CN109881478A - A kind of antimicrobial health care function scrambled eggs fabric and preparation method thereof - Google Patents
A kind of antimicrobial health care function scrambled eggs fabric and preparation method thereof Download PDFInfo
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- CN109881478A CN109881478A CN201910176047.6A CN201910176047A CN109881478A CN 109881478 A CN109881478 A CN 109881478A CN 201910176047 A CN201910176047 A CN 201910176047A CN 109881478 A CN109881478 A CN 109881478A
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Abstract
The invention discloses a kind of antimicrobial health care function scrambled eggs fabrics and preparation method thereof, scrambled eggs fabric is plain weave, include warp thread and weft yarn, the warp thread is cotton and lyocell scribbled, blending ratio is 50:50, yarn count is 14.6tex, weft yarn is coconut palm charcoal and lyocell scribbled, yarn count is 14.6tex, it further include antimicrobial health-care material, antimicrobial health-care material is arranged in the form of microcapsules on scrambled eggs fabric, it joined coconut palm Carbon fibe in fabric of the invention, it is acted on fabric by hydroxypropyl chitosan and rich in Grape Seed Extract Procyanidin simultaneously, antibacterial is given full play to, deodorization, hydroscopic fast-drying, it promotes blood circulation, anti-aging, the multi-efficiencies such as uvioresistant and release anion.The action time of effect is effectively extended using microcapsules technology, in addition, as the wall material that microcapsules make also making to operate using hydroxypropyl chitosan more convenient.
Description
Technical field
The present invention relates to scrambled eggs fabric manufacture technology field, specially a kind of antimicrobial health care function scrambled eggs fabric and its system
Preparation Method.
Background technique
Coconut palm Carbon fibe is a kind of environment-protection fiber, has activating cell, eliminates fatigue, absorption peculiar smell, promote blood circulation, inhale
The functions such as wet quick-drying, while far infrared and release anion can be emitted, thus it is particularly suitable for production scrambled eggs fabric.Grape pip extracts
Object procyanidine is a kind of bioflavonoid for having special molecular structure, is free in the removing human body generally acknowledged in the world at present
The effective natural of base.Procyanidine has unique chemistry and physiological activity, has anti-aging, uvioresistant, resists
The multiple actions such as radiation.Hydroxypropyl chitosan is the chitosan derivatives prepared using chitosan as raw material, and can be directly dissolved in water makes
With simple and convenient.With a variety of excellent properties such as good biological degradability, biocompatibility, environmental-friendly, it can assign and knit
The characteristics such as the excellent antibacterial crease-resistant of object, moisture absorption be antistatic.Above-mentioned several functions are effectively combined, scrambled eggs face can be played to greatest extent
The functionality of material, has broad application prospects.
Summary of the invention
It is above-mentioned to solve the purpose of the present invention is to provide a kind of antimicrobial health care function scrambled eggs fabric and preparation method thereof
The problem of being proposed in background technique.
To achieve the above object, the invention provides the following technical scheme: a kind of antimicrobial health care function scrambled eggs fabric, described
Scrambled eggs fabric is plain weave, includes warp thread and weft yarn, and the warp thread is cotton and lyocell scribbled, blending ratio 50:50,
Yarn count is 14.6tex, and weft yarn is coconut palm charcoal and lyocell scribbled, and yarn count 14.6tex further includes antimicrobial health-care material, is resisted
Bacterium health-care material is arranged in the form of microcapsules on scrambled eggs fabric, and the antimicrobial health-care material component includes α-in parts by weight
2-6 parts of L- guluronic acid, 1-4 parts of nano zine oxide, 2-4 parts of polyvinyl alcohol, 1-3 parts of lignin, hydroxypropyl chitosan 10-20
Part, 4-10 parts of Grape Seed Extract Procyanidin, 3-9 parts of calcium chloride, 2-6 parts of sodium alginate.
Preferably, preparation method includes the following steps:
A, certain density hydroxypropyl sugar juice and calcium chloride solution are prepared, is mixed with the ratio of 2:1, hydroxypropyl is made
Base enclosure glycan calcium chloride mixed solution；
B, prepare 2% sodium alginate soln, and Grape Seed Extract Procyanidin is dissolved according to a certain percentage wherein,
Under the at the uniform velocity stirring of 300-400r/min, 60 DEG C of sodium alginate solns are instilled into rapidly hydroxypropyl chitosan calcium chloride mixed solution
In, continue to stir 20min, sequentially add α-L- guluronic acid, nano zine oxide, polyvinyl alcohol, lignin in whipping process,
It being filtered, washs later, hydroxypropyl chitosan and sodium alginate are attracted by positive and negative charge, polyelectrolyte film is formed, thus
Sodium alginate-hydroxypropyl chitosan the microcapsules for being rich in Grape Seed Extract Procyanidin are formed, are reacted as follows:
C, it will be enriched in sodium alginate-hydroxypropyl chitosan microcapsules 10-30g/L, low of Grape Seed Extract Procyanidin
Warm adhesive 20-30g/L, amido silicon oil 10-20g/L, bleeding agent 2-4g/L, are made into finishing fluid.
Preferably, in the step C, fabric is first immersed into 20min-30min in finishing fluid, then using second dipping and rolling
Fabric is put into preliminary drying 10-20min in pre-baking box later in finishing fluid processing to fabric by mode, and preliminary drying temperature is 80-85
DEG C, it is put into baking oven further dries later, temperature is 120-130 DEG C, time 5-8min, and pick-up is controlled 100%.
Preferably, the weft yarn is coconut palm charcoal and lyocell scribbled, blending ratio 50-70:50-30.
Preferably, in the step A, the concentration of hydroxypropyl sugar juice is 2%-3%.
Preferably, the concentration of calcium chloride solution is 2%-4% in the step A.
Preferably, middle hydroxypropyl chitosan is o- hydroxypropyl chitosan in the step A, and structure is as follows:
Preferably, the weight ratio of Grape Seed Extract Procyanidin and sodium alginate soln is 1:25-1 in the step B:
15。
Compared with prior art, the beneficial effects of the present invention are: joined coconut palm Carbon fibe in fabric of the invention, simultaneously will
It hydroxypropyl chitosan and is acted on fabric rich in Grape Seed Extract Procyanidin, it is fast to have given full play to antibacterial, deodorization, moisture absorption
It does, promote blood circulation, anti-aging, uvioresistant and the release multi-efficiencies such as anion.Effectively extended using microcapsules technology
The action time of effect, in addition, as the wall material that microcapsules make also making to operate using hydroxypropyl chitosan more convenient.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
The invention provides the following technical scheme: a kind of antimicrobial health care function scrambled eggs fabric, the scrambled eggs fabric is plain weave
Tissue, includes warp thread and weft yarn, and the warp thread is cotton and lyocell scribbled, blending ratio 50:50, yarn count 14.6tex,
Weft yarn is coconut palm charcoal and lyocell scribbled, and yarn count 14.6tex further includes antimicrobial health-care material, and antimicrobial health-care material is with micro-
The form of capsule is arranged on scrambled eggs fabric, and the antimicrobial health-care material component includes α-L- guluronic acid 2- in parts by weight
6 parts, 1-4 parts of nano zine oxide, 2-4 parts of polyvinyl alcohol, 1-3 parts of lignin, 10-20 parts of hydroxypropyl chitosan, grape pip extraction
4-10 parts of object procyanidine, 3-9 parts of calcium chloride, 2-6 parts of sodium alginate.
Embodiment one:
Antimicrobial health-care material component includes 2 parts of α-L- guluronic acid, 1 part of nano zine oxide, polyethylene in parts by weight
2 parts of alcohol, 1 part of lignin, 10 parts of hydroxypropyl chitosan, 4 parts of Grape Seed Extract Procyanidin, 3 parts of calcium chloride, sodium alginate 2
Part.
The preparation method of the present embodiment the following steps are included:
A, certain density hydroxypropyl sugar juice and calcium chloride solution are prepared, is mixed with the ratio of 2:1, hydroxypropyl is made
Base enclosure glycan calcium chloride mixed solution；
B, prepare 2% sodium alginate soln, and Grape Seed Extract Procyanidin is dissolved according to a certain percentage wherein,
Under the at the uniform velocity stirring of 300r/min, 60 DEG C of sodium alginate solns are instilled rapidly in hydroxypropyl chitosan calcium chloride mixed solution,
Continue to stir 20min, sequentially adds α-L- guluronic acid, nano zine oxide, polyvinyl alcohol, lignin in whipping process, it
After be filtered, washed, hydroxypropyl chitosan and sodium alginate pass through positive and negative charge and attract, and polyelectrolyte film are formed, thus shape
At the sodium alginate-hydroxypropyl chitosan microcapsules for being rich in Grape Seed Extract Procyanidin, react as follows:
C, sodium alginate-hydroxypropyl chitosan microcapsules 10g/L, the low temperature that will be enriched in Grape Seed Extract Procyanidin are viscous
Mixture 20g/L, amido silicon oil 10g/L, bleeding agent 2g/L, are made into finishing fluid.
In the present embodiment, in step C, fabric is first immersed into 20min in finishing fluid, it then will by the way of second dipping and rolling
In finishing fluid processing to fabric, fabric is put into preliminary drying 10min in pre-baking box later, preliminary drying temperature is 80 DEG C, is put into baking later
It is further dried in case, temperature is 120 DEG C, time 5min, and pick-up is controlled 100%.
In the present embodiment, weft yarn is coconut palm charcoal and lyocell scribbled, blending ratio 50:50.
In the present embodiment, in step A, the concentration of hydroxypropyl sugar juice is 2%.
In the present embodiment, the concentration of calcium chloride solution is 2% in step A.
In this implementation, middle hydroxypropyl chitosan is o- hydroxypropyl chitosan in step A, and structure is as follows:
In the present embodiment, the weight ratio of Grape Seed Extract Procyanidin and sodium alginate soln is 1:25 in step B.
Embodiment two:
Antimicrobial health-care material component includes 6 parts of α-L- guluronic acid, 4 parts of nano zine oxide, polyethylene in parts by weight
4 parts of alcohol, 3 parts of lignin, 20 parts of hydroxypropyl chitosan, 10 parts of Grape Seed Extract Procyanidin, 9 parts of calcium chloride, sodium alginate 6
Part.
The preparation method of the present embodiment the following steps are included:
A, certain density hydroxypropyl sugar juice and calcium chloride solution are prepared, is mixed with the ratio of 2:1, hydroxypropyl is made
Base enclosure glycan calcium chloride mixed solution；
B, prepare 2% sodium alginate soln, and Grape Seed Extract Procyanidin is dissolved according to a certain percentage wherein,
Under the at the uniform velocity stirring of 400r/min, 60 DEG C of sodium alginate solns are instilled rapidly in hydroxypropyl chitosan calcium chloride mixed solution,
Continue to stir 20min, sequentially adds α-L- guluronic acid, nano zine oxide, polyvinyl alcohol, lignin in whipping process, it
After be filtered, washed, hydroxypropyl chitosan and sodium alginate pass through positive and negative charge and attract, and polyelectrolyte film are formed, thus shape
At the sodium alginate-hydroxypropyl chitosan microcapsules for being rich in Grape Seed Extract Procyanidin, react as follows:
C, sodium alginate-hydroxypropyl chitosan microcapsules 30g/L, the low temperature that will be enriched in Grape Seed Extract Procyanidin are viscous
Mixture 30g/L, amido silicon oil 20g/L, bleeding agent 4g/L, are made into finishing fluid.
In the present embodiment, in step C, fabric is first immersed into 30min in finishing fluid, it then will by the way of second dipping and rolling
In finishing fluid processing to fabric, fabric is put into preliminary drying 20min in pre-baking box later, preliminary drying temperature is 85 DEG C, is put into baking later
It is further dried in case, temperature is 130 DEG C, time 8min, and pick-up is controlled 100%.
In the present embodiment, weft yarn is coconut palm charcoal and lyocell scribbled, blending ratio 55:50.
In the present embodiment, in step A, the concentration of hydroxypropyl sugar juice is 3%.
In the present embodiment, the concentration of calcium chloride solution is 4% in step A.
In this implementation, middle hydroxypropyl chitosan is o- hydroxypropyl chitosan in step A, and structure is as follows:
In the present embodiment, the weight ratio of Grape Seed Extract Procyanidin and sodium alginate soln is 1:15 in step B.
Embodiment three:
Antimicrobial health-care material component includes 4 parts of α-L- guluronic acid, 2 parts of nano zine oxide, polyethylene in parts by weight
3 parts of alcohol, 2 parts of lignin, 15 parts of hydroxypropyl chitosan, 7 parts of Grape Seed Extract Procyanidin, 6 parts of calcium chloride, sodium alginate 4
Part.
The preparation method of the present embodiment the following steps are included:
A, certain density hydroxypropyl sugar juice and calcium chloride solution are prepared, is mixed with the ratio of 2:1, hydroxypropyl is made
Base enclosure glycan calcium chloride mixed solution；
B, prepare 2% sodium alginate soln, and Grape Seed Extract Procyanidin is dissolved according to a certain percentage wherein,
Under the at the uniform velocity stirring of 350r/min, 60 DEG C of sodium alginate solns are instilled rapidly in hydroxypropyl chitosan calcium chloride mixed solution,
Continue to stir 20min, sequentially adds α-L- guluronic acid, nano zine oxide, polyvinyl alcohol, lignin in whipping process, it
After be filtered, washed, hydroxypropyl chitosan and sodium alginate pass through positive and negative charge and attract, and polyelectrolyte film are formed, thus shape
At the sodium alginate-hydroxypropyl chitosan microcapsules for being rich in Grape Seed Extract Procyanidin, react as follows:
C, sodium alginate-hydroxypropyl chitosan microcapsules 20g/L, the low temperature that will be enriched in Grape Seed Extract Procyanidin are viscous
Mixture 25g/L, amido silicon oil 15g/L, bleeding agent 3g/L, are made into finishing fluid.
In the present embodiment, in step C, fabric is first immersed into 25min in finishing fluid, it then will by the way of second dipping and rolling
In finishing fluid processing to fabric, fabric is put into preliminary drying 15min in pre-baking box later, preliminary drying temperature is 82 DEG C, is put into baking later
It is further dried in case, temperature is 125 DEG C, time 6min, and pick-up is controlled 100%.
In the present embodiment, weft yarn is coconut palm charcoal and lyocell scribbled, blending ratio 50:50.
In the present embodiment, in step A, the concentration of hydroxypropyl sugar juice is 2%.
In the present embodiment, the concentration of calcium chloride solution is 3% in step A.
In this implementation, middle hydroxypropyl chitosan is o- hydroxypropyl chitosan in step A, and structure is as follows:
In the present embodiment, the weight ratio of Grape Seed Extract Procyanidin and sodium alginate soln is 1:20 in step B.
Experimental example:
It is tested for the property using scrambled eggs fabric made from various embodiments of the present invention, obtains data and be as follows:
In conclusion joined coconut palm Carbon fibe in fabric of the invention, while by hydroxypropyl chitosan and being rich in grape pip
Extract procyanidine acts on fabric, given full play to antibacterial, deodorization, hydroscopic fast-drying, promote blood circulation, anti-aging,
The multi-efficiencies such as uvioresistant and release anion.The action time that effect is effectively extended using microcapsules technology, in addition, adopting
Use hydroxypropyl chitosan also make to operate as the wall material that microcapsules make it is more convenient.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of antimicrobial health care function scrambled eggs fabric, it is characterised in that: the scrambled eggs fabric is plain weave, comprising warp thread and
Weft yarn, the warp thread are cotton and lyocell scribbled, and blending ratio 50:50, yarn count 14.6tex, weft yarn is coconut palm charcoal and Lay
Sai Er scribbled, yarn count 14.6tex further includes antimicrobial health-care material, and antimicrobial health-care material is arranged in the form of microcapsules
In on scrambled eggs fabric, the antimicrobial health-care material component includes 2-6 parts of α-L- guluronic acid, nano zine oxide in parts by weight
1-4 parts, 2-4 parts of polyvinyl alcohol, 1-3 parts of lignin, 10-20 parts of hydroxypropyl chitosan, Grape Seed Extract Procyanidin 4-10
Part, 3-9 parts of calcium chloride, 2-6 parts of sodium alginate.
2. realizing a kind of preparation method of antimicrobial health care function scrambled eggs fabric described in claim 1, it is characterised in that: it is made
Preparation Method the following steps are included:
A, certain density hydroxypropyl sugar juice and calcium chloride solution are prepared, is mixed with the ratio of 2:1, hydroxypropyl base enclosure is made
Glycan calcium chloride mixed solution；
B, 2% sodium alginate soln is prepared, and Grape Seed Extract Procyanidin is dissolved according to a certain percentage wherein, in 300-
Under the at the uniform velocity stirring of 400r/min, 60 DEG C of sodium alginate solns are instilled rapidly in hydroxypropyl chitosan calcium chloride mixed solution,
Continue to stir 20min, sequentially adds α-L- guluronic acid, nano zine oxide, polyvinyl alcohol, lignin in whipping process, it
After be filtered, washed, hydroxypropyl chitosan and sodium alginate pass through positive and negative charge and attract, and polyelectrolyte film are formed, thus shape
At the sodium alginate-hydroxypropyl chitosan microcapsules for being rich in Grape Seed Extract Procyanidin, react as follows:
C, sodium alginate-hydroxypropyl chitosan microcapsules 10-30g/L, the low temperature that will be enriched in Grape Seed Extract Procyanidin are viscous
Mixture 20-30g/L, amido silicon oil 10-20g/L, bleeding agent 2-4g/L, are made into finishing fluid.
3. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 2, it is characterised in that: it is described
In step C, fabric is first immersed into 20min-30min in finishing fluid, is then arrived finishing fluid processing by the way of second dipping and rolling
On fabric, fabric is put into preliminary drying 10-20min in pre-baking box later, preliminary drying temperature is 80-85 DEG C, be put into baking oven later into
The drying of one step, temperature are 120-130 DEG C, time 5-8min, and pick-up is controlled 100%.
4. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 1, it is characterised in that: it is described
Weft yarn is coconut palm charcoal and lyocell scribbled, blending ratio 50-70:50-30.
5. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 2, it is characterised in that: it is described
In step A, the concentration of hydroxypropyl sugar juice is 2%-3%.
6. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 2, it is characterised in that: it is described
The concentration of calcium chloride solution is 2%-4% in step A.
7. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 2, it is characterised in that: it is described
Middle hydroxypropyl chitosan is o- hydroxypropyl chitosan in step A, and structure is as follows:
8. a kind of preparation method of antimicrobial health care function scrambled eggs fabric according to claim 2, it is characterised in that: it is described
The weight ratio of Grape Seed Extract Procyanidin and sodium alginate soln is 1:25-1:15 in step B.
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| CN111850738A (en) * | 2020-07-03 | 2020-10-30 | 浙江裕源纺织有限公司 | DTY (draw textured yarn) containing anti-ultraviolet agent and production process thereof |
| CN114960183A (en) * | 2022-05-12 | 2022-08-30 | 浙江艺纺纺织品有限公司 | Production process of antibacterial home textile fabric |
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| CN111850738A (en) * | 2020-07-03 | 2020-10-30 | 浙江裕源纺织有限公司 | DTY (draw textured yarn) containing anti-ultraviolet agent and production process thereof |
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Application publication date: 20190614 |