CN105969502A - Drawing oil for quick drawing of enameled wire - Google Patents

Drawing oil for quick drawing of enameled wire Download PDF

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Publication number
CN105969502A
CN105969502A CN201610309506.XA CN201610309506A CN105969502A CN 105969502 A CN105969502 A CN 105969502A CN 201610309506 A CN201610309506 A CN 201610309506A CN 105969502 A CN105969502 A CN 105969502A
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China
Prior art keywords
parts
acid
wire drawing
drawing oil
oil
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Pending
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CN201610309506.XA
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Chinese (zh)
Inventor
张军
何孔田
唐兰花
何孔高
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ANHUI JIUHUA KIMRUN COPPER INDUSTRY Co Ltd
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ANHUI JIUHUA KIMRUN COPPER INDUSTRY Co Ltd
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Priority to CN201610309506.XA priority Critical patent/CN105969502A/en
Publication of CN105969502A publication Critical patent/CN105969502A/en
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
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    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
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    • C10M2207/04—Ethers; Acetals; Ortho-esters; Ortho-carbonates
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    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
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    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
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    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
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    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/08—Resistance to extreme temperature
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    • C10N2040/00—Specified use or application for which the lubricating composition is intended
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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Metal Extraction Processes (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses drawing oil for quick drawing of an enameled wire. The drawing oil is prepared from the following raw materials in parts by weight: 10 to 15 parts of fatty acid methyl ester, 10 to 15 parts of trimellitate, 8 to 16 parts of lauryl polyoxyethylene ether, 8 to 16 parts of sodium dodecyl benzene sulfonate, 8 to 16 parts of 3-methoxy-4-hydroxy cinnamic acid, 6.2 to 12.2 parts of geranium acid, 6.2 to 12.2 parts of adenosylmethionine, 4 to 8.5 parts of glycerol triacetate, 20 to 28 parts of soybean peptide, 55 to 68 parts of water and 10 to 18 parts of modified assistant. The drawing oil disclosed by the invention has very good lubricating performance and good drawing effect, can greatly shorten the drawing time of the enameled wire and enables the enameled wire after drawing to have good toughness, and the enameled wire has good surface compactness; the drawing oil disclosed by the invention is simple in preparation, can obviously reduce the production cost and can restrain infectious microbes from propagating, so that the damage of the infectious microbes to the drawing oil can be avoided; the drawing oil disclosed by the invention can resist low temperature, the drawing is not in solidification or is in half solidification under the environment of -10 DEG C and can still be used for drawing, and the use is very convenient.

Description

A kind of enamel-covered wire quick wire drawing wire drawing oil
Technical field
The present invention relates to wire drawing oil field, be specifically related to a kind of enamel-covered wire quick wire drawing wire drawing oil.
Background technology
Wire drawing oil, it is also that the one playing lubrication is oily as butter, but its viscosity The highest, silk can be pulled out if pullling, so referred to as wire drawing oil.Wire drawing oil is that a class is important Commercial auxiliaries, during wire drawing, drawing process, do efficient lubricant oil use, have lubrication, Clean, cooling, the effect such as antirust, assist metal flow, it is to avoid mould drags colored bracing wire, improve yield rate, Reduce and produce loss.Existing wire drawing oil is broadly divided into oiliness wire drawing oil and aqueous wire drawing oil, and this two class is drawn Silk oil cuts both ways when actually used, and such as oiliness wire drawing oil, to there is heat dispersion poor, cleans chip removal difficulty, The problems such as waste liquid difficult degradation, although and the wire drawing of aqueous oil heat dispersion excellent compared with oiliness wire drawing oil, but Lubricant effect is the most not fully up to expectations, it is difficult to group technological requirement is drawn in the wire drawing meeting various metals line.
Often cause enamel-covered wire to rupture owing to wire drawing liquid is of poor quality during enamel-covered wire wire drawing, or enamel-covered wire is tough Property poor, cause enamel-covered wire winding trouble, bring the biggest trouble to production and application.
Summary of the invention
The technical problem to be solved is to provide one can be greatly shortened the enamel-covered wire wire drawing time, The enamel-covered wire quick wire drawing wire drawing oil of low-temperature-resistant.
The technical problem to be solved realizes by the following technical solutions:
A kind of enamel-covered wire quick wire drawing wire drawing oil, is made up of the raw material of following weight portion: fatty acid methyl ester 10-15 part, trimellitate 10-15 part, polyoxyethylene lauryl ether 8-16 part, DBSA Sodium 8-16 part, ferulic acid 8-16 part, pelargonic acid 6.2-12.2 part, S-adenosine first Methyllanthionine 6.2-12.2 part, glycerol triacetate 4-8.5 part, soybean peptide 20-28 part, water 55-68 part, change Property auxiliary agent 10-18 part；
Described modified additive is made up of the raw material of following weight portion: calcium stearate 3-4 part, 1-amyl group-4- Furan hendecanoic acid 8-11 part, polyoxyethylene carboxylate 8-11 part, epoxy resin 8-11 part, lauric acid Glyceride polyoxyethylene ether 8-11 part, behenate 13-18 part, amyl acetate 13-18 part, stearic acid close Ammonium stearate 13-18 part, potassium iodide acetic acid 13-18 part, molybdenum bisuphide 2-6 part, isopropyl myristate 2-6 Part, polyethylene glycol laurate 4-6 part, octadecyldimethyl tertiary amine 4-6 part, deionized water 30-42 part；
The preparation method of described modified additive is, first calcium stearate, epoxy resin, molybdenum bisuphide is mixed Conjunction grinds to form 20-50 mesh powder, the powder obtained and 1-amyl group-4-furan hendecanoic acid, fatty acid polyoxy Vinyl acetate, glyceryl laurate ester polyoxyethylene ether, potassium iodide acetic acid mix, at 800-1200 rev/min Stir 30min under rotating speed, make emulsion standby；Behenate, amyl acetate, stearic acid are puted the palms together before one eight Acid ammonium, isopropyl myristate, polyethylene glycol laurate, octadecyldimethyl tertiary amine and deionization Water mix, be heated to 70 DEG C, then emulsion be added thereto, continue to be heated to 85 DEG C, the most again with 1200-1500 rev/min of rotating speed stirring 30min, stirring stands 2h after terminating, and obtains wire drawing oil.
A kind of enamel-covered wire quick wire drawing wire drawing oil, preparation method is as follows:
(1) fatty acid methyl ester, trimellitate, polyoxyethylene lauryl ether are mixed and heated to 60 DEG C, Be subsequently adding ferulic acid, pelargonic acid, S-adenosylmethionine, soybean peptide add again Heat is to 80 DEG C and keeps this temperature 3 minutes, standby after cooling；
(2) heat water to 70 DEG C, be subsequently adding dodecylbenzene sodium sulfonate, glycerol triacetate, then Use high-shear emulsion machine dispersion to process 50min, obtain mixed solution standby；
(3) step (1) and step (2) gained material being mixed with modified additive, stirring after standing is Obtain wire drawing oil.
The invention has the beneficial effects as follows: wire drawing oil lubricity of the present invention is the best, and wire-drawing effect is good, can be big The big shortening enamel-covered wire wire drawing time, and the enamel-covered wire good toughness after wire drawing can be made, enamelled wire surface causes Close property is good, and wire drawing oil of the present invention makes simple, can substantially reduce production cost, and wire drawing oil can suppress miscellaneous bacteria Grow, it is to avoid the miscellaneous bacteria destruction to wire drawing oil, and wire drawing oil low-temperature-resistant of the present invention, at the ring of-10 DEG C The drop-down silk oil in border does not solidifies or half solidification, still can be used for wire drawing, very easy to use.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of enamel-covered wire quick wire drawing wire drawing oil, is made up of the raw material of following weight portion (kilogram): fat Fatty acid methyl esters 12 parts, trimellitate 12 parts, polyoxyethylene lauryl ether 12 parts, DBSA 12 parts of sodium, ferulic acid 12 parts, pelargonic acid 9 parts, S-adenosylmethionine 9 parts, Glycerol triacetate 6 parts, soybean peptide 24 parts, 62 parts of water, modified additive 14 parts；
Described modified additive is made up of the raw material of following weight portion: calcium stearate 3 parts, 1-amyl group-4-furan Mutter hendecanoic acid 10 parts, polyoxyethylene carboxylate 10 parts, epoxy resin 10 parts, glyceryl laurate ester gather Oxygen vinyl Ether 10 parts, behenate 16 parts, amyl acetate 16 parts, stearic acid close ammonium stearate 16 parts, iodine Change potassium acetic acid 16 parts, molybdenum bisuphide 4 parts, isopropyl myristate 4 parts, polyethylene glycol laurate 5 parts, Octadecyldimethyl tertiary amine 5 parts, deionized water 36 parts；
The preparation method of described modified additive is, first calcium stearate, epoxy resin, molybdenum bisuphide is mixed Conjunction grinds to form 20-50 mesh powder, the powder obtained and 1-amyl group-4-furan hendecanoic acid, fatty acid polyoxy Vinyl acetate, glyceryl laurate ester polyoxyethylene ether, potassium iodide acetic acid mix, at 800-1200 rev/min Stir 30min under rotating speed, make emulsion standby；Behenate, amyl acetate, stearic acid are puted the palms together before one eight Acid ammonium, isopropyl myristate, polyethylene glycol laurate, octadecyldimethyl tertiary amine and deionization Water mix, be heated to 70 DEG C, then emulsion be added thereto, continue to be heated to 85 DEG C, the most again with 1200-1500 rev/min of rotating speed stirring 30min, stirring stands 2h after terminating, and obtains wire drawing oil.
A kind of enamel-covered wire quick wire drawing wire drawing oil, preparation method is as follows:
(1) fatty acid methyl ester, trimellitate, polyoxyethylene lauryl ether are mixed and heated to 60 DEG C, Be subsequently adding ferulic acid, pelargonic acid, S-adenosylmethionine, soybean peptide add again Heat is to 80 DEG C and keeps this temperature 3 minutes, standby after cooling；
(2) heat water to 70 DEG C, be subsequently adding dodecylbenzene sodium sulfonate, glycerol triacetate, then Use high-shear emulsion machine dispersion to process 50min, obtain mixed solution standby；
(3) step (1) and step (2) gained material being mixed with modified additive, stirring after standing is Obtain wire drawing oil.
Embodiment 2
A kind of enamel-covered wire quick wire drawing wire drawing oil, is made up of the raw material of following weight portion: fatty acid methyl ester 10 parts, trimellitate 10 parts, polyoxyethylene lauryl ether 8 parts, dodecylbenzene sodium sulfonate 8 parts, 3- Methoxyl group-4-hydroxycinnamic acid 8 parts, pelargonic acid 6.2 parts, S-adenosylmethionine 6.2 parts, glycerol three Acetas 4 parts, soybean peptide 20 parts, 55 parts of water, modified additive 10 parts；
Described modified additive is made up of the raw material of following weight portion: calcium stearate 3 parts, 1-amyl group-4-furan Mutter hendecanoic acid 8 parts, polyoxyethylene carboxylate 8 parts, epoxy resin 8 parts, glyceryl laurate ester polyoxy second 8 parts of alkene ether, behenate 13 parts, amyl acetate 13 parts, stearic acid close ammonium stearate 13 parts, potassium iodide vinegar Acid 13 parts, molybdenum bisuphide 2 parts, isopropyl myristate 2 parts, polyethylene glycol laurate 4 parts, octadecane Base dimethyl tertiary amine 4 parts, deionized water 30 parts；
The preparation method of described modified additive is, first calcium stearate, epoxy resin, molybdenum bisuphide is mixed Conjunction grinds to form 20-50 mesh powder, the powder obtained and 1-amyl group-4-furan hendecanoic acid, fatty acid polyoxy Vinyl acetate, glyceryl laurate ester polyoxyethylene ether, potassium iodide acetic acid mix, at 800-1200 rev/min Stir 30min under rotating speed, make emulsion standby；Behenate, amyl acetate, stearic acid are puted the palms together before one eight Acid ammonium, isopropyl myristate, polyethylene glycol laurate, octadecyldimethyl tertiary amine and deionization Water mix, be heated to 70 DEG C, then emulsion be added thereto, continue to be heated to 85 DEG C, the most again with 1200-1500 rev/min of rotating speed stirring 30min, stirring stands 2h after terminating, and obtains wire drawing oil.
A kind of enamel-covered wire quick wire drawing wire drawing oil, preparation method is as follows:
(1) fatty acid methyl ester, trimellitate, polyoxyethylene lauryl ether are mixed and heated to 60 DEG C, Be subsequently adding ferulic acid, pelargonic acid, S-adenosylmethionine, soybean peptide add again Heat is to 80 DEG C and keeps this temperature 3 minutes, standby after cooling；
(2) heat water to 70 DEG C, be subsequently adding dodecylbenzene sodium sulfonate, glycerol triacetate, then Use high-shear emulsion machine dispersion to process 50min, obtain mixed solution standby；
(3) step (1) and step (2) gained material being mixed with modified additive, stirring after standing is Obtain wire drawing oil.
Embodiment 3
A kind of enamel-covered wire quick wire drawing wire drawing oil, is made up of the raw material of following weight portion: fatty acid methyl ester 15 parts, trimellitate 15 parts, polyoxyethylene lauryl ether 16 parts, dodecylbenzene sodium sulfonate 16 parts, Ferulic acid 16 parts, pelargonic acid 12.2 parts, S-adenosylmethionine 12.2 parts, sweet Oil triacetate 8.5 parts, soybean peptide 28 parts, 68 parts of water, modified additive 18 parts；
Described modified additive is made up of the raw material of following weight portion: calcium stearate 4 parts, 1-amyl group-4-furan Mutter hendecanoic acid 11 parts, polyoxyethylene carboxylate 11 parts, epoxy resin 11 parts, glyceryl laurate ester gather Oxygen vinyl Ether 11 parts, behenate 18 parts, amyl acetate 18 parts, stearic acid close ammonium stearate 18 parts, iodine Change potassium acetic acid 18 parts, molybdenum bisuphide 6 parts, isopropyl myristate 6 parts, polyethylene glycol laurate 6 parts, Octadecyldimethyl tertiary amine 6 parts, deionized water 42 parts；
The preparation method of described modified additive is, first calcium stearate, epoxy resin, molybdenum bisuphide is mixed Conjunction grinds to form 20-50 mesh powder, the powder obtained and 1-amyl group-4-furan hendecanoic acid, fatty acid polyoxy Vinyl acetate, glyceryl laurate ester polyoxyethylene ether, potassium iodide acetic acid mix, at 800-1200 rev/min Stir 30min under rotating speed, make emulsion standby；Behenate, amyl acetate, stearic acid are puted the palms together before one eight Acid ammonium, isopropyl myristate, polyethylene glycol laurate, octadecyldimethyl tertiary amine and deionization Water mix, be heated to 70 DEG C, then emulsion be added thereto, continue to be heated to 85 DEG C, the most again with 1200-1500 rev/min of rotating speed stirring 30min, stirring stands 2h after terminating, and obtains wire drawing oil.
A kind of enamel-covered wire quick wire drawing wire drawing oil, preparation method is as follows:
(1) fatty acid methyl ester, trimellitate, polyoxyethylene lauryl ether are mixed and heated to 60 DEG C, Be subsequently adding ferulic acid, pelargonic acid, S-adenosylmethionine, soybean peptide add again Heat is to 80 DEG C and keeps this temperature 3 minutes, standby after cooling；
(2) heat water to 70 DEG C, be subsequently adding dodecylbenzene sodium sulfonate, glycerol triacetate, then Use high-shear emulsion machine dispersion to process 50min, obtain mixed solution standby；
(3) step (1) and step (2) gained material being mixed with modified additive, stirring after standing is Obtain wire drawing oil.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (2)

1. an enamel-covered wire quick wire drawing wire drawing oil, it is characterised in that by the raw material system of following weight portion Become: fatty acid methyl ester 10-15 part, trimellitate 10-15 part, polyoxyethylene lauryl ether 8-16 part, Dodecylbenzene sodium sulfonate 8-16 part, ferulic acid 8-16 part, pelargonic acid 6.2-12.2 part, S-adenosylmethionine 6.2-12.2 part, glycerol triacetate 4-8.5 part, soybean peptide 20-28 part, water 55-68 part, modified additive 10-18 part；
Described modified additive is made up of the raw material of following weight portion: calcium stearate 3-4 part, 1-amyl group-4- Furan hendecanoic acid 8-11 part, polyoxyethylene carboxylate 8-11 part, epoxy resin 8-11 part, lauric acid Glyceride polyoxyethylene ether 8-11 part, behenate 13-18 part, amyl acetate 13-18 part, stearic acid close Ammonium stearate 13-18 part, potassium iodide acetic acid 13-18 part, molybdenum bisuphide 2-6 part, isopropyl myristate 2-6 Part, polyethylene glycol laurate 4-6 part, octadecyldimethyl tertiary amine 4-6 part, deionized water 30-42 part；
The preparation method of described modified additive is, first calcium stearate, epoxy resin, molybdenum bisuphide is mixed Conjunction grinds to form 20-50 mesh powder, the powder obtained and 1-amyl group-4-furan hendecanoic acid, fatty acid polyoxy Vinyl acetate, glyceryl laurate ester polyoxyethylene ether, potassium iodide acetic acid mix, at 800-1200 rev/min Stir 30min under rotating speed, make emulsion standby；Behenate, amyl acetate, stearic acid are puted the palms together before one eight Acid ammonium, isopropyl myristate, polyethylene glycol laurate, octadecyldimethyl tertiary amine and deionization Water mix, be heated to 70 DEG C, then emulsion be added thereto, continue to be heated to 85 DEG C, the most again with 1200-1500 rev/min of rotating speed stirring 30min, stirring stands 2h after terminating, and obtains wire drawing oil.
2. a kind of enamel-covered wire quick wire drawing wire drawing oil as claimed in claim 1, it is characterised in that system Preparation Method is as follows:
(1) fatty acid methyl ester, trimellitate, polyoxyethylene lauryl ether are mixed and heated to 60 DEG C, Be subsequently adding ferulic acid, pelargonic acid, S-adenosylmethionine, soybean peptide add again Heat is to 80 DEG C and keeps this temperature 3 minutes, standby after cooling；
(2) heat water to 70 DEG C, be subsequently adding dodecylbenzene sodium sulfonate, glycerol triacetate, then Use high-shear emulsion machine dispersion to process 50min, obtain mixed solution standby；
(3) step (1) and step (2) gained material being mixed with modified additive, stirring after standing is Obtain wire drawing oil.
CN201610309506.XA 2016-05-10 2016-05-10 Drawing oil for quick drawing of enameled wire Pending CN105969502A (en)

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CN107603714A (en) * 2017-11-07 2018-01-19 刘兴满 Magnetic drive pump bearing lubricating fluid
CN107603715A (en) * 2017-11-07 2018-01-19 刘兴满 Water pump lubricating fluid
CN107892977A (en) * 2017-11-07 2018-04-10 刘兴满 Diving pump rotor lubricating fluid
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CN116727475A (en) * 2023-06-19 2023-09-12 沈阳宏远电磁线股份有限公司 Copper wire drawing process based on modified wire drawing liquid treatment
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CN103966005A (en) * 2014-03-28 2014-08-06 安徽九华金润铜业有限公司 Drawing fluid for rapidly drawing copper wire
CN103992868A (en) * 2014-04-25 2014-08-20 蚌埠市正园电子科技有限公司 High temperature resistant high speed wire drawing oil

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CN103614219A (en) * 2013-10-21 2014-03-05 全威（铜陵）铜业科技有限公司 High-temperature wire drawing lubricant and preparation method thereof
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CN107603714A (en) * 2017-11-07 2018-01-19 刘兴满 Magnetic drive pump bearing lubricating fluid
CN107603715A (en) * 2017-11-07 2018-01-19 刘兴满 Water pump lubricating fluid
CN107892977A (en) * 2017-11-07 2018-04-10 刘兴满 Diving pump rotor lubricating fluid
CN108587744A (en) * 2018-05-31 2018-09-28 广州特鲁勃润滑技术有限公司 A kind of metal wire-drawing oil and its production technology
CN116727475A (en) * 2023-06-19 2023-09-12 沈阳宏远电磁线股份有限公司 Copper wire drawing process based on modified wire drawing liquid treatment
CN116727475B (en) * 2023-06-19 2023-11-14 沈阳宏远电磁线股份有限公司 Copper wire drawing process based on modified wire drawing liquid treatment
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CN117070131B (en) * 2023-10-12 2024-03-01 广州境好新材料有限公司 Single-component waterborne epoxy emulsion coating and preparation method thereof

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