CN103992867B - A kind of anti-oxidant wire drawing oil containing origanum oil - Google Patents
A kind of anti-oxidant wire drawing oil containing origanum oil Download PDFInfo
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- CN103992867B CN103992867B CN201410174118.6A CN201410174118A CN103992867B CN 103992867 B CN103992867 B CN 103992867B CN 201410174118 A CN201410174118 A CN 201410174118A CN 103992867 B CN103992867 B CN 103992867B
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- origanum
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- 238000005491 wire drawing Methods 0.000 title claims abstract description 35
- 235000011203 Origanum Nutrition 0.000 title claims abstract description 20
- 241001529744 Origanum Species 0.000 title claims abstract description 20
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 10
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 10
- 235000006708 antioxidants Nutrition 0.000 title claims abstract description 10
- 239000003921 oil Substances 0.000 claims abstract description 49
- 235000019198 oils Nutrition 0.000 claims abstract description 49
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000012424 soybean oil Nutrition 0.000 claims abstract description 10
- 239000003549 soybean oil Substances 0.000 claims abstract description 10
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical compound CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 8
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims abstract description 7
- QCJQWJKKTGJDCM-UHFFFAOYSA-N [P].[S] Chemical compound [P].[S] QCJQWJKKTGJDCM-UHFFFAOYSA-N 0.000 claims abstract description 7
- -1 alkyl zinc salt Chemical class 0.000 claims abstract description 7
- 239000003225 biodiesel Substances 0.000 claims abstract description 7
- 229940114930 potassium stearate Drugs 0.000 claims abstract description 7
- ANBFRLKBEIFNQU-UHFFFAOYSA-M potassium;octadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCCCC([O-])=O ANBFRLKBEIFNQU-UHFFFAOYSA-M 0.000 claims abstract description 7
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 5
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 5
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims abstract description 4
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims abstract description 4
- 235000010234 sodium benzoate Nutrition 0.000 claims abstract description 3
- 239000004299 sodium benzoate Substances 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 229920001285 xanthan gum Polymers 0.000 claims description 8
- 238000002360 preparation method Methods 0.000 claims description 7
- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 229910021389 graphene Inorganic materials 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims description 5
- 239000000839 emulsion Substances 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- 239000004115 Sodium Silicate Substances 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 3
- 235000019795 sodium metasilicate Nutrition 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 3
- 229940082509 xanthan gum Drugs 0.000 claims description 3
- 235000010493 xanthan gum Nutrition 0.000 claims description 3
- 239000000230 xanthan gum Substances 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000012467 final product Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 7
- 229910052751 metal Inorganic materials 0.000 abstract description 4
- 239000002184 metal Substances 0.000 abstract description 4
- 150000002739 metals Chemical class 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract description 3
- 238000007254 oxidation reaction Methods 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract description 2
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 239000002199 base oil Substances 0.000 abstract description 2
- 238000003860 storage Methods 0.000 abstract description 2
- 230000006866 deterioration Effects 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000010687 lubricating oil Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000346 nonvolatile oil Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
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- Lubricants (AREA)
Abstract
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of anti-oxidant wire drawing oil containing origanum oil, wire drawing oil of the present invention is made up of the raw material of following weight portion: epoxidized soybean oil 120-140, biodiesel 45-60, Decanol 5-8, sulphur phosphorus brothers alkyl zinc salt 1-2, origanum oil 1-2, isomerous tridecanol polyoxyethylene ether 10-12, potassium stearate 0.1-0.2, Sodium Benzoate 0.2-0.3, sulfide isobutene 1-2, auxiliary agent 2-3; Wire drawing oil of the present invention has added especially the origanum oil with excellent antibacterial oxidation resistance in formula, effectively improve the problem of the epoxidized soybean oil in base oil with oxidation deterioration, again in conjunction with other class additive, make wire drawing oil ring prepared by the present invention protect easily degraded, thermally-stabilised good, more resistance to storage, the low greasy property of cost is excellent, and wire drawing, the drawing process that can meet various metals wire rod are used.
Description
Technical field
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of anti-oxidant wire drawing oil and preparation work thereof containing origanum oilSkill.
Background technology
Wire drawing oil is the important industrial auxiliary agent of a class, in wire drawing, drawing process process, does high-efficiency lubricatingOil use, has lubricated, cleaning, the effect such as cooling, antirust, assists metal flow, avoids mould to drag colored bracing wire,Improve yield rate, reduce production loss. Existing wire drawing oil is mainly divided into oiliness wire drawing oil and water-based wire drawing oil,This two classes wire drawing oil cuts both ways in the time that reality is used, and as oiliness wire drawing oil exists heat dispersion poor, cleans chip removalDifficulty, the problems such as waste liquid difficult degradation, although and the wire drawing oil heat dispersion of water-based is good compared with oiliness wire drawing oil,Be that lubricant effect is not fully up to expectations, the wire drawing that is difficult to meet various metals line is drawn and is dialled technological requirement, therefore forImprove enterprise machined level, reduce production costs, need to improve wire drawing oil formula and technique, makeIt reaches good serviceability.
Summary of the invention
The object of the invention is to, a kind of anti-oxidant wire drawing oil containing origanum oil is provided, improve wire drawing oil antibacterial anti-Rotten performance, to achieve these goals, the technical solution used in the present invention is as follows:
Containing an anti-oxidant wire drawing oil for origanum oil, it is characterized in that, material of the present invention is former by following weight portionMaterial is made: epoxidized soybean oil 120-140, biodiesel 45-60, Decanol 5-8, sulphur phosphorus brothers zinc alkylSalt 1-2, origanum oil 1-2, isomerous tridecanol polyoxyethylene ether 10-12, potassium stearate 0.1-0.2, benzoic acidSodium 0.2-0.3, sulfide isobutene 1-2, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight portion:Butyl stearate 12-15, Graphene 1-2, sodium metasilicate 1-2, xanthans 10-12, lauryl alcohol polyethylene glycol oxideEther 4-5, deionized water are appropriate; Preparation method is: first by butyl stearate, add ethoxylated dodecyl alcohol,Graphene stirs 20-30min under 1000-1500 rev/min, makes emulsion for subsequent use, then by xanthansMix with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally by waterSolution, emulsion and other residual components are mixed, and continue to stir with 1000-1500 rev/min of rotating speed15-20min, stirs and finishes rear standing 2-4h, to obtain final product.
Described a kind of anti-oxidant wire drawing oil containing origanum oil, its preparation technology is:
(1) first Decanol, sulphur phosphorus brothers alkyl zinc salt, potassium stearate, origanum oil are mixed, fully stir20-30min, mixed solution is for subsequent use;
(2) epoxidized soybean oil, biodiesel are mixed, be heated to 50-60 DEG C, add isomerous tridecanol polyoxyVinethene, stirs 20-30min, adds subsequently the material of step (1), step (2) gained and other is surplus againRemaining composition, continues to stir 60-80min, after stirring finishes, through naturally cooling to room temperature, gets product.
The wire drawing oil that the present invention prepares, mixes as base oil using epoxidized soybean oil, biodiesel, possessesGood greasy property, Viscosity Index is high, and lightning is high, and environmentally friendly easy degraded, but, this containingIn use there is the oxidizable problem such as rotten in the wire drawing oil of vegetable oil, in order to improve the anti-of epoxidized soybean oilOxidability has been added especially origanum oil in formula, and origanum oil is a class yellowish red color or brownish red essential oil, energyBe dissolved in most of non-volatile oils, having very strong is sterilization oxidation resistance, can effectively slow down epoxyThe oxidizing process of soybean oil in storage process, the service life of prolongation wire drawing oil, then in conjunction with other additive,Not only environmental protection low toxicity of lubricating oil prepared by the present invention, Heat stability is good, greasy property is good, and more resistance to storageDeposit, longer service life, wire drawing, the drawing process that can be applicable to various metals material are used.
Detailed description of the invention
Embodiment
The present embodiment wire drawing oil by following weight portion (kilogram) raw material make: epoxidized soybean oil 140, biologyDiesel oil 50, Decanol 8, sulphur phosphorus brothers alkyl zinc salt 1, origanum oil 2, isomerous tridecanol polyoxyethylene ether 10,Potassium stearate 0.1, Sodium Benzoate 0.3, sulfide isobutene 1, auxiliary agent 3; Described auxiliary agent is by following weight portionRaw material make: butyl stearate 15, Graphene 1, sodium metasilicate 2, xanthans 10, laruyl alcohol polyoxy secondAlkene ether 4, deionized water are appropriate; Preparation method is: first by butyl stearate, add ethoxylated dodecyl alcohol,Graphene stirs 20min under 1500 revs/min, makes emulsion for subsequent use, then by xanthans and appropriateDeionized water is mixed, and is mixed with mass concentration and is 70% xanthan gum solution, finally by the aqueous solution, emulsionAnd other residual components mixing, continue to stir 15min with 1500 revs/min of rotating speeds, stir and finish rear standing 3h,Obtain.
Described a kind of anti-oxidant wire drawing oil containing origanum oil, its preparation technology is:
(1) first Decanol, sulphur phosphorus brothers alkyl zinc salt, potassium stearate, origanum oil are mixed, fully stir30min, mixed solution is for subsequent use;
(2) epoxidized soybean oil, biodiesel are mixed, be heated to 50-60 DEG C, add isomerous tridecanol polyoxyVinethene, stirs 30min, adds subsequently material and other residue of step (1), step (2) gained againComposition, continues to stir 80min, after stirring finishes, through naturally cooling to room temperature, gets product.
Wire drawing oil of the present invention can stablize at ambient temperature deposit at least one year, during this time without precipitating, lamination;Concrete each performance indications are as follows:
Claims (1)
1. the anti-oxidant wire drawing oil containing origanum oil, it is characterized in that, this wire drawing oil is made up of the raw material of following weight portion: epoxidized soybean oil 120-140, biodiesel 45-60, Decanol 5-8, sulphur phosphorus brothers alkyl zinc salt 1-2, origanum oil 1-2, isomerous tridecanol polyoxyethylene ether 10-12, potassium stearate 0.1-0.2, Sodium Benzoate 0.2-0.3, sulfide isobutene 1-2, auxiliary agent 2-3; Described auxiliary agent is made up of the raw material of following weight portion: butyl stearate 12-15, Graphene 1-2, sodium metasilicate 1-2, xanthans 10-12, ethoxylated dodecyl alcohol 4-5, deionized water are appropriate; Preparation method is: first will in butyl stearate, add ethoxylated dodecyl alcohol, Graphene, under 1000-1500 rev/min, stir 20-30min, make emulsion for subsequent use, again xanthans is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion and other residual components mixed, continue to stir 15-20min with 1000-1500 rev/min of rotating speed, stirring finishes rear standing 2-4h, to obtain final product;
Described a kind of anti-oxidant wire drawing oil containing origanum oil, its preparation technology is as follows:
(1) first Decanol, sulphur phosphorus brothers alkyl zinc salt, potassium stearate, origanum oil are mixed, fully stir 20-30min, mixed solution is for subsequent use;
(2) epoxidized soybean oil, biodiesel are mixed, be heated to 50-60 DEG C, add isomerous tridecanol polyoxyethylene ether, stir 20-30min, add again subsequently material and other residual components of step (1), step (2) gained, continue to stir 60-80min, after stirring finishes, through naturally cooling to room temperature, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410174118.6A CN103992867B (en) | 2014-04-25 | 2014-04-25 | A kind of anti-oxidant wire drawing oil containing origanum oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410174118.6A CN103992867B (en) | 2014-04-25 | 2014-04-25 | A kind of anti-oxidant wire drawing oil containing origanum oil |
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| Publication Number | Publication Date |
|---|---|
| CN103992867A CN103992867A (en) | 2014-08-20 |
| CN103992867B true CN103992867B (en) | 2016-05-18 |
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| CN201410174118.6A Active CN103992867B (en) | 2014-04-25 | 2014-04-25 | A kind of anti-oxidant wire drawing oil containing origanum oil |
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| CN111423924B (en) * | 2020-04-03 | 2022-06-28 | 贵州水钢金属科技有限公司 | Improved wire drawing oil and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JP4792216B2 (en) * | 2004-11-01 | 2011-10-12 | Ｊｘ日鉱日石エネルギー株式会社 | Oil composition for cutting / grinding with ultra-trace oil supply |
| CN101386804A (en) * | 2008-10-11 | 2009-03-18 | 佛山市威奇电工材料有限公司 | Drawing oil special for aluminum wire and production process thereof |
| CN101838579B (en) * | 2010-03-31 | 2013-04-24 | 宜春德源欣茂铝业有限公司 | Special aluminum wire drawing oil used for aluminum wires and production method thereof |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Oregano-oil-containing antioxidant wire drawing oil Effective date of registration: 20191206 Granted publication date: 20160518 Pledgee: Bengbu Science and Technology Financing Guarantee Co., Ltd. Pledgor: Bengbu Zhengyuan Electronic Technology Co., Ltd. Registration number: Y2019990000670 |
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Address after: 233000 No. 1259 Changqing South Road, hi tech Zone, Anhui, Bengbu Patentee after: Bengbu Zhengyuan Electronic Technology Co., Ltd Address before: 233000 No. 1259 Changqing South Road, hi tech Zone, Anhui, Bengbu Patentee before: BENGBU ZHENGYUAN ELECTRONIC TECHNOLOGY Co.,Ltd. |
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Date of cancellation: 20220107 Granted publication date: 20160518 Pledgee: Bengbu Science and Technology Financing Guarantee Co.,Ltd. Pledgor: BENGBU ZHENGYUAN ELECTRONIC TECHNOLOGY Co.,Ltd. Registration number: Y2019990000670 |
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Denomination of invention: Antioxidant wire drawing oil containing oregano oil Effective date of registration: 20220228 Granted publication date: 20160518 Pledgee: Bengbu Science and Technology Financing Guarantee Co.,Ltd. Pledgor: Bengbu Zhengyuan Electronic Technology Co.,Ltd. Registration number: Y2022980001890 |