CN111719193A - Natural moxa fiber and preparation method thereof - Google Patents
Natural moxa fiber and preparation method thereof Download PDFInfo
- Publication number
- CN111719193A CN111719193A CN202010561959.8A CN202010561959A CN111719193A CN 111719193 A CN111719193 A CN 111719193A CN 202010561959 A CN202010561959 A CN 202010561959A CN 111719193 A CN111719193 A CN 111719193A
- Authority
- CN
- China
- Prior art keywords
- fiber
- natural
- cellulose
- moxa
- natural moxa
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F2/00—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof
- D01F2/06—Monocomponent artificial filaments or the like of cellulose or cellulose derivatives; Manufacture thereof from viscose
- D01F2/08—Composition of the spinning solution or the bath
- D01F2/10—Addition to the spinning solution or spinning bath of substances which exert their effect equally well in either
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D1/00—Treatment of filament-forming or like material
- D01D1/02—Preparation of spinning solutions
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/06—Wet spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
Abstract
The invention discloses a natural moxa fiber and a preparation method thereof, wherein the natural moxa fiber is prepared from the following raw materials in percentage by weight: 1 to 30 percent of natural moxa superfine powder, 0.1 to 8 percent of fiber reinforcing agent and the balance of natural regenerated cellulose, wherein the fiber reinforcing agent is cellulose esterified derivative or cellulose etherified derivative. The invention also specifically discloses a preparation method of the natural moxa fiber. The natural moxa fiber provided by the invention has a natural moxa effect, the physical index of the fiber reaches or exceeds that of the conventional viscose fiber due to the unique formula design, and the product is soft and smooth in hand feeling, bright and attractive in appearance and is an ideal material for manufacturing home textiles, fashionable underwear, scarves, infants and old people clothes.
Description
Technical Field
The invention belongs to the technical field of spinning, and particularly relates to natural moxa fiber and a preparation method thereof.
Background
The unique aromatic components of the wormwood mainly comprise micromolecular volatile terpenoid compounds, and also comprise aliphatic compounds and micromolecular aromatic compounds, so that the wormwood has a special fragrance, can purify air, has the functions of aromatic resuscitation, and can make human head and brain clear, improve hearing and eyesight and improve memory by normal smell. The modern medical pharmacology proves that the wormwood is an antibacterial and antiviral drug, has the effects of inhibiting and killing germs, preventing and treating respiratory system diseases and preventing cold. The moxa leaves are dried in the sun and smashed to obtain moxa wool, the moxa wool is made into fibers, and the clothes made of the fibers not only have the mosquito repellent effect, but also can smooth qi and blood of the whole body, improve the blood circulation of a human body, improve the immunity of the human body, and have a good health care effect.
In the prior art, there are patents disclosing the technology of making wormwood extract into textile fiber, for example, the invention patent application with application number 201610216440.X discloses a preparation method of wormwood antibacterial viscose fiber, wherein wormwood is cooked in water, the cooking liquor obtained after cooking is filtered to obtain wormwood extracting solution, and the wormwood extracting solution is added in the process of alkaline leaching or dissolving plant pulp or in the spinning stock solution to obtain antibacterial fiber. The invention patent application with the application number of 201810246695.X discloses a preparation method of wormwood fiber applied to home textile fabrics, which comprises the steps of washing wormwood, removing impurities, grinding, adding a solution with the concentration of 62-68% of ethanol, cooking, soaking to extract wormwood liquid, and blending and spinning the extracted wormwood liquid and a viscose spinning solution to prepare the wormwood-containing fiber. The invention application with application number 201510151268.X discloses a health care functional wormwood viscose fiber and a preparation method thereof, wherein the diameter and the leaves of wormwood are subjected to impurity removal, the wormwood powder and a dispersing agent are mechanically ground into wormwood powder, the wormwood powder and the dispersing agent are added into water according to a certain proportion to prepare wormwood aqueous emulsion, the wormwood aqueous emulsion is added into viscose according to a certain proportion in a cellulose sulfonate dissolving process, the wormwood aqueous emulsion is fully mixed and dissolved to prepare spinning solution, and then the wormwood viscose staple fiber or the wormwood viscose filament with various health care functions of antibiosis, bacteriostasis, hemostasis, allergy resistance and the like is prepared through a certain spinning process. And the requirements of downstream fabric manufacturing are difficult to meet. The invention patent application with the application number of 201510442140.9 provides a preparation method of wormwood rod-based viscose rayon fiber, which comprises the steps of preparing wormwood rod pulp by using wormwood rods as a raw material, further preparing wormwood rod pulp spinning solution by using the wormwood rod pulp, uniformly mixing the wormwood rod pulp spinning solution with common viscose prepared by using common cellulose pulp as a raw material, filtering the blended viscose, introducing the filtered viscose into a coagulating bath for spinning and forming, and then drawing and post-treating through silk strips to obtain the wormwood rod-based viscose rayon fiber. Although the technology can produce fiber, firstly, the moxa stick is required to be made into pulp, and the pulp is prepared by putting the moxa stick and alkali into a rotary spherical digester for papermaking together in the manufacturing process and steaming the moxa stick for a period of time under the conditions of high temperature and high pressure, so that the alpha-cellulose contained in the moxa stick is mainly extracted in the process, the main active ingredients in the moxa are destroyed early, and the manufactured fiber is difficult to show the special energy efficiency of the moxa. .
Disclosure of Invention
The invention solves the technical problem of providing natural moxa fiber and a preparation method thereof.
The invention adopts the following technical scheme for solving the technical problems, and the natural moxa fiber is characterized by being prepared from the following raw materials in percentage by weight: 1 to 30 percent of natural moxa superfine powder, 0.1 to 8 percent of fiber reinforcing agent and the balance of natural regenerated cellulose, wherein the fiber reinforcing agent is cellulose esterified derivative or cellulose etherified derivative.
Further limited, the natural moxa ultra-fine powder is obtained by separating and extracting natural moxa, and the particle size of the natural moxa ultra-fine powder is less than or equal to 2 mu m.
Further defined, the cellulose esterified derivative is cellulose acetate or cellulose acetate butyrate.
Further defined, the cellulolated derivative is hydroxymethyl cellulose, carboxymethyl cellulose, hydroxyethyl cellulose, cyanoethyl cellulose, hydroxypropyl cellulose, or hydroxypropyl methyl cellulose.
The preparation method of the natural moxa fiber is characterized by comprising the following specific steps: the natural moxa incense fiber is prepared by adopting natural regenerated cellulose as a base material, preparing a spinning glue solution through a glue preparation process, adding natural moxa superfine powder into a water emulsion of a fiber reinforcing agent, fully mixing to form a uniform and stable dispersed emulsion, then adding the dispersed emulsion into the spinning glue solution at a constant speed, fully mixing under the mechanical action, and forming through an acid bath to obtain the natural moxa incense fiber.
Compared with the prior art, the invention has the following beneficial effects and advantages: the natural moxa fiber provided by the invention has a natural moxa effect, the physical index of the fiber reaches or exceeds that of the conventional viscose fiber due to the unique formula design, and the product is soft and smooth in hand feeling, bright and attractive in appearance and is an ideal material for manufacturing home textiles, fashionable underwear, scarves, infants and old people clothes. Because the fiber base material is the natural regenerated cellulose fiber, the moxa is tightly combined with the cellulose base material under the action of the fiber reinforcing agent, the manufacturing process is simple, the physical indexes of the fiber can be ensured, and the manufactured moxa fiber has good moisture absorption, sweat releasing and heat preservation properties, has the effects of repelling mosquitoes and preventing mites and can be used as a raw material of army field clothing and bedding.
Detailed Description
The present invention is described in further detail below with reference to examples, but it should not be construed that the scope of the above subject matter of the present invention is limited to the following examples, and that all the technologies realized based on the above subject matter of the present invention belong to the scope of the present invention.
Example 1
81Kg of natural regenerated cellulose is used as a base material, a spinning glue solution is prepared by a glue making process, 15Kg of natural moxa superfine powder with the grain size less than or equal to 2 mu m is added into aqueous emulsion containing 4Kg of cellulose acetate butyrate as a fiber reinforcing agent, uniform and stable dispersion emulsion is formed by full mixing, then the dispersion emulsion is added into the spinning glue solution at a constant speed, the full mixing purpose is achieved by mechanical action, and the natural moxa fiber is obtained by acid bath forming and spinning.
Example 2
The natural moxa fiber is prepared by adopting 64Kg of natural regenerated cellulose as a base material through a glue making process to prepare a spinning glue solution, adding 28Kg of natural moxa superfine powder with the particle size of less than or equal to 2 mu m into aqueous emulsion containing 8Kg of fiber reinforcing agent hydroxymethyl cellulose, fully mixing to form uniform and stable dispersed emulsion, then adding the dispersed emulsion into the spinning glue solution at a constant speed, achieving the purpose of fully mixing through mechanical action, and spinning through acid bath molding to obtain the natural moxa fiber.
Example 3
The natural moxa incense fiber is prepared by adopting 98.8Kg of natural regenerated cellulose as a base material, preparing a spinning glue solution through a glue preparation process, adding 1Kg of natural moxa superfine powder with the particle size of less than or equal to 2 mu m into aqueous emulsion containing 0.2Kg of fiber reinforcing agent hydroxypropyl methyl cellulose, fully mixing to form uniform and stable dispersed emulsion, then adding the dispersed emulsion into the spinning glue solution at a constant speed, achieving the purpose of fully mixing through mechanical action, and spinning through acid bath molding to obtain the natural moxa incense fiber.
The foregoing embodiments illustrate the principles, principal features and advantages of the invention, and it will be understood by those skilled in the art that the invention is not limited to the foregoing embodiments, which are merely illustrative of the principles of the invention, and that various changes and modifications may be made therein without departing from the scope of the principles of the invention.
Claims (5)
1. The natural moxa fiber is characterized by being prepared from the following raw materials in percentage by weight: 1 to 30 percent of natural moxa superfine powder, 0.1 to 8 percent of fiber reinforcing agent and the balance of natural regenerated cellulose, wherein the fiber reinforcing agent is cellulose esterified derivative or cellulose etherified derivative.
2. The natural moxa fiber of claim 1, wherein: the natural moxa superfine powder is obtained by separating and extracting natural moxa, and the particle size of the natural moxa superfine powder is less than or equal to 2 mu m.
3. The natural moxa fiber of claim 1, wherein: the cellulose esterified derivative is cellulose acetate or cellulose acetate butyrate.
4. The natural moxa fiber of claim 1, wherein: the cellulose etherified derivative is hydroxymethyl cellulose, carboxymethyl cellulose, hydroxyethyl cellulose, cyanoethyl cellulose, hydroxypropyl cellulose or hydroxypropyl methyl cellulose.
5. A preparation method of the natural moxa fiber according to any one of claims 1 to 4, characterized by comprising the following steps: the natural moxa incense fiber is prepared by adopting natural regenerated cellulose as a base material, preparing a spinning glue solution through a glue preparation process, adding natural moxa superfine powder into a water emulsion of a fiber reinforcing agent, fully mixing to form a uniform and stable dispersed emulsion, then adding the dispersed emulsion into the spinning glue solution at a constant speed, fully mixing under the mechanical action, and forming through an acid bath to obtain the natural moxa incense fiber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010561959.8A CN111719193A (en) | 2020-06-18 | 2020-06-18 | Natural moxa fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010561959.8A CN111719193A (en) | 2020-06-18 | 2020-06-18 | Natural moxa fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN111719193A true CN111719193A (en) | 2020-09-29 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202010561959.8A Pending CN111719193A (en) | 2020-06-18 | 2020-06-18 | Natural moxa fiber and preparation method thereof |
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| CN (1) | CN111719193A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114311769A (en) * | 2021-11-19 | 2022-04-12 | 青铜峡市华峰塑胶有限公司 | Method for producing ton bag |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003138483A (en) * | 2001-10-30 | 2003-05-14 | Unitika Ltd | Biodegradable fiber containing extracted solution of mugwort |
| CN104963026A (en) * | 2015-07-24 | 2015-10-07 | 湖北蕲艾堂科技有限公司 | Preparation method of wormwood-stem-based viscose rayon fiber |
| CN105316785A (en) * | 2015-12-04 | 2016-02-10 | 威海皓菲集团有限公司 | Preparation method of Chinese mugwort fibers |
| CN106149082A (en) * | 2015-04-02 | 2016-11-23 | 江苏南纬悦达纺织研究院有限公司 | A kind of Folium Artemisiae Argyi viscose rayon and preparation method thereof |
-
2020
- 2020-06-18 CN CN202010561959.8A patent/CN111719193A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003138483A (en) * | 2001-10-30 | 2003-05-14 | Unitika Ltd | Biodegradable fiber containing extracted solution of mugwort |
| CN106149082A (en) * | 2015-04-02 | 2016-11-23 | 江苏南纬悦达纺织研究院有限公司 | A kind of Folium Artemisiae Argyi viscose rayon and preparation method thereof |
| CN104963026A (en) * | 2015-07-24 | 2015-10-07 | 湖北蕲艾堂科技有限公司 | Preparation method of wormwood-stem-based viscose rayon fiber |
| CN105316785A (en) * | 2015-12-04 | 2016-02-10 | 威海皓菲集团有限公司 | Preparation method of Chinese mugwort fibers |
Non-Patent Citations (2)
| Title |
|---|
| 夏建明 等: "《染整工艺学 第1册》", 31 July 2004, 中国纺织出版社 * |
| 高秀丽 等: "艾草纤维性能测试分析", 《纺织检测与标准》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114311769A (en) * | 2021-11-19 | 2022-04-12 | 青铜峡市华峰塑胶有限公司 | Method for producing ton bag |
| CN114311769B (en) * | 2021-11-19 | 2023-11-03 | 青铜峡市华峰塑胶有限公司 | Ton bag production method |
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Application publication date: 20200929 |
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