms according to parts by weight: carboxymethyl cellulose: 2.0 ~ 3.0 parts, ethyl cellulose: 2.0 ~ 2.5 parts, polyvinylamine: 0.2-0.5 part; The mass concentration of control composition A in Sucrose Acetate ester solution is 20-40g/L; Grape Seed Extract Procyanidin, at 5-8 DEG C, adds in the Sucrose Acetate ester solution of composition A by control temperature, and it is 3g/L that Grape Seed Extract Procyanidin adds mass concentration in the Sucrose Acetate ester solution of composition A; Under 2000r/min condition, stir 5min, must organic phase B be clarified;
Step 2:
Emulsifying agent glycerin monostearate is selected to prepare 0.5% ~ 0.9% glycerin monostearate aqueous solution, organic phase B and 0.5% ~ 0.9% glycerin monostearate aqueous solution are joined in the High Rotation Speed stirred tank of 1800r/min, the consumption of described organic phase B and 0.5% ~ 0.9% glycerin monostearate aqueous solution forms according to parts by weight: organic phase B:3.4 ~ 6.8 part, 0.5% ~ 0.9% glycerin monostearate aqueous solution: 3.0 ~ 4.0 parts, in ice-water bath, carry out stirring reaction 10 minutes, vacuumize standing 1h, suction filtration, 45 DEG C of dryings, obtain Powdered microcapsules C,
Step 3:
Urea, adhesive, Powdered microcapsules C, water is selected to make finishing agent, the consumption of described urea, adhesive, Powdered microcapsules C and water forms according to parts by weight: urea: 0.1 ~ 0.5 part, thickener KT-501:0.2 ~ 0.6 part, adhesive: 1.2 ~ 1.5 parts, Powdered microcapsules C:3.4 ~ 4.5 part, water: 30 ~ 40 parts, fabric makes finished product by following steps
Padding method:
Technological process: fabric → pad, pick-up rate 80--100% → oven dry, bake out temperature is 100 DEG C → finished product.
2. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 1, it is characterized in that: comprise warp thread and weft yarn, described warp thread is the siro-spinning yarn that Coolmax hygroscopic fibre and Modal fibre are spun into, and described weft yarn is the siro-spinning yarn that bamboo-carbon fibre and TENCEL fiber are spun into.
3. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: in described warp thread, Coolmax hygroscopic fibre and Modal fibre weight ratio are 30-35:65-70.
4. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: in described weft yarn, bamboo-carbon fibre and TENCEL fibre weight are than being 15-20:80-85.
5. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: described Coolmax hygroscopic fibre fineness is 5-30dtex.
6. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: described Modal fibre fineness is 10-20dtex.
7. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: described bamboo-carbon fibre fineness is 1-15dtex.
8. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: described TENCEL fibre fineness is 5-20dtex.
9. the fabric prepared of the preparation method being rich in Grape Seed Extract Procyanidin health care man textile fabric according to claim 2, is characterized in that: during described siro-spinning yarn spinning, twist multiplier is 460-840.
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| CN105797657A (en) * | 2014-12-30 | 2016-07-27 | 上海水星家用纺织品股份有限公司 | Preparation method and use of anthocyanidin microcapsule finishing agent |
| CN105442075B (en) * | 2016-01-26 | 2018-04-17 | 中科纺织研究院（青岛）有限公司 | A kind of procyanidine cellulose fibre and preparation method thereof |
| CN108118536A (en) * | 2016-11-28 | 2018-06-05 | 丹阳市丹祈纺织有限公司 | Ms's fragrance skin makeup fabric |
| CN109881478A (en) * | 2019-03-08 | 2019-06-14 | 中服帽饰创意研发南通有限公司 | A kind of antimicrobial health care function scrambled eggs fabric and preparation method thereof |
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Effective date of registration: 20180626 Address after: 226000 3 3 Yonghe Road, Gangzha District, Nantong, Jiangsu. Patentee after: ZHONGFU CAP DECORATION ORIGINALITY RESEARCH AND DEVELOPMENT NANTONG Co.,Ltd. Address before: 226000 No. 105 youth East Road, Chongchuan District, Nantong, Jiangsu Patentee before: JIANGSU College OF ENGINEERING AND TECHNOLOGY |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Health home textile fabric rich in grape seed extract proanthocyanidin and its preparation method Effective date of registration: 20230217 Granted publication date: 20150708 Pledgee: Bank of China Limited by Share Ltd. Nantong Chengdong sub branch Pledgor: ZHONGFU CAP DECORATION ORIGINALITY RESEARCH AND DEVELOPMENT NANTONG Co.,Ltd. Registration number: Y2023980032896 |